First, stoichiometric mixtures of LiCl (99.9%; Sigma-Aldrich), NH4Cl (>99.5%; Sigma-Aldrich), and YCl3·6H2O (99.99%; Sigma-Aldrich) were weighed and dissolved into water. After complete dissolution, the mixture solution was transferred to a glass oven (Büchi glass oven, B-585) for drying at 80°C under vacuum. After drying, the white powder was transferred to a glove box and pressed into pellets for annealing at various temperatures (350° to 550°C) for 5 hours, respectively. The heating rate was 2°C min−1. Similar procedures were followed to synthesize Li3YBr6, Li3ScCl6, and Li3ErCl6 but changing the YCl3·6H2O to YBr3 (99.9%; Sigma-Aldrich), ScCl3 (99.99%; Sigma-Aldrich), and ErCl3 (99.99%; Sigma-Aldrich), respectively.
Sccl3
Manufactured by Merck Group
ScCl3 is a chemical compound consisting of scandium and chlorine. It is a crystalline solid that is used as a precursor in the synthesis of other scandium compounds. The core function of ScCl3 is to serve as a source of scandium for various industrial and scientific applications.
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Lab products found in correlation
2 protocols using sccl3
1
Synthesis of Lithium-based Solid Electrolytes
2
Synthesis of Halide-Based Solid Electrolytes
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The halide SEs were prepared by ball milling and subsequent solid-state reaction. Raw materials of LiCl (99.9%), InCl3 (99.99%), ScCl3 (99.99%,), YCl3 (99.99%), YbCl3 (99.99%), LuCl3 (99.99%) and ZrCl4 (99.9%) were used as starting materials from Sigma-Aldrich. The stoichiometric starting materials were weighed and ball milled at 350 rpm for 12 h sealed in a ZrO2 jar using 18 ZrO2 balls in an Ar-filled glovebox with p(H2O)/p < 0.1 ppm, p(O2)/p < 0.1 ppm. During ball milling, the jar was opened to make the samples homogenous at each 5 h in a glovebox. Then, the resulting mixture was sealed in quartz tubes and annealed at 260 °C for 12 h with a heating rate of 2 °C min−1 and cooled naturally to room temperature. After that, the obtained material was directly stored in an Ar-filled glovebox to prevent any moisture exposition.
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