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Spectrum gx ftir spectrometer

Manufactured by PerkinElmer
Sourced in United States

The Spectrum GX FTIR spectrometer is a high-performance analytical instrument designed for materials characterization and identification. It utilizes Fourier Transform Infrared (FTIR) spectroscopy technology to analyze the infrared absorption spectrum of a sample, providing information about its molecular composition and structure.

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24 protocols using spectrum gx ftir spectrometer

1

Characterization of Peptide-Imprinted Nanoparticles

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Wide-angle X-ray diffractograms (WAXD) were obtained with a Bruker D8 ADVANCE diffractometer, using Cu Ka radiation with a step size of 0.05° and a scanning speed of 4°/min. Transmission electron microscopy (TEM) images were obtained using a JEOL JEM1230 transmission electron microscope. Photoluminescence (PL) spectra were recorded on a Hitachi F-7000 fluorescence spectrophotometer (Japan). Scanning electron microscopy (SEM) images were obtained using a Hitachi S4800 scanning electron microscope. Fourier-transform infrared spectroscopy (FTIR) spectra were recorded using a Spectrum GX FTIR spectrometer (PerkinElmer, Inc. Waltham, MA, USA). The transmission spectra of the KBr sample pellets were collected at a resolution of 4 cm−1, acquiring a total of 16 scans in the wavenumber region of 400–4000 cm−1. Ultraviolet-visible (UV-vis) spectroscopic analysis (SP-8001, Shishin Technology Co., Ltd., Taipei, Taiwan) was performed to evaluate the binding of the PD-L1 peptide to the imprinted or non-imprinted particles. One milligram of composite nanoparticles was added into 10 mL of peptide E solution (20 μg/mL) and allowed to bind for 10 to 60 min. After magnetically removing the particles, the peptide E concentration was assayed using the absorption at 295 nm.
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2

FTIR Analysis of Nanofibre Scaffolds

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To characterize the chemical composition of the nanofibre scaffolds, FTIR was performed using Spectrum GX FTIR spectrometer (Perkin Elmer, Waltham, MA, USA). The samples were scanned in the range of 4000–500 cm−1. In total, three samples from each scaffold were assessed.
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3

FTIR Analysis of Polymer Blends

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A Perkin Elmer Spectrum GX FTIR spectrometer (Waltham, MA, USA) operating in attenuated total reflection mode, in a wave number range of 4000 to 650 cm−1. Thirty-two (32) cycles of scanning, and a resolution of 2 cm−1 was used to record the Fourier transform infrared (FTIR) spectra of pure MVR, PVAc, PHEMA homopolymers, and VAC-HEMA copolymer. The samples were analyzed in the form of thin transparent films except that of MVR which was analyzed as powder diluted in dehydrated KBr.
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4

FTIR Spectroscopic Analysis of Film Dressing

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The film dressing (1 cm × 1 cm) was prepared. The Fourier Transform Infrared Spectroscopy (FTIR) spectra were recorded using a Spectrum GX FTIR spectrometer (PerkinElmer, United States of America) in the 650–4,000 cm−1 range.
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5

FTIR Analysis of Extracted Polymer

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The extracted polymer was mixed with KBr spectra was noted in 4000 – 400 cm–1 range with PerkinElmer spectrum GX FTIR spectrometer in by mixing the extracted polymer with.
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6

Characterization of Nanocrystals via Multimodal Techniques

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Wide-angle X-ray diffractograms (WAXD) were obtained with a Bruker D8 ADVANCE diffractometer, using Cu Ka radiation with a step size of 0.05° and a scanning speed of 4° min−1. Transmission electron microscopy (TEM) images were obtained using a JEOL JEM1230 transmission electron microscope. Dynamic light scattering (DLS) measurements were achieved by a Brookhaven Instruments 90PLUS instrument. Fourier-transform infrared spectroscopy (FTIR) spectra were recorded using a Spectrum GX FTIR spectrometer (PerkinElmer, Inc.). The transmission spectra of the KBr sample pellets were collected with a resolution of 4 cm−1, acquiring a total of 16 scans in a wavenumber region of 400–4000 cm−1. Ultraviolet-visible (UV-vis) spectroscopic analysis was performed using a PerkinElmer Lambda 35 UV-vis spectrophotometer. Photoluminescence (PL) spectra were recorded on a Hitachi F-7000 fluorescence spectrophotometer (Japan). The emission spectra of the nanocrystals were obtained upon 980 nm NIR excitation using a SDL980-LM-5000T laser diode (980 nm, 3 W cm−2) obtained from Shanghai Dream Lasers Technology Co., Ltd. (China).
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7

FTIR Analysis of Polymer Blends

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A Perkin Elmer Spectrum GX FTIR spectrometer (Waltham, MA, USA) operating in attenuated total reflection mode, in a wave number range of 4000 to 650 cm−1. Thirty-two (32) cycles of scanning, and a resolution of 2 cm−1 was used to record the Fourier transform infrared (FTIR) spectra of pure MVR, PVAc, PHEMA homopolymers, and VAC-HEMA copolymer. The samples were analyzed in the form of thin transparent films except that of MVR which was analyzed as powder diluted in dehydrated KBr.
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8

Characterization of Biomass Feedstocks

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Woodchips, grains of feed barley (Hordeum vulgare L.), and peanut (Arachis hypogaea) shells were studied as potential carbon sources. Woodchips were obtained from untreated pine (Pinus sylvestris). According to screen analysis, 85.5% of the woodchips were retained over a 2 mm mesh sieve, while 10.4% passed through a 2 mm mesh sieve but were retained over a 1 mm mesh sieve. The remaining fraction (4.1%) passed through a 1 mm mesh sieve but was retained over a 0.6 mm mesh sieve. Barley grains (0.6 ± 0.05 cm) and peanut shells (3.2 ± 0.47 cm) were obtained, respectively, from Apan and Temascalapa, both in the State of Hidalgo, Mexico. All foreign matter (such as stones, dust, or stalks) and damaged kernels were removed from barley by hand.
Elemental composition and Fourier Transform Infrared (FT-IR) analyses were made on 1.5–3.0 mg samples of the natural materials previously ground to a homogeneous fine powder and dried at 105°C for 24 h using a 2400 Series II CHNS Elemental Analyzer and a Spectrum GX FT-IR spectrometer (both from Perkin-Elmer, Waltham, MA, USA), respectively. The IR spectra were obtained from KBr pellets (1 : 100 weight ratio of sample/KBr). The spectrometer was set to scan from 4000 to 400 cm−1.
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9

X-Ray Diffraction and FT-IR Analysis

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X-ray diffraction patterns were obtained using an Ultima IV multipurpose XRD system (Rigaku, The Woodland, TX, USA) at 40 kV and 40 mA, with a scanning speed of 0.1°/min. Functionalized surfaces were investigated using the ATR method of FT-IR; specifically, the Spectrum GX FT-IR Spectrometer (PerkinElmer Inc., Waltham, MA, USA) was used.
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10

Characterization of Luminescent Metal Complexes

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All reagents and solvents were used as received from commercial suppliers without further purification. Infrared spectra were recorded on a PerkinElmer Spectrum GX FT-IR spectrometer in ATR mode in the range 4000–400 cm−1. The following abbreviations were used to describe the peak characteristics: br = broad, sh = shoulder, s = strong, m = medium and w = weak. NMR spectra of the compounds were measured using a Bruker Ultrashield plus 500 (500 MHz) and Varian 500 MHz spectrometer. 1H- and 13C-measurements were recorded using deuterated solvents and referenced to tetramethylsilane (TMS) as an internal standard (δ = 0 ppm). The single crystal X-ray diffraction (SCXRD) data were collected on a STADIVARI diffractometer using Ga-Kα, λ = 1.34143 Å radiation with area detection using a Dectris Eiger2 R 4M detector. Powder X-ray diffraction (PXRD) measurements were performed on a STOE STADI-P diffractometer with Cu-Kα radiation. The optical properties were investigated using Fluoromax-4 spectrofluorometer and Shimadzu UV-24500 in the range 200–800 nm at room temperature using 1 cm path length cells. The stock solution of H6L (100 μM) and the corresponding metal ions solutions (1000 μM) were prepared in DMSO.
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