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930 compact ic

Manufactured by Metrohm

The 930 Compact IC Flex is an ion chromatography (IC) system designed for routine anion and cation analysis. It features a compact and robust design with a small footprint, suitable for installation in limited laboratory spaces. The system combines high-performance liquid chromatography (HPLC) with suppressed conductivity detection, providing reliable and accurate measurements of ion concentrations in various sample types.

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Lab products found in correlation

3 protocols using 930 compact ic

1

Quantification of Haloacetic Acids and Chloride

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All aqueous samples for TCAA, DCAA, MCAA, AA, and chloride were first filtered though 0.22-μm polyvinylidene difluoride syringe filter and then quantified using anionic chromatography (IC) (Metrohm 930 Compact IC). The IC had a Metrosep A supp 5 −250/4.0 column and an eluent of 1 mM sodium bicarbonate (NaHCO3) and 3.2 mM sodium carbonate (Na2CO3) with a flow rate of 0.7 mL/min. The detection limits of TCAA, DCAA, MCAA, AA, and chloride were 15, 15, 10, 10, and 3 μg/L, respectively.
To verify the actual PdNPs loading on membrane surface, an entire bundle of fiber membranes coated with PdNPs was dissolved through microwave-assisted total digestion (Luo et al., 2020 ) at the end of catalysts loading batch tests. An inductively coupled plasma mass spectrometry (ICP-MS; PerkinElmer NexION 1000) was used to measure the Pd concentration of digestied Pd solutions and effuents taken during continuous operation.
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2

Quantifying Sulfur Metabolism in Thermophilic Cultures

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Triplicate 100 ml dilutions with 20 ml headspace were prepared from C6- and C14-oxidizing cultures, supplied with substrate and incubated at 70 °C, complemented by a substrate-free negative control. Sulfate and DIC concentrations were measured from weekly subsamples until the cultures had reached sulfide concentrations of ≥15 mM. Samples were sterile filtered using a GTTP polycarbonate filter (0.2 μM pore size; Millipore). For DIC measurements, 1 ml filtrate was transferred into synthetic-air-purged 12 ml Exetainer vials (Labco) filled with 100 µl phosphoric acid (45%). After 10 h of equilibration, headspace DIC was measured by isotope ratio infrared spectroscopy (Thermo Fisher; Delta Ray IRIS with URI connect and Cetac ASX-7100 autosampler) with standards of known concentration. To determine sulfate concentrations, 1 ml of the filtrate was fixed in 0.5 ml 100 mM zinc acetate. The sample was centrifuged and the clear supernatant was diluted 1:50 in deionized water. Sulfate was measured by ion chromatography (930 compact IC, Metrohm) against standards with known concentrations.
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3

Quantifying Sulfide and Sulfate Levels

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Sulfide and sulfate concentrations were determined from the Zn acetate–fixed medium samples. Exact sample/fixative ratios were determined by weighing empty vials, Zn acetate–filled vials, and vials with samples. To determine sulfide concentrations, zinc acetate–fixed samples were resuspended, and 100-ml aliquots were sampled. Samples were measured using the diamine assay and spectrophotometric detection using standards with known sulfide concentrations (65 , 66 ). For sulfate measurements, zinc-fixed samples were 1:50 diluted in Milli-Q water and measured by ion chromatography (930 compact IC, Metrohm) against standards with known sulfate concentrations.
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