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Lead chloride

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Lead chloride is an inorganic compound with the chemical formula PbCl2. It is a white, crystalline solid that is used as a laboratory reagent.

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Lab products found in correlation

Methylammonium iodide, by Xi'an Yuri Solar Co. (3 mentions) Ultra pure ce water, by Agilent Technologies (2 mentions) 18 crown 6 ether, by Merck Group (2 mentions) Glacial acetic acid, by Thermo Fisher Scientific (2 mentions) Imidazole, by Merck Group (2 mentions) Malonic acid, by Merck Group (2 mentions) Lead iodide, by Thermo Fisher Scientific (1 mentions) Dimethyl sulfoxide (dmso), by Merck Group (1 mentions) N n dimethylformamide (dmf), by Merck Group (1 mentions) Diethyl ether, by Merck Group (1 mentions) 1 butanol, by Merck Group (1 mentions) Polymethyl methacrylate, by Maclin Biochemical Technology (1 mentions) Isopropanol ipa, by Merck Group (1 mentions) Toluene, by Merck Group (1 mentions) Chlorobenzene, by Merck Group (1 mentions) Methylammonium iodide, by Greatcell Solar (1 mentions) Rubidium bromide, by Merck Group (1 mentions) Lead bromide, by Thermo Fisher Scientific (1 mentions) Polyvinyl pyridine, by Merck Group (1 mentions) Formamidinium bromide, by Greatcell Solar (1 mentions)

Spelling variants of this product

Lead (II) chloride (3 citations) Lead (II) chloride (PbCl2), (2 citations)

7 protocols using lead chloride

1

Perovskite Solar Cell Fabrication

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Methylammonium iodide (MAI, ≥99.5%) was purchased from Xi’an Polymer Light Technology Corp., Xi’an, China. Lead iodide (PbI2, 99.9985%) and lead chloride (PbCl2, 98%) were purchased from Alfa-Aesar, Ward Hill, MA, USA. Titanium (IV) diisopropoxide bis (acetylacetonate) (75 wt.%) and 1-butanol (99.8%) for the TiO2 blocking layer were purchased from Sigma-Aldrich, St. Louis, MO, USA. N, N-Dimethylformamide (DMF, 99.8% anhydrous), dimethyl sulfoxide (DMSO, ≥99.9% anhydrous), and diethyl ether (DEE, ≥99.7 anhydrous) were purchased from Sigma-Aldrich, St. Louis, MO, USA.
Vidyasagar D., Yun Y.H., Shin S., Jung J., Park W., Lee J.W., Han G.S., Ko C, & Lee S. (2021). In-Situ Nano-Auger Probe of Chloride-Ions during CH3NH3PbI3−xClx Perovskite Formation. Materials, 14(5), 1102.
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2

Perovskite Solar Cell Fabrication

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Methylammonium iodide (MAI) was purchased from Great Cell Solar. Lead acetate trihydrate (Pb(CH3COOH)2 ∙ 3H2O, >99.5%) was purchased from TCI. Lead chloride (PbCl2, >99.999%) was purchased from Alfa Aesar. Poly [bis (4-phenyl) (2,4,6-trimethylphenyl) amine] (PTAA) and Bathocuproine (BCP) were purchased from Xi’an p-OLED Corp. [6,6]-phenyl-C61-butyric acid methyl ester (PCBM) was purchased from Solarmer. Polymethyl methacrylate (PMMA) was purchased from Shanghai Macklin Biochemical. Toluene, dimethylformamide (DMF), isopropanol (IPA), ethanol, and chlorobenzene (CB) were purchased from Sigma Aldrich and used as received.
Qin W., Ali W., Wang J., Liu Y., Yan X., Zhang P., Feng Z., Tian H., Yin Y., Tian W, & Li C. (2023). Suppressing non-radiative recombination in metal halide perovskite solar cells by synergistic effect of ferroelasticity. Nature Communications, 14, 256.
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3

Perovskite Solar Cell Material Synthesis

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Caesium bromide (CsBr, 99.999%), lead bromide (PbBr2, 99.999%), lead chloride (PbCl2, 99.999%) was purchased from Alfa Aesar. Formamidinium bromide (FABr) and phenethylammonium bromide (PEABr) were purchased from Greatcell Solar. Rubidium bromide (RbBr, 99.99%), polyvinylpyridine (PVP, average Mw ~55,000), 4,7,10-trioxa-1,13-tridecanediamin (TTDDA), poly(9-vinylcarbazole) (PVK, average Mn 25,000–50,000) were purchased from Sigma Aldrich. The NiOx nano-crystals were purchased from Avantama AG and were used without additional treatment. 1,3,5-tris(1-phenyl-1H-benzimidazol-2-yl)benzene (TPBi) was purchased from Luminescence Technology corp. Other materials for device fabrication were all purchased from Sigma-Aldrich.
Karlsson M., Yi Z., Reichert S., Luo X., Lin W., Zhang Z., Bao C., Zhang R., Bai S., Zheng G., Teng P., Duan L., Lu Y., Zheng K., Pullerits T., Deibel C., Xu W., Friend R, & Gao F. (2021). Mixed halide perovskites for spectrally stable and high-efficiency blue light-emitting diodes. Nature Communications, 12, 361.
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4

Synthesis of Mixed Halide Perovskite Precursor

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ITO substrates were all purchased from Shenzhen Nanbo Ltd. Titanium isopropoxide (97%), methylamine (CH 3 NH 2 ) and hydrogen iodide (HI) were purchased from Sigma Aldrich. 2-isopropanol (HPLC, 99.9%), ethanol (HPLC, 99%), lead chloride (PbCl 2 , 99.99%), N, N-Dimethylformamide (DMF, 99.9%) were purchased from Alfa Aesar. All the materials were used as received without further purification.
Methylammonium iodide (CH 3 NH 3 I) was synthesized by following reported method 47 and purified with ethanol twice. CH 3 NH 3 I crystals was dried at 45 ℃ in vacuum for 48 h before usage. The precursor solution of mixed halide perovskite with a concentration of 40 wt % and 50 wt % are prepared by mixing CH 3 NH 3 I with PbCl 2 powder with a molar ration of 1:3 in DMF. The mixture solution was stirred at 70 ℃ over 8 h and filtered with a 0.45 μm filter before film preparation.
Yuan Z., Yang Y., Wu Z., Bai S., Xu W., Song T., Gao X., Gao F, & Sun B. (2016). Approximately 800-nm-Thick Pinhole-Free Perovskite Films via Facile Solvent Retarding Process for Efficient Planar Solar Cells. ACS applied materials & interfaces, 8(50).
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5

Synthesis and Characterization of Lead-Based Compounds

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Lead chloride and glacial acetic acid were purchased from Fisher Scientific (Fairlawn, NJ, USA), imidazole and malonic acid were obtained from Aldrich (Milwaukee, WI, USA), 18-crown-6 ether was acquired from Sigma-Aldrich (St. Louis, MO, USA), and methanol was attained from Pharmco-Aaper (Brookfield, CT, USA). All reagents were of analytical grade. Ultra pure CE water obtained from Agilent Technologies (Santa Clara, CA, USA).
Varden L, & Bou-Abdallah F. (2017). Detection and Separation of Inorganic Cations in Natural, Potable, and Wastewater Samples Using Capillary Zone Electrophoresis with Indirect UV Detection. American journal of analytical chemistry, 8(1), 81-94.
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6

Synthesis and Characterization of Tungsten Oxide Nanoparticles

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Tungsten oxide (WO3, orthorhombic crystal) nanoparticles (spherical, 23–65 nm in diameter, and 99.95% purity) were purchased from US Research Nanomaterials (USA). Pyridine and toluene were purchased from Alfa Aesar (USA). (3-aminopropyl)triethoxysilane (APTES, 99%) was purchased from Sigma-Aldrich (USA). Cadmium chloride anhydrous, lead chloride, ethylenediaminetetraacetic acid (EDTA), and tris (hydroxymethyl)aminomethane were purchased from Fisher Scientific (USA). Diethyl ether and sodium dihydrogen phosphate were purchased from Acros Organics (Geel, Belgium). Standard Suwannee River natural organic matter (NOM) was obtained from the International Humic Substances Society (IHSS, USA). A NOM stock solution (100 mg/L) was prepared by mixing a known amount of NOM with DI water for 24 h. The pH of the stock solutions was adjusted to 8 with 0.1 M and 0.01 M NaOH and HCl. All chemicals were used as received, without further purification. All solutions were prepared with deionized water (18 MΩ-cm) from a Barnstead NANOpure Diamond water purification system (USA).
Huang Y, & Keller A.A. (2020). Remediation of heavy metal contamination of sediments and soils using ligand-coated dense nanoparticles. PLoS ONE, 15(9), e0239137.
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7

Synthesis and Characterization of Lead-Based Compounds

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Lead chloride and glacial acetic acid were purchased from Fisher Scientific (Fairlawn, NJ, USA), imidazole and malonic acid were obtained from Aldrich (Milwaukee, WI, USA), 18-crown-6 ether was acquired from Sigma-Aldrich (St. Louis, MO, USA), and methanol was attained from Pharmco-Aaper (Brookfield, CT, USA). All reagents were of analytical grade. Ultra pure CE water obtained from Agilent Technologies (Santa Clara, CA, USA).
Varden L, & Bou-Abdallah F. (2017). Detection and Separation of Inorganic Cations in Natural, Potable, and Wastewater Samples Using Capillary Zone Electrophoresis with Indirect UV Detection. American journal of analytical chemistry, 8(1), 81-94.
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