1-Vinylimidazole (1-VIm, purity of 99%), 2-bromoethanamine hydrobromide (98%), and 2,2-azobisisobutyronitrile (AIBN) were purchased from Alfa Aesar (MA, US). Prior to use, AIBN was recrystallized from methanol. Triethylamine (>99.5%), copper (II) nitrate hydrate (99%), and 1,3,5-benzenetricarboxylic acid (98%) were received from Aladdin (Shanghai, China). Deionized water with resistivity of 18.2 MΩ·cm−1 was generated from an Ulupure-H ultrapure water generator (Ulup, China). Unless otherwise specified, all the other solvents and reagents were used as received. The Cu3(BTC)2 was synthesized by following the literature [31 ].
1 vinylimidazole
Manufactured by Thermo Fisher Scientific
Sourced in United States
1-vinylimidazole is a chemical compound used as a laboratory reagent. It is a colorless liquid with a pungent odor. 1-vinylimidazole is used in various chemical synthesis and analysis applications, but its core function is not provided in order to maintain an unbiased and factual approach.
Automatically generated - may contain errors
Lab products found in correlation
1 bromobutane, by Thermo Fisher Scientific (2 mentions)
Bromoethane, by Thermo Fisher Scientific (2 mentions)
1 bromohexane, by Thermo Fisher Scientific (2 mentions)
Bis acrylamide, by Thermo Fisher Scientific (2 mentions)
Ammonium persulfate, by Thermo Fisher Scientific (2 mentions)
Acrylic acid, by Thermo Fisher Scientific (2 mentions)
Acrylate peg, by Thermo Fisher Scientific (2 mentions)
Acrylate peg nh2, by JenKem Technology (2 mentions)
4 imidazolecarboxylic acid, by Merck Group (2 mentions)
N 3 aminopropyl methacrylamide hydrochloride apma, by Merck Group (2 mentions)
N n bis acryloyl cystamine baca, by Merck Group (2 mentions)
Acrylate peg mal apeg mal, by Creative PEGWorks (2 mentions)
2 2 azo bis isobutyronitrile, by Thermo Fisher Scientific (1 mentions)
Bromoethane, by Merck Group (1 mentions)
Ammonium persulfate, by Carl Roth (1 mentions)
Poly ethylene glycol diacrylate pegda, by Merck Group (1 mentions)
2 methacryloyloxyethyl phosphorylcholine, by Merck Group (1 mentions)
2 methacryloyloxy ethyl dimethyl 3 sulfopropyl ammoniumhydroxide, by Merck Group (1 mentions)
2 hydroxyethyl methacrylate, by Thermo Fisher Scientific (1 mentions)
3 sulfopropylmethacrylate potassium, by Merck Group (1 mentions)
11 protocols using 1 vinylimidazole
1
Synthesis of Cu3(BTC)2 Metal-Organic Framework
2
Hydrogel Polymer Synthesis Protocols
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N,Nʼ-methylenebis(acrylamide) (MBAA, 99%; Sigma-Aldrich), poly(ethyleneglycol)diacrylate (PEGDA, Mn = 250, 575, 700; Sigma-Aldrich); ethyleneglycoldimethacrylate (≥97%; TCI), N,N,Nʼ,Nʼ-tetramethylethylendiamine (TMEDA, ≥99.5%; Sigma-Aldrich), ammoniumpersulfate (APS, 98%; Roth), 3-sulfopropylmethacrylate potassium (98%; Sigma-Aldrich), 3-sulfopropylacrylate potassium (Sigma-Aldrich), 2-acrylamido-2-methyl-1-propanesulfonicacid (99%; Sigma-Aldrich), (vinylbenzyl)trimethylammonium chloride (99%; ACROS Organics), [2-(acryloyloxy)ethyl]trimethylammonium chloride (80 wt.% in H2O; Aldrich), [2-(methacryloyloxy)ethyl]trimethylammonium chloride (75 wt.% in H2O; Aldrich), 2-hydroxyethylmethacrylate (97%; Alfa Aesar), [2-(methacryloyloxy)ethyl]dimethyl-(3-sulfopropyl)ammoniumhydroxide (95%; Sigma-Aldrich), 2-methacryloyloxyethylphosphorylcholine (97%; Sigma-Aldrich), 1-vinylimidazole (≥99%; Alfa Aesar), bromoethane(≥99%; Sigma-Aldrich), amino-2-propanol(93%; TCI), methacrylicanhydride (94%; Alfa Aesar) were all used as received without further treatment. 1-Vinyl-3-ethyl-imidazoliumbromide (VEtImBr) and 2-Hydroxypropyl methacrylamide (HPMAA) were prepared according to published procedures.[21 (link),22 (link)]
3
Synthesis and Characterization of Polymeric Electrolytes
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1-Bromobutane (Alfa Aesar, Tewksbury, MA, USA), 1,4-dibromobutane (Alfa Aesar, Tewksbury, MA, USA), 1-vinylimidazole (Alfa Aesar, Tewksbury, MA, USA), 1-methylimidazole (Alfa Aesar, Tewksbury, MA, USA), lithium bis(trifluoromethane sulfonamide) (LiTFSI, Acros, Geel, Belgium), photoinitiators: diphenyl (2,4,6-trimethylbenzoyl)-phosphine oxide (TPO, Aldrich, Milwaukee, WI, USA), 1-hydroxy-cyclohexyl-phenyl-ketone (Irgacure 184, Ciba, Tarrytown, NY, USA), 2-methyl-1-[4-(methylthio)phenyl]-2-(4-morpholinyl)-1-propanone (Irgacure 907, Ciba, Tarrytown, NY, USA), poly(vinylidene fluoride) (PVDF, Solf®PVDF 6020, Solvay, Bruxelles, Belgium), 1-methyl-2-pyrrolidone (NMP, Riedel-de Haën, Seelze, Germany), carbon nanoparticles (CNP, ~15 nm, UniRegion Bio-Tech, Taoyuan, Taiwan), and activated carbon (AC, ACS-2930, China steel chem. Co., Kaohsiung, Taiwan) were used as received.
4
Synthesis and Characterization of Imidazolium-based Ionic Liquids
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Rotiphorese Gel B (MBAA) (2% w/w N,N′-methylenebis(acrylamide), Carl Roth, Karlsruhe, Germany), N,N,N′,N′-tetramethylethylenediamine (TEMED) (≥99.5%; Sigma Aldrich, St. Louis, MO, USA), ammonium persulfate (APS) (98%; Acros Organics, Fair Lawn, NJ, USA), 1-vinylimidazole (≥99%; Alfa Aesar, Haverhill, MA, USA), bromoethane (98%; Alfa Aesar), 1-chlorobutane (≥99%; Acros Organics), 1 bromobutane (99%; Sigma Aldrich), ethanol (EtOH) (≥99.8%), n-heptane (n-Hep) (≥99.5%), and tetrahydrofuran (THF) (≥99.8%) were used in this study. Additionally, ultrapure water was used throughout the study.
5
Synthesis and Characterization of Imidazolium Compounds
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1-Vinylimidazole
(99%) was purchased from Alfa Aesar (Kandel, Germany)
and distilled under reduced pressure at 80 °C prior to use. Tributylphosphine
(97%), diallyldimethylammonium chloride (65% solution in water), 1-bromoethane,
1-chlorobutane, and 1-methylimidazole were purchased from Sigma-Aldrich
(Steinheim, Germany). 1-methylimidazole was distilled over KOH before
use. Sodium salicylate (99%) and lanthanum(III)-chloride heptahydrate
were purchased from ABCR (Kalrsruhe, Germany) and used as received.
Terbium (III,IV) oxide (99.99%) was purchased from SmartElements (Vienna,
Austria). Choline chloride (97%) and ethanol (99.5%) were purchased
from Acros Organics (Geel, Belgium).
(99%) was purchased from Alfa Aesar (Kandel, Germany)
and distilled under reduced pressure at 80 °C prior to use. Tributylphosphine
(97%), diallyldimethylammonium chloride (65% solution in water), 1-bromoethane,
1-chlorobutane, and 1-methylimidazole were purchased from Sigma-Aldrich
(Steinheim, Germany). 1-methylimidazole was distilled over KOH before
use. Sodium salicylate (99%) and lanthanum(III)-chloride heptahydrate
were purchased from ABCR (Kalrsruhe, Germany) and used as received.
Terbium (III,IV) oxide (99.99%) was purchased from SmartElements (Vienna,
Austria). Choline chloride (97%) and ethanol (99.5%) were purchased
from Acros Organics (Geel, Belgium).
6
Synthesis of Ferrocene Ionic Liquids
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1-Vinylimidazole (99%) and sodium tetrafluoroborate were obtained from Alfa Aesar. Potassium hexafluorophosphate was purchased from Acros Organics. 1,1′-Ferrocene dicarboxylic acid was bought from Energy Chemical. Bromoacetonitrile (95%) was purchased from TCI Europe. Lithium bis(trifluoromethane sulfonyl)imide (LiTFSI, 99.95%) was purchased from Io-li-tec. Lithium nitrate (LiNO3), polyvinylidene fluoride (PVDF), N-methyl-2-pyrrolidone (NMP), 1,2-dimethoxyethane (DME), and 1,3-dioxolane (DOL) were purchased from Sigma-Aldrich. Sulfur powder was purchased from Alfa Aesar. All chemicals were used without any further purification. Solvents were of analytical grade.
7
Synthesis of 1-Bromohexane and 1-Vinylimidazole Derivatives
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1-Bromohexane (99%) and 1-vinylimidazole (>99%) were purchased from Alfa Assar (Alfa Aesar GmbH & Co KG, Haverhill, MA, USA). Propylene carbonate (99.7%), lithium bis(trifluoromethylsulfonyl)imide (LiTFSI, 99%) and α,α’-azoisobutyronitrile (AIBN, 98%) were obtained from Sigma-Aldrich (Taufkirchen, Germany) and used as received. All other solvents, diethylether, acetonitrile, acetone and methanol, were HPLC grade and purchased from Sigma-Aldrich (Taufkirchen, Germany). Milli-Q+ water (high-resistance ultra-purified water, Tallinn, Estonia) was used as supplied.
8
Synthesis of Polymerized Acrylamide Compounds
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Acrylamide, polyAcrylamide (average MW 10,000) and trifluoroacetic acid were obtained from Acros Organics (Geel, Antwerp, Belgium). Potassium persulfate, sodium alginate and methacrylic anhydride were purchased from Sigma-Aldrich (St. Louis, MO, USA). N,N′-MethylenebisAcrylamide, 1-vinylimidazole, bromoethane, 1-bromobutane, 1-bromohexane and 1-bromooctane were gained from Alfa Aesar (Ward Hill, MA, USA). Calcium chloride and Boc-Lys-OH were obtained from Merck (Darmstadt, Germany) and Carbosynth (Compton, UK), respectively. Deionized water was used in all the experiments.
9
Synthesis of 1-Vinylimidazole Derivative
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1-Vinylimidazole and 2-bromoethylamine
hydrobromide (98%) were purchased from Alfa Aesar. Benzene (>99.5%)
and triethylamine (TEA) were obtained from Dae Jung, Corp (South Korea).
Hexanes (extra pure grade) and ethyl alcohol (95%, extra pure grade)
were purchased from Duksan, Corp (South Korea). Acetone (99.5%) was
obtained from Samchun, Corp (South Korea). All reagents and solvents
were used as received without further purification. The distilled
water used in all experiments was purified using a Milli-Q water purification
system. The resistivity of the water was higher than 18 MΩ·cm–1.
hydrobromide (98%) were purchased from Alfa Aesar. Benzene (>99.5%)
and triethylamine (TEA) were obtained from Dae Jung, Corp (South Korea).
Hexanes (extra pure grade) and ethyl alcohol (95%, extra pure grade)
were purchased from Duksan, Corp (South Korea). Acetone (99.5%) was
obtained from Samchun, Corp (South Korea). All reagents and solvents
were used as received without further purification. The distilled
water used in all experiments was purified using a Milli-Q water purification
system. The resistivity of the water was higher than 18 MΩ·cm–1.
10
Modular Polymer Functionalization Protocol
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