CALB immobilised in acrylic resin (EC 3.1.1.3, 10,000 U/g) (Novozyme 435), xanthine oxidase from bovine milk, xanthine, allopurinol, hesperidin, naringin, and rutin standards and hexanoic, octanoic, decanoic, lauric, and oleic acids were obtained from the Sigma-Aldrich Chemical Co., St. Louis, MO. All the solvents and reagents were of analytical, spectrometric, or chromatographic quality.
Decanoic
Manufactured by Merck Group
Sourced in United Kingdom
Decanoic is a straight-chain saturated fatty acid with the chemical formula CH3(CH2)8COOH. It is a colorless liquid with a mild odor. Decanoic acid is commonly used as a laboratory reagent and in the production of various chemicals and materials.
Automatically generated - may contain errors
Lab products found in correlation
Allopurinol, by Merck Group (1 mentions)
Hesperidin, by Merck Group (1 mentions)
Naringin, by Merck Group (1 mentions)
Xanthine, by Merck Group (1 mentions)
Hexanoic, by Merck Group (1 mentions)
Octanoic, by Merck Group (1 mentions)
Lauric, by Merck Group (1 mentions)
Oleic acid, by Merck Group (1 mentions)
Rutin, by Merck Group (1 mentions)
Rs100, by Merck Group (1 mentions)
Eudragit rs100, by Evonik (1 mentions)
Stearic, by Merck Group (1 mentions)
Myristic, by Merck Group (1 mentions)
3 protocols using decanoic
1
Enzymatic Biocatalysis with Immobilized CALB
2
Electrospun Fatty Acid-Loaded Polymer Patches
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Electrospinning
methods including solution preparation and patch
production for both PCL and PVP/RS100 patches were performed as previously
described by Santocildes et al.(23 (link)) Briefly, PCL (Mw 80 kDa; Sigma-Aldrich,
Poole, UK) was added at 10 wt % to a solution of dichloromethane/N,N-dimethylformamide (93:7 w/w %; Thermo
Fisher Scientific, Altrincham, UK) and mixed at room temperature until
dissolved. PVP (Kollidon 90 F, Mw 1000–1500
kDa; BASF, Cheadle, UK) at 10 wt % and Eudragit RS100 (Mw 32 kDa; Evonik Industries AG, Essen, Germany) at 12.5
wt % were dissolved in 97% w/w ethanol prepared in deionized water
at room temperature. In this study, short-to-medium-chain fatty acids
including butanoic (C5), hexanoic (C6), heptanoic (C7), octanoic (C8),
nonanoic (C9), decanoic (C10), undecanoic (C11), or dodecanoic (C12)
(all from Sigma-Aldrich, Poole, UK) were added to the polymer dope
solutions at a concentration of 0.2 M prior to spinning. Spinning
conditions were 17 kV, 3 mL/h with a 15 cm tip-to-collector distance. 1H NMR spectroscopy was used to show that solvents were absent
in the final composition of patches (Figure S1 ).
methods including solution preparation and patch
production for both PCL and PVP/RS100 patches were performed as previously
described by Santocildes et al.(23 (link)) Briefly, PCL (Mw 80 kDa; Sigma-Aldrich,
Poole, UK) was added at 10 wt % to a solution of dichloromethane/N,N-dimethylformamide (93:7 w/w %; Thermo
Fisher Scientific, Altrincham, UK) and mixed at room temperature until
dissolved. PVP (Kollidon 90 F, Mw 1000–1500
kDa; BASF, Cheadle, UK) at 10 wt % and Eudragit RS100 (Mw 32 kDa; Evonik Industries AG, Essen, Germany) at 12.5
wt % were dissolved in 97% w/w ethanol prepared in deionized water
at room temperature. In this study, short-to-medium-chain fatty acids
including butanoic (C5), hexanoic (C6), heptanoic (C7), octanoic (C8),
nonanoic (C9), decanoic (C10), undecanoic (C11), or dodecanoic (C12)
(all from Sigma-Aldrich, Poole, UK) were added to the polymer dope
solutions at a concentration of 0.2 M prior to spinning. Spinning
conditions were 17 kV, 3 mL/h with a 15 cm tip-to-collector distance. 1H NMR spectroscopy was used to show that solvents were absent
in the final composition of patches (
3
Fatty Acid Hydrogenation and Acetylation
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Chemicals were purchased from Sigma-Aldrich (Brazil and Canada). Decanoic, myristic, stearic, and oleic acids were purchased from Sigma-Aldrich. Cardanol mixture was donated by Resibras/Cashol (Fortaleza, Brazil). Hydrogenation were performed in a shaker hydrogenation apparatus (Paar Instruments). The acetylation reactions were performed in a household microwave Brastemp BMK38ABHNA model and power 900 W. Chromatographic separations were performed using silica gel columns by flash (silica gel 60, 230â€"400 and 70â€"230 mesh, Silicycle) chromatography with the solvent
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