Profile mass spectrometer

Manufactured by Shimadzu

The Profile mass spectrometer is a versatile analytical instrument designed for the identification and quantification of chemical compounds. It utilizes high-resolution mass spectrometry to precisely measure the mass-to-charge ratio of ionized molecules, enabling the determination of their elemental composition and molecular structure.

Automatically generated - may contain errors

Lab products found in correlation

Inova 300 spectrometer, by Agilent Technologies (3 mentions) Alpha p diamond atr spectrometer, by Bruker (3 mentions) Lambda 5 spectrometer, by PerkinElmer (2 mentions) 535 apparatus, by Büchi (1 mentions)

Close spelling variants of this product

Spectrometers

4 protocols using profile mass spectrometer

Synthesis and Characterization of Air-Sensitive Organometallic Compounds

Check if the same lab product or an alternative is used in the 5 most similar protocols

All experiments were performed
under a nitrogen atmosphere using standard Schlenk or glovebox techniques.
Solvents were dried using a column solvent purification system.^{56 (link)} Commercial KO^tBu (97%), MeLi (1.6
M in Et₂O), MeI, MeOH, Et₃N, 2-adamantanone,
benzophenone, acetone (99%), 9-fluorenone, and 1,2-diphenylcyclopropenone
were used as purchased. ¹H (299.95 MHz), ¹³C
(75.43 MHz), and ²⁹Si (59.59 MHz) NMR spectra were recorded
on a Varian INOVA 300 spectrometer either in C₆D₆ solution using the internal ²H-lock signal of the solvent
or in toluene solution with a D₂O capillary as an external
lock. Chemical shift values are referenced versus TMS. Compounds 1 and 2b were synthesized according to published
procedures.^{28 (link)} HRMS spectra were run on
a Kratos Profile mass spectrometer equipped with a solid probe inlet.
Infrared spectra were obtained on a Bruker Alpha-P Diamond ATR spectrometer
from the solid samples. Melting points were determined in capillaries
melted off on one side using a Büchi 535 apparatus and are
uncorrected. Elemental analyses were carried out on a Hanau Vario
Elementar EL apparatus. UV absorption spectra were recorded on a PerkinElmer
Lambda 5 spectrometer.

Kyri A.W., Schuh L., Knoechl A., Schalli M., Torvisco A., Fischer R.C., Haas M, & Stueger H. (2020). Sila-Peterson Reaction of Cyclic Silanides. Organometallics, 39(10), 1832-1841.

+ Open protocol

+ Expand

Synthesis of Cyclopentasilane and Imidazolium Compounds

Check if the same lab product or an alternative is used in the 5 most similar protocols

All experiments were performed under a dinitrogen atmosphere using standard Schlenk techniques. Solvents were dried using a column solvent purification system.^[27] Commercial reagents were used as purchased unless otherwise noted. ¹H (299.95 MHz), ¹³C (75.43 MHz) and ²⁹Si (59.59 MHz) NMR spectra were either recorded on a Varian INOVA MHz 300 or a Varian Mercury MHz 300 spectrometer in C₆D₆ or THF‐d₈ solutions and referenced to TMS using the internal ²H lock signal of the solvent. 1‐chloro‐3,3,4,4‐tetramethyl‐2,2,5,5‐tetrakis (trimethylsilyl)cyclopenta‐silane^[13] and 1,3,4,5‐tetramethylimidazol‐2‐ylidene (IMe₄)^[28] were synthesized according to published procedures. HRMS spectra were recorded on a Kratos Profile mass spectrometer. Infrared spectra were obtained on a Bruker Alpha‐P Diamond ATR Spectrometer from the solid sample. Melting points were determined using a Buechi 535 apparatus and are reported uncorrected. Elemental analyses were carried out on a Hanau Vario Elementar EL apparatus. Irradiations were carried out using a Kessil PR160L blue (λ=456 nm, 50 W) light LED lamp, with the reaction vessel placed approximately 2 cm from the light source, whilst being cooled by an external fan.

Lainer T., Dange D., Pillinger M., Fischer R.C., Kelterer A., Jones C, & Haas M. (2022). An NHC‐Mediated Metal‐Free Approach towards an NHC‐Coordinated Endocyclic Disilene. ChemistryOpen, 11(3), e202100240.

+ Open protocol

+ Expand

Synthesis and Characterization of Organogermane Compounds

Check if the same lab product or an alternative is used in the 5 most similar protocols

All experiments
were performed under a nitrogen atmosphere using
standard Schlenk techniques. Solvents were dried using a column solvent
purification system.^{75 (link)} Me₃SiCl
(95%), GeCl₄ (>98%), KOtBu (>98%),
ClCOMes
(99%), ClCO(oTol) (98%), C₆H₄-1-4–(COCl)₂ (>99%), C₆H₄-1-3–(COCl)₂ (>99%), Br(CH₂)₄Br (99%), MeI (>99%) and [18]-crown-6 (99%), toluene (≥99%),
toluene-d₈ (99 atom % D), THF-d₈ (99.5 atom % D), CDCl₃ (99.8 atom % D), butyl acrylate
(≥99%), styrene (≥99%), and methyl methacrylate (99%)
were used without any further purification. Tetrakis(trimethylsilyl)germane,^{76 (link)} tetraacylgermane 1 and FCOMes were
prepared according to published procedures.^{54 (link)}¹H, ¹³C, and ²⁹Si NMR spectra
were recorded on either a Varian INOVA 300 spectrometer in C₆D₆, THF-d₈, or CDCl₃ solutions and referenced versus TMS using the internal ²H-lock signal of the solvent. HRMS spectra were run on a Kratos Profile
mass spectrometer. Infrared spectra were obtained on a Bruker Alpha-P
Diamond ATR Spectrometer from the solid sample. Melting points were
determined using a Stuart SMP50 apparatus and are uncorrected. Elemental
analyses were carried out on a Hanau Vario Elementar EL apparatus.
UV absorption spectra were recorded on a PerkinElmer Lambda 5 spectrometer.

Frühwirt P., Knoechl A., Pillinger M., Müller S.M., Wasdin P.T., Fischer R.C., Radebner J., Torvisco A., Moszner N., Kelterer A.M., Griesser T., Gescheidt G, & Haas M. (2020). The Chemistry of Acylgermanes: Triacylgermenolates Represent Valuable Building Blocks for the Synthesis of a Variety of Germanium-Based Photoinitiators. Inorganic Chemistry, 59(20), 15204-15217.

+ Open protocol

+ Expand

Schlenk Techniques for Organometallic Synthesis

Check if the same lab product or an alternative is used in the 5 most similar protocols

All experiments
were performed under a nitrogen atmosphere using
standard Schlenk techniques. Solvents were dried using a column solvent
purification system.^{33 (link)} ClSiMe₃ (95%), KOtBu (>98%), ClCOMes (99%), ClCOAd (98%)
and 18-cr-6 (99%), were used without any further purification. ¹H, ¹³C, and ²⁹Si NMR spectra were recorded
on a Varian INOVA 300 spectrometer in C₆D₆,
THF-d₈, or CDCl₃ solutions
and were referenced versus TMS using the internal ²H-lock
signal of the solvent. HRMS spectra were obtained on a Kratos Profile
mass spectrometer. Infrared spectra were obtained on a Bruker Alpha-P
Diamond ATR spectrometer from the solid sample. Melting points were
determined using a Stuart SMP50 apparatus and are uncorrected. Elemental
analyses were carried out on a Hanau Vario Elementar EL apparatus.
UV absorption spectra were recorded on a PerkinElmer Lambda 5 spectrometer.

Wiesner T., Leypold M., Steinmaurer A., Schnalzer D., Fischer R.C., Torvisco A, & Haas M. (2020). Synthesis of Stable Dianionic Cyclic Silenolates and Germenolates. Organometallics, 39(15), 2878-2887.

+ Open protocol

+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Revolutionizing how scientists
search and build protocols!