1H NMR (Bruker ARX 400) and LC-MS (Shimadzu, 2020) methods were used to characterize the synthesized compounds. HPLC was conducted with a LUMTECH HPLC (Germany) system using a C18 RP column with MeOH (0.05% TFA) and water (0.05% TFA) as eluents. TEM images were obtained using a HT7700 Exalens system (Hitachi, Japan). Rheology studies were performed with an AR 1500ex (TA instrument) system using a parallel plate (25 mm) with a gap of 500 μm.
Ht7700 exalens system
Manufactured by Hitachi
Sourced in Japan
The HT7700 Exalens system is a laboratory equipment product offered by Hitachi. It serves as a high-performance electron microscope, designed for advanced imaging and analysis applications. The core function of the HT7700 Exalens system is to provide users with detailed, high-resolution visualization and examination of samples at the nanoscale level.
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2 protocols using ht7700 exalens system
1
Analytical Characterization of Synthetic Compounds
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1H NMR (Bruker ARX 400) and LC-MS (Shimadzu, 2020) methods were used to characterize the synthesized compounds. HPLC was conducted with a LUMTECH HPLC (Germany) system using a C18 RP column with MeOH (0.05% TFA) and water (0.05% TFA) as eluents. TEM images were obtained using a HT7700 Exalens system (Hitachi, Japan). Rheology studies were performed with an AR 1500ex (TA instrument) system using a parallel plate (25 mm) with a gap of 500 μm.
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1H NMR (Bruker ARX 400) and LC-MS (Shimadzu, 2020) methods were used to characterize the synthesized compounds. HPLC was conducted with a LUMTECH HPLC (Germany) system using a C18 RP column with MeOH (0.05% TFA) and water (0.05% TFA) as eluents. TEM images were obtained using a HT7700 Exalens system (Hitachi, Japan). Rheology studies were performed with an AR 1500ex (TA instrument) system using a parallel plate (25 mm) with a gap of 500 μm.
2
Comprehensive Characterization of Synthesized Compounds
Check if the same lab product or an alternative is used in the 5 most similar protocols
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1H NMR (Bruker ARX 400) was used to characterize the synthesized compounds. HPLC was conducted with the LUMTECH HPLC (Germany) system using a C18 RP column with MeOH (0.05% of TFA) and water (0.05% of TFA) as the eluents. TEM images were done on a HT7700 Exalens system (Hitachi, Japan). Circular dichroism spectrum was done using a circular dichrometer (MOS-450, BioLogic). Rheology was performed on an AR 1500ex (TA instrument) system using a parallel plate (25 mm) at the gap of 500 μm. Optical density values were obtained by a microreader (Synergy 4, BioTek).
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