Anhydrousnmp

Manufactured by Merck Group

AnhydrousNMP is a laboratory solvent used in various chemical processes. It is a colorless, odorless liquid with a high boiling point. The product is designed to meet the needs of researchers and chemists who require a reliable and consistent solvent for their experiments.

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Lab products found in correlation

2 protocols using anhydrousnmp

Bisphenol A Functionalization Protocols

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All reagents were used
without further purification unless otherwise mentioned. Bisphenol
A (99+%), boron trifluoride etherate, methyl iodide, anhydrous tetrahydrofuran
(THF), tert-butyl nitrite, sodium chloride, copper(I)
chloride, potassium carbonate (K₂CO₃, 99+%),
benzyl chloride, TMHD, sodium iodide, cesium carbonate, and anhydrous
NMP 99% were purchased from Sigma-Aldrich Chemical Co. and used as
received. Hexane, anhydrous diethyl ether, anhydrous sodium thiosulfate,
methylene chloride stabilized, sodium hydroxide (97%), toluene, methanol,
ethyl acetate, and 37% hydrochloric acid were purchased from Fisher
Chemicals and used without further modification. Acetonitrile was
purchased from Spectrum and used without further modification. Sodium
sulfate was purchased from Alfa Aesar and used without further modification.
All solvents were dried and purified by using the standard procedures.

Alomar M.S, & Boyles D.A. (2019). Synthesis of a Regioregular Series of Poly(aryl ether carbonates) and Their Glass Transition Temperatures. ACS Omega, 4(27), 22363-22372.

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Synthesis of Tin and Cobalt Nanoparticles

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To prepare Sn NPs, a solution of NaBH 4 (96 mmol, 98%, ACBR) in anhydrous 1-methyl-2-pyrrolidone (NMP, 85 mL, 99.5%, Fisher BioReagents) was heated to 60 °C under flowing N 2 . Then, a solution of SnCl 2 (1 mmol, ≥99%, Alfa Aesar) in anhydrous NMP (3 mL) was injected and the reaction mixture was immediately cooled to room temperature using a water-ice bath. To prepare Co NPs, a NaBH 4 solution in anhydrous NMP (32 mmol in 15 mL) was heated to 150 °C under flowing N 2 , followed by the injection of CoCl 2 (8 mmol, ≥98%, Sigma-Aldrich) and immediate cooling to room temperature using a water-ice bath. The obtained Co NPs and Sn NPs were purified by washing once with dimethyl sulfoxide and then two times with water after separation from the supernatant by centrifugation. Finally, the reaction product was dried under vacuum at room temperature.

Walter M., Doswald S., Krumeich F., He M., Widmer R., Stadie N.P, & Kovalenko M.V. (2018). Oxidized Co-Sn nanoparticles as long-lasting anode materials for lithium-ion batteries. Nanoscale, 10(8).

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