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3 protocols using hgcl2

1

Synthesis of Chalcogenide Nanocrystals

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Mercury chloride (HgCl2, Strem Chemicals, 99%), tellurium powder (Te, Sigma-Aldrich, 99.99%), selenium powder (Se, Sigma-Aldrich, 99,99%), trioctylphosphine (TOP, Cytek, 90%), oleylamine (Acros, 80–90%), dodecanethiol (Sigma-Aldrich, 98%), EDT (Fluka, 98.0%), lithium perchlorate (LiClO4, Sigma-Aldrich, 98%), polyethylene glycol (PEG, Mw = 6 kg mol−1), chloroform (VWR), ethanol absolute anhydrous (VWR), methanol (Carlo Erba, 99.8%), acetone (VWR), n-hexane (VWR), n-octane (SDS, 99%), and toluene (Carlo Erba, 99.3%) were used. All chemicals were used as received, except oleylamine, which was centrifuged before use. Mercury compounds are highly toxic and must be handled with special care.
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2

Synthesis of Tellurium Nanoparticles

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Mercury chloride (HgCl2, Strem Chemicals, 99%), Mercury compounds are highly toxic. Handle them with special care. Tellurium powder (Te, Sigma-Aldrich, 99.99%), trioctylphosphine (TOP, Alfa, 90%), oleylamine (OLA, Acros, 80–90%), dodecanethiol (DDT, Sigma-Aldrich, 98%), methanol (VWR, 98.5%) acetone (VWR rectapur), ethanol (absolute VWR), toluene (VWR, 99.8%), hexane (VWR), dimethylformamide (DMF, VWR, 99.9%), mercaptoethanol (MpOH, Merck, >99%). All chemicals are used without any further purification.
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3

Synthesis of Colloidal Nanocrystals

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Mercury chloride (HgCl2, Strem Chemicals, 99%), tellurium powder (Te, Sigma-Aldrich, 99.99%), trioctylphosphine (TOP, Cytek, 90%), oleylamine (Acros, 80-90%), dodecanethiol (DDT, Sigma-Aldrich, 98%), 1,2,ethanedithiol (EDT, Fluka, 98.0%), hydrochloric acid (HCl, Mieuxa, 25%), lithium perchlorate (LiClO4, Sigma-Aldrich, 98%), polyethylene glycol (PEG, Mw = 6kg.mol -1 ), chloroform (Carlo Erba), ethanol absolute anhydrous (Carlo Erba, 99.9%), methanol (Carlo Erba, 99.8%), acetone (Carlo Erba, 99.8%), n-hexane (Carlo Erba), n-octane (SDS, 99%), toluene (Carlo Erba, 99.3%),. All chemical are used as received, except oleylamine which is centrifuged before used. Mercury compounds are highly toxic. Handle them with special care.
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