Soybean oil was purchased from the local market in Silchar, Assam, India and its physical properties and compositions are listed in Table 1 of the ESI.† Waste snail shells (Pila spp.) were procured from Mizoram, India. Methanol of analytical reagent (AR) grade was acquired from Merck, India. Double distilled water was used throughout the experiments. Bromothymol blue (pKa = 7.2), phenolphthalein (pKa = 9.8), indigo carmine (pKa = 12.2), 2,4-dinitroaniline (pKa = 15.0) and 4-nitroaniline (pKa = 18.4) were purchased from Sigma Aldrich.
2 4 dinitro aniline
Manufactured by Merck Group
2,4-dinitro aniline is a synthetic organic compound that is commonly used as a chemical intermediate in the production of various pharmaceutical and agrochemical products. It serves as a precursor for the synthesis of other compounds and is a versatile laboratory reagent. The core function of 2,4-dinitro aniline is to facilitate chemical reactions and transformations in a controlled laboratory setting.
Automatically generated - may contain errors
Lab products found in correlation
4 nitroaniline, by Merck Group (2 mentions)
Phenolphthalein, by Merck Group (1 mentions)
Bromothymol blue, by Merck Group (1 mentions)
Indigo carmine, by Merck Group (1 mentions)
Dichloromethane, by Merck Group (1 mentions)
Sodium azide, by Merck Group (1 mentions)
3 trifluoromethyl aniline, by Merck Group (1 mentions)
3 nitroaniline, by Merck Group (1 mentions)
Nmr spectrometer, by Bruker (1 mentions)
Silica gel 60 f254, by Merck Group (1 mentions)
1 bromohexane, by Merck Group (1 mentions)
1 3 dicyclohexylcarbodiimide, by Merck Group (1 mentions)
1000 spectrometer, by PerkinElmer (1 mentions)
2 fluoroaniline, by Merck Group (1 mentions)
4 fluoroaniline, by Merck Group (1 mentions)
4 n n dimethylaminopyridine, by Merck Group (1 mentions)
Ethyl 4 aminobenzoate, by Merck Group (1 mentions)
2 nitroaniline, by Merck Group (1 mentions)
3 protocols using 2 4 dinitro aniline
1
Soybean Oil and Waste Snail Shell Characterization
2
Synthesis of Substituted Anilines
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
4-Nitroaniline (Sigma Aldrich), 3-Nitroaniline(Alfa Aesar), 3-(trifluoromethyl) aniline, 4-Nitro-2-(trifluoromethyl) aniline(Alfa Aesar), 3,5-dinitro aniline (Sigma Aldrich), 2,4-dinitro aniline (Sigma Aldrich), Sodium Azide (Sigma Aldrich), Copper Sulphate and Sodium ascorbate were used as received. Dichloromethane (Merck) was distilled. Triethyl amine was also distilled. Acryloyl chloride(Alfa Aesar) were used under inert conditions. AIBN (Sigma Aldrich) as obtained. All the solvents were purified by distillation prior to their use.
3
Synthesis and Characterization of Substituted Anilines
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The analytical grades of ethyl 4-aminobenzoate, sodium nitrite (NaNO2), phenol, 1-bromohexane, 1,3-dicyclohexylcarbodiimide (DCC), 4-(N,N-dimethyl amino)pyridine (DMAP), 4-fluoro aniline, 2-fluoro aniline, 2-nitro aniline, 2-trifluoromethyl aniline, 2,4-dinitro aniline, potassium carbonate (K2CO3), sodium hydroxide (NaOH), potassium hydroxide (KOH), potassium iodide (KI) were procured from Sigma Aldrich and Spectrochem. For column chromatography silica gel 60-120 and neutral alumina were procured from Thomas baker. Acetone, hexane, ethyl acetate and dichloromethane were dried over phosphorus pentaoxide and calcium hydride, respectively. These solvents were distilled using standard methods when required for the experiment. Thin-layer chromatography (TLC) were performed on aluminium sheet precoated with silica gel-60 F254 (Merck). Infrared (IR) spectra were recorded using a PerkinElmer 1000 spectrometer. Proton nuclear magnetic resonance (1H NMR) spectra were recorded on a 400 MHz Bruker NMR spectrometer, using CDCl3 as a solvent and tetramethyl silane (TMS) as an internal standard.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!