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Lambda 650s spectrometer

Manufactured by PerkinElmer

The Lambda 650S spectrometer is a high-performance, double-beam UV-Vis spectrophotometer designed for a wide range of analytical applications. It features a wavelength range of 190 to 900 nm and a spectral bandwidth of 0.1 to 5.0 nm. The instrument provides accurate and reliable absorbance, transmittance, and reflectance measurements.

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2 protocols using lambda 650s spectrometer

1

Visible Spectrum Reflectance Characterization

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Reflectance
measurements
in the visible region (400–800 nm) were recorded on BSi samples
using a Lambda 650S spectrometer (Perkin Elmer) equipped with an integrating
sphere. The spectra resolution of the instrument is 0.17 nm, and the
measurements were recorded with a 1 nm step.
Angle-resolved
reflectivity measurements were carried out using a custom-built 2θ
system, as shown in Figure S12. The system
consisted of a Thorlabs halogen lamp weakly focused onto a sample
positioned on the inner stage of the rotating 2θ system. The
reflected light was collected by means of a collection lens and optical
fiber mounted on the outer stage of the system, which rotated at twice
the rate of the inner stage. The fiber was connected to an Ocean Optics
USB4000 visible range spectrometer with a spectral resolution of 0.2
nm. The measurements were carried out with an angular step of 0.5°
and for the wavelength range 400–750 nm (where applicable,
values are reported as average value ±1 s, where s stands for sample standard deviation).
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2

Synthesis and Characterization of Na-Based Polyoxometalate

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Na 9 [B-α-SbW 9 O 33 ]•19.5H 2 O as a precursor material was prepared according to literature protocols 58 and its purity was confirmed by FT-IR spectroscopy. Other chemicals were commercially purchased and used without further purification. Elemental analyses of all polyanions were performed by Mikroanalytisches Labor Pascher, Remagen, Germany. Fourier transform infrared (FT-IR) spectra were recorded on a Bruker Optics Vertex 70 Spectrometer. Raman spectroscopy was performed on a Renishaw Ramascope 1000 with a green SpectraPhysics Argon laser with a wavelength of 524.5 nm and 50 mW capacity. TG measurements were conducted on a Netzsch STA 449 C between 25 and 800 °C with a heating rate of 5 K min -1 in nitrogen atmosphere. UV/vis spectra were recorded on a PerkinElmer Lambda 650S spectrometer. Cyclic voltammetry experiments were performed on a Metrohm Computrace Voltammetric Analyzer model 757 VA. The system was operated with 757 VA Computrace software (Metrohm). The three-electrode cell system consisted of a 2 mm glassy carbon working electrode (GCE, modified or unmodified), a saturated Ag/AgCl reference electrode and a Pt wire as the counter electrode.
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