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2 protocols using vinyl decanoate

1

Enzymatic Synthesis of Glycolipids

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Glucose, (-)-menthol and all solvents (HPLC grade) were acquired from Carl-Roth (Karlsruhe, Germany). Lipase B from Candida antarctica, immobilized on acrylic resin (iCalB), was purchased from Strem Chemicals (Strem chemicals Europe, Germany). Vinyl decanoate and decanoic acid were acquired from Tokyo Chemical Industry Co., Ltd. (TCI Europe, Belgium). 6-Decanoyl-d-glucose was purchased from Sohena (Tübingen, Germany).
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2

Enzymatic Synthesis of Fatty Acid Esters

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Raffinose (99.0%), t-BuOH (anhydrous), pyridine (anhydrous), N, N-dimethylformamide (DMF), benzene, Span 20, Span 40, Span 60, Span 80, Tween 20 and Tween 80 were purchased from the Energy Chemical Co., Ltd (Shanghai, China). Vinyl hexanoate (>99.0%), vinyl n-octanoate (>99.0%), vinyl decanoate (>99.0%), vinyl laurate (>99.0%), vinyl myristate (>99.0%), vinyl palmitate (>96.0%) and vinyl stearate (>95.0%) were purchased from the Tokyo Chemical Industry Co. Ltd. (Tokyo, Japan). Novo Nordisk (Bagsvaerd, Denmark) provided lipozyme TLIM while the Mitsubishi-Chemical Foods Corporation was the source of the sucrose esters P-1570 and P-1670. Pure olive oil, on the other hand, was purchased from a local food store.
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