VOSO4·xH2O, 1,3,5-benzene tricarboxylic acid (BTC), adenine, DMF, ethanol (≥99.5%) and, methanol (99.8%) were purchased from Sigma-Aldrich and used as supplied. All aqueous solutions were prepared with deionized water.
1 3 5 benzene tricarboxylic acid btc
Manufactured by Merck Group
Sourced in France
1,3,5-benzene tricarboxylic acid (BTC) is a chemical compound that consists of a benzene ring with three carboxylic acid functional groups attached. It is a white crystalline solid and is used as a starting material in various chemical synthesis processes.
Automatically generated - may contain errors
Lab products found in correlation
Ethanol, by Merck Group (3 mentions)
N n dimethylformamide (dmf), by Merck Group (3 mentions)
Ni no3 2 6h2o, by Merck Group (2 mentions)
Co no3 2 6h2o, by Merck Group (2 mentions)
Methylcyclohexane, by Merck Group (2 mentions)
Cu no3 2 3h2o, by Merck Group (2 mentions)
Fecl2.6h2o, by Merck Group (2 mentions)
Toluene, by Merck Group (2 mentions)
Acetonitrile, by Merck Group (2 mentions)
Zn no3 2 6h2o, by Merck Group (2 mentions)
Cyclohexane, by Merck Group (2 mentions)
Voso4 xh2o, by Merck Group (1 mentions)
Methanol, by Merck Group (1 mentions)
Adenine, by Merck Group (1 mentions)
Iron 3 chloride hexahydrate, by Thermo Fisher Scientific (1 mentions)
Absolute ethanol, by Carlo Erba (1 mentions)
Deferoxamine mesylate salt, by Merck Group (1 mentions)
Sodium phosphate monobasic dihydrate, by Merck Group (1 mentions)
Doxorubicin, by Merck Group (1 mentions)
Trimethyl trimesate, by Merck Group (1 mentions)
5 protocols using 1 3 5 benzene tricarboxylic acid btc
1
Synthesis of Metal-Organic Frameworks
2
Synthesis of Metal-Organic Frameworks
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EXAMPLE 1
Chemicals and Materials
All reagents were used as purchased without further purification. 1,3,5-benzene tricarboxylic acid (BTC), Cu(NO3)2.3H2O, Co(NO3)2.6H2O, Ni(NO3)2.6H2O, Zn(NO3)2.6H2O, FeCl2.6H2O, N,N-dimethylformamide (DMF) and ethanol were obtained from Sigma-Aldrich. Acetonitrile was obtained from Sigma-Aldrich. Toluene, cyclohexane and methylcyclohexane were used as purchased from Sigma-Aldrich. New 10 mL and 20 mL kimble scintillation vials were used for the synthesis of various metal organic frameworks (MOFs).
3
Synthesis and Functionalization of Metal-Organic Frameworks
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Iron (III) chloride hexahydrate (98%, Alfa Aesar, Schiltigheim, France), 1,3,5-benzenetricarboxylic acid (BTC, 95%, Sigma-Aldrich, Saint-Quentin-Fallavier, France) and absolute ethanol (99%, Carlo Erba, Val-de-Reuil, France) were used for MOF synthesis. PBS (11.9 mM, pH 7.4 ± 0.1) was purchased from Life Technology Co., Ltd. (Saint Aubin, France). It contains 11.9 mM phosphates, 137 mM NaCl and 2.7 mM KCl. Gem-MP (CH12F2N3OP) was purchased from Toronto Research Chemicals, Canada. Phosphated β-cyclodextrin sodium salt (CD-P, Cyclolab, CY-2017.1, molecular formula: C42H70O47P4Na4) was used for coating. Milli-Q water was obtained from a Millipore apparatus equipped with a 0.22 μm filter. Reagents and solvents were used without further purification.
4
Doxorubicin-Loaded Nanoscale Metal-Organic Frameworks
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Doxorubicin (DOX, 98%), citric acid (≥99.5%), sodium phosphate monobasic dihydrate (≥99%, NaH2PO4·2H2O), hydrochloric acid (HCl, 34–37%), sodium hydroxide (NaOH, ≥97%) potassium chloride (powder, ≥99%) and deferoxamine mesylate salt (≥92.5%) were purchased from Sigma-Aldrich (Saint-Quentin-Fallavier, France). γ-CD was purchased from Cyclolab (Budapest, Hungary). Dimethylsulfoxide (DMSO, ACS) was from Panreac Applichem (Barcelona, Spain). Deuterated DMSO (DMSO-d6, 99.8% D) and water (D2O, 99.9% D) were obtained from Eurisotop (Gif sur Yvette, France). 1,5-13C2 citric acid was obtained from CortecNet (Les Ulis, France). 1,3,5-benzenetricarboxylic acid (BTC, 95%, Sigma-Aldrich, Saint-Quentin-Fallavier, France), aluminum nitrate nonahydrate (98%, Sigma-Aldrich, Saint-Quentin-Fallavier, France) and trimethyl trimesate (98%, Sigma-Aldrich, Saint-Quentin-Fallavier, France) and absolute ethanol (99%, Carlo Erba, Val-de-Reuil, France) were used for the synthesis of nanoMOFs. Water was purified by a Millipore MilliQ system.
Phosphate buffer saline (PBS, pH 7.4, containing 9.5 mM phosphates) was purchased from Life Technologies (Saint-Aubin, France) and was used for DOX release study.
Phosphate buffer saline (PBS, pH 7.4, containing 9.5 mM phosphates) was purchased from Life Technologies (Saint-Aubin, France) and was used for DOX release study.
5
Synthesis of Metal-Organic Frameworks
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EXAMPLE 1
Chemicals and Materials
All reagents were used as purchased without further purification. 1,3,5-benzene tricarboxylic acid (BTC), Cu(NO3)2.3H2O, Co(NO3)2.6H2O, Ni(NO3)2.6H2O, Zn(NO3)2.6H2O, FeCl2.6H2O, N,N-dimethylformamide (DMF) and ethanol were obtained from Sigma-Aldrich. Acetonitrile was obtained from Sigma-Aldrich. Toluene, cyclohexane and methylcyclohexane were used as purchased from Sigma-Aldrich. New 10 mL and 20 mL kimble scintillation vials were used for the synthesis of various metal organic frameworks (MOFs).
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