The chemicals used in this study were ethanol analytical grade (Merck CAS 64-17-5100983), chloroform (Merck CAS 67-66-3102445), acetic acid (Merck CAS 64-19-7100056), Mayer’s reagent (Sigma-Aldrich), Dragendorff’s reagent (Sigma-Aldrich), sulfuric acid (Merck CAS 7664-93-9100731), sodium hydroxide (Merck), sodium carbonate (Merck), magnesium turnings (Sigma-Aldrich), Folin-Ciocalteu’s reagent (Merck), gallic acid (Merck), dimethyl sulfoxide (DMSO), beta-sitosterol (Sigma-Aldrich), toluene (Merck), ethyl acetate (Merck), Lieberman Burchard’s reagent (Merck).
Magnesium turnings
Manufactured by Merck Group
Sourced in Canada
Magnesium turnings are small, thin strips of the metallic element magnesium. They are commonly used in various laboratory applications, serving as a reducing agent and a source of magnesium in scientific experiments and research.
Automatically generated - may contain errors
Lab products found in correlation
Ethyl acetate, by Merck Group (2 mentions)
Sulfuric acid, by Merck Group (1 mentions)
Dimethyl sulfoxide (dmso), by Merck Group (1 mentions)
Sodium hydroxide (naoh), by Merck Group (1 mentions)
Sodium carbonate, by Merck Group (1 mentions)
Chloroform, by Merck Group (1 mentions)
Toluene, by Merck Group (1 mentions)
Folin ciocalteu s reagent, by Merck Group (1 mentions)
Dragendorff s reagent, by Merck Group (1 mentions)
Mayer s reagent, by Merck Group (1 mentions)
Acetic acid, by Merck Group (1 mentions)
Gallic acid, by Merck Group (1 mentions)
Beta sitosterol, by Merck Group (1 mentions)
Hexane, by Merck Group (1 mentions)
Glycerol, by Merck Group (1 mentions)
Poly l lysine (pll), by Merck Group (1 mentions)
N n dimethylformamide (dmf), by Merck Group (1 mentions)
Laminin, by Thermo Fisher Scientific (1 mentions)
Iodine, by Merck Group (1 mentions)
D mannitol, by Merck Group (1 mentions)
4 protocols using magnesium turnings
1
Phytochemical Screening of Extracts
2
Chemical Preparation and Characterization
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Oxaliplatin (L-OHP), H2O2 and AITC were purchased from Wako Pure Chemical Industries (Osaka, Japan). HC030031 was obtained from Shanghai Haoyuan Chemexpress (Shanghai, China). Menthol, 2-aminoethoxydiphenyl borate, PBN, DMO, Pt(DACH)Cl2, cremophore EL, poly-L-lysine, D-mannitol, glycerol, 2,2′,4,4′-tetrahydroxybenzophenone, magnesium turnings, hexane, DMF, THF, iodine and ethyl acetate were purchased from Sigma-Aldrich (St Louis, MO). The BAPTA (1,2-bis(2-aminophenoxy)ethane-N,N,N',N'-tetraacetic acid) was acquired from Dojindo Laboratories (Kumamoto, Japan). DMOG was purchased from Frontier Scientific (Logan, Utah). The mitoTEMPO was obtained from Santa Cruz (Dallas, TX). Laminin was acquired from Life Technologies (Carlsbad, CA). N,N-diisopropylethylamine, 2-bromo-5-methoxytoluene, TBDMS-Cl and PdCl2(dppf)·CH2Cl2 complex (1:1) were purchased from Tokyo Chemical Industry (Tokyo, Japan). Sodium acetate and bis(pinacolato)diboron was purchased from WAKO (Osaka, Japan). Other drugs and chemicals were obtained from Nacalai Tesuque (Kyoto, Japan).
3
Isolation and Characterization of Coal Tar Components
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Anthracene (>90%) was purchased
from Alfa Aesar and used as received. Nitrobenzene (99%) as an internal
standard was purchased from Fisher Scientific (New Jersey), toluene
(99.5%) was purchased from Caledon Laboratories Ltd. (Georgetown,
ON, Canada), acetonitrile (high-performance liquid chromatography
grade, 99.9%) was purchased from ACP Chemicals (Montreal, Canada),
and anhydrous ethanol was purchased from Commercial Alcohols (Brampton,
ON, Canada). All of these chemicals were used without further purification
except acetonitrile, which was dried over molecular sieves for 2 weeks.
Glacial acetic acid (>99.85%), magnesium powder (≤150 μm,
98% purity), magnesium turnings (∼4000 μm, 98% purity),
and graphite (99.99%) were purchased from Sigma-Aldrich, Canada. Coal
tar samples were collected from Sydney Tar Ponds, Nova Scotia, Canada,
according to the coal tar sampling methodology.38
from Alfa Aesar and used as received. Nitrobenzene (99%) as an internal
standard was purchased from Fisher Scientific (New Jersey), toluene
(99.5%) was purchased from Caledon Laboratories Ltd. (Georgetown,
ON, Canada), acetonitrile (high-performance liquid chromatography
grade, 99.9%) was purchased from ACP Chemicals (Montreal, Canada),
and anhydrous ethanol was purchased from Commercial Alcohols (Brampton,
ON, Canada). All of these chemicals were used without further purification
except acetonitrile, which was dried over molecular sieves for 2 weeks.
Glacial acetic acid (>99.85%), magnesium powder (≤150 μm,
98% purity), magnesium turnings (∼4000 μm, 98% purity),
and graphite (99.99%) were purchased from Sigma-Aldrich, Canada. Coal
tar samples were collected from Sydney Tar Ponds, Nova Scotia, Canada,
according to the coal tar sampling methodology.38
4
Synthesis of Functional Polymers
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Acrylic acid (Sigma-Aldrich, anhydrous, contains 200 ppm MEHQ as inhibitor, 99%,), and pyrrole (Sigma-Aldrich, 98%) were distilled before use. Anhydrous N,N-dimethylformamide (DMF) and tetrahydrofuran (THF) were obtained using a Grubbs dry solvent system 34 (models SPS 400-6 and SPS200-6).
Sodium hydride (Sigma-Aldrich, 60% in mineral oil), carbon disulfide (Sigma-Aldrich, 99.9%), 4-vinylbenzyl chloride (Sigma-Aldrich, 90%), magnesium turnings (Sigma Aldrich, 98%), bromobenzene (Sigma-Aldrich, 99% C NMR spectra were recorded on a Bruker AV-400 instrument running at 100MHz at ambient temperature. 50 mg samples were dissolved in deuterated solvent, filtered and placed into a 7 inch NMR tube.
Sodium hydride (Sigma-Aldrich, 60% in mineral oil), carbon disulfide (Sigma-Aldrich, 99.9%), 4-vinylbenzyl chloride (Sigma-Aldrich, 90%), magnesium turnings (Sigma Aldrich, 98%), bromobenzene (Sigma-Aldrich, 99% C NMR spectra were recorded on a Bruker AV-400 instrument running at 100MHz at ambient temperature. 50 mg samples were dissolved in deuterated solvent, filtered and placed into a 7 inch NMR tube.
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