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4 protocols using sulfuric acid h2so4

1

Synthesis of Mesoporous Silica Nanoparticles

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Kaolinite (K7375) and fumed silica (S5130, 0.007 μm) were purchased from Sigma-Aldrich. Cetrimonium bromide (CTAB, 99%), potassium hydroxide (KOH, 85%), hydrochloric acid (HCl, 35–37%), sucrose (C12H22O11, EP) and sulfuric acid (H2SO4, 98%) were purchased from Daejung Chemicals. HF (49%) was purchased from J. T. Baker. Air gas and N2 gas were purchased from Daesung Industrial Gases Co. Ltd. All the chemicals were used without further purification.
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2

Synthesis and Characterization of PMPS-PEES Polymers

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(PMPS and poly (1,4-phenylene ether-ether-sulfone) (PEES) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Methanol, acetone, N, N-dimethylacetamide (DMAc), N, N-dimethylformamide (DMF), tetrahydrofuran (THF), N-methylpyrrolidone (NMP), dimethyl sulfoxide (DMSO) and sulfuric acid (H2SO4) were purchased from Daejung Reagents & Chemicals (Daejung, Korea).
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3

Polypropylene Composite Synthesis

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Polypropylene (PP) having melt index of 16 g/10 min was kindly supplied by S-Oil Corp. (Korea). Citric acid (CA), 4-dimethylaminopyridine (DMAP), and tannic acid (TA) were purchased from Alfa Aesar Korea. Graphite powders were purchased from BASF (Germany). N,N′-Dicyclohexylcarbodiimide (DCC), phosphorus pentoxide (P2O5), potassium permanganate (KMnO4), sodium nitrate (NaNO3) were purchased from Sigma-Aldrich Korea. Cardanol was received from Mercury Co., Ltd. (India). Ethanol, hydrogen peroxide (H2O2), petroleum ether, sulfuric acid (H2SO4), and tetrahydrofuran (THF) were purchased from Daejung Chemicals & Metals. All reagents and solvents were used as received.
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4

Synthesis of Graphene-CMC Composite

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Sodium carboxymethyl cellulose (CMC, average M  ~ 250,000) and graphite flakes were purchased from Sigma Aldrich Korea. Sulfuric acid (H2SO4; 98%) and phosphoric acid (H3PO4; 85%) were purchased from DAEJUNG and DUKSAN, respectively. Potassium permanganate (KMnO4; 99.3%) and hydrogen peroxide (H2O2; 30%) were purchased from OCI Company Ltd., Korea. Hydrochloric acid (HCl; 35%–37%) and anhydrous ethyl alcohol (99.5%) were purchased from SAMCHUN and DAEJUNG, respectively. CNTs were supplied by Nanosolution Co., Korea.
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