Iron acetylacetonate (Fe(acac)3 99%), 1,2-tetradecanediol (technical grade, 90%), oleic acid (technical grade, 90%), oleylamine (technical grade, 70%), benzyl ether (98%), and 1,1′-dioctadecyl-3,3,3′,3′-tetramethylindocarbocyanine perchlorate (DiI) were purchased from Sigma-Aldrich. 1,2-Distearoyl-snglycero-3-phosphoethanolamine-N-[methoxy(polyethylene glycol)-2000] (ammonium salt) (DSPE-PEG2000) were purchased from Avanti Polar Lipids. All chemicals were used as received.
Iron acetylacetonate
Manufactured by Merck Group
Sourced in United States
Iron acetylacetonate is a coordination compound used as a precursor and reagent in various chemical processes. It is a crystalline solid that is soluble in organic solvents. The compound is commonly utilized in research and industrial applications that require the introduction of iron into a reaction or system.
Automatically generated - may contain errors
Lab products found in correlation
Oleic acid, by Merck Group (12 mentions)
Benzyl ether, by Merck Group (10 mentions)
Oleylamine, by Merck Group (10 mentions)
Sodium hydroxide (naoh), by Merck Group (5 mentions)
1 2 hexadecanediol, by Merck Group (4 mentions)
Manganese acetylacetonate, by Merck Group (4 mentions)
Hydrochloric acid (hcl), by Merck Group (3 mentions)
Silver nitrate, by Merck Group (3 mentions)
Hexane, by Merck Group (3 mentions)
1 2 tetradecanediol, by Merck Group (2 mentions)
1 1 dioctadecyl 3 3 3 3 tetramethylindocarbocyanine perchlorate dii, by Merck Group (2 mentions)
Toluene, by Merck Group (2 mentions)
Ferrous chloride, by Merck Group (2 mentions)
Iron pentacarbonyl, by Merck Group (2 mentions)
Cobalt nitrate, by Merck Group (2 mentions)
Oxalic acid, by Merck Group (2 mentions)
Copper nitrate, by Merck Group (2 mentions)
Sodium molybdate dehydrate, by Merck Group (2 mentions)
Lanthanum oxide, by Merck Group (2 mentions)
Cobalt oxalates, by Merck Group (2 mentions)
18 protocols using iron acetylacetonate
1
Synthesis of Fluorescent Nanoparticles
2
Synthesis and Functionalization of SPIO Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
SPIO nanocrystals were synthesized by thermal decomposition of iron acetylacetonate (Sigma Aldrich, St Louis, MO, USA), and the crystal size was tuned by modifying the reaction conditions (namely the reaction temperature and solvent) as previously reported.27 (link) The detailed procedures were described in Supporting Information. The citric acid (1 g) was dissolved in 70 mL of ultrapure water, and NaOH was added to adjust the pH as 7.2. One hundred and ten milliliter acetone and 70-mL SPIO hexane solution (containing 50-mg nanoparticles) were added. The mixture was stirred and refluxed for 48 h. The sodium citrate coated SPIO (SPIO@CA) was obtained by centrifugation after ligand exchange, and subsequently dispersed in ultrapure water. Then, 150 mg of mPEG-DA (Mn = 550, 2k or 5k Da) and 5 mL of SPIO@CA solution (containing 10-mg nanoparticles) were mixed and magnetically stirred under a flow of nitrogen for 72 h at 40°C after being deoxidized. The solution was dialyzed against water for 2 days to obtain PEGylated SPIO (SPIO@PEG). The concentration of iron was determined using an atomic absorption spectrometer (AAS).
3
Synthesis of PAN-based Nanocomposite Fibers
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All chemicals were analytical pure and used without any pre-purification. Polyacrylonitrile (PAN, Mw = 150,000) and Iron acetylacetonate (97%) were purchased from Sigma-Aldrich Company. N, N-dimethyl formamide (DMF, 99.5%), Ethyl orthosilicate (TEOS), ammonium hydroxide (NH3·H2O, 25%), ethanol (C2H5OH, 99.7%) and sodium hydroxide (NaOH, 96%) were obtained from Beijing Chemical Reagent Co. Ltd.
4
Synthesis and Characterization of Iron Oxide Nanoparticles
5
Synthesis of Nanocomposite Materials
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Iron acetylacetonate, oleic acid, oleyl amine, ammonia (28 wt % in water), hydrogen peroxide (30 wt % in water), sodium chloride, sodium molybdate dehydrate, thiourea, ferrous chloride, cobalt acetate, ethylene glycol, zinc acetate, lanthanum oxide, cobalt nitrate, tetraethyl orthosilicate, sodium hydroxide, oxalic acid, strontium carbonate, cobalt oxalates, bismuth nitrate pentahydrate, diboron trioxide, 1-butyl-3-methlyimidazolium hexafluorophosphate (BmimPF6), silver nitrate, stannous chloride, sulfur powder, ethylenediaminetetraacetic acid disodium, copper nitrate, hexadecyltrimethylammonium bromide, formaldehyde, mercury oxide, mercury, cyclohexane, isopropanol, iron pentacarbonyl, 1,3-dimethylimidazoline-2-selenone, hydrochloric acid (38 wt % in water), tellurium power, selenium powder, potassium hydroxide, sulfuric acid and sulfide powder were purchased from Sigma-Aldrich. Raw graphene and multiwall carbon nanotubes were obtained from XF-NANO Tech. Co. All chemical reagents are analytical pure reagents and were used without further purification. Polydimethylsiloxane (PDMS) film was purchased from Shanghai Muke Technol. Co. Deionized water used in all the experiments was purified using a Simplicity C9210 Milli-Q water purification system.
6
Synthesis of Multifunctional Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The reagents cobalt acetylacetonate
[Co(acac)2, purity
97%], iron acetylacetonate [Fe(acac)3, purity ≥99.9%],
silver nitrate (AgNO3, purity ≥99.9999%), 1,2-hexadecanediol
(purity 90%), sodium hydroxide (NaOH, purity ≥98%), oleylamine
(OLA, purity 70%), oleic acid (OA, purity 90%), and tetraethylene
glycol (TEG, purity 99%) were purchased from Sigma-Aldrich (St. Louis,
USA) and were used as received. PLL was purchased from JNC Co. (Tokyo,
Japan), and 2-iminothiolane and ethanol were purchased from Nacalai
Tesque (Kyoto, Japan). Acetone and hexane were purchased from Kanto
Chemical (Tokyo, Japan), and toluene and hydrochloric acid (HCl) were
purchased from Wako Pure Chemical (Osaka, Japan).
[Co(acac)2, purity
97%], iron acetylacetonate [Fe(acac)3, purity ≥99.9%],
silver nitrate (AgNO3, purity ≥99.9999%), 1,2-hexadecanediol
(purity 90%), sodium hydroxide (NaOH, purity ≥98%), oleylamine
(OLA, purity 70%), oleic acid (OA, purity 90%), and tetraethylene
glycol (TEG, purity 99%) were purchased from Sigma-Aldrich (St. Louis,
USA) and were used as received. PLL was purchased from JNC Co. (Tokyo,
Japan), and 2-iminothiolane and ethanol were purchased from Nacalai
Tesque (Kyoto, Japan). Acetone and hexane were purchased from Kanto
Chemical (Tokyo, Japan), and toluene and hydrochloric acid (HCl) were
purchased from Wako Pure Chemical (Osaka, Japan).
7
Synthesis of Functional Nanomaterials
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Poly(maleic
anhydride-alt-1-octadecene), Mn 30 000–50 000
g/mol (Aldrich),
Milli-Q water (18.2 MΩ, filtered with filter pore size 0.22
μM) from Millipore, acetonitrile (HPLC grade, J. T. Baker) and
tetrahydrofuran anhydride (Carlo Erba, p.a.), iron oxide hydroxide
(Sigma-Aldrich, #371254), iron acetylacetonate (Sigma-Aldrich, 99%),
manganese acetylacetonate (Sigma-Aldrich, #245763), hexadecanediol
(Sigma-Aldrich, 90%), dodecylamine (Sigma-Aldrich, 98%), lauric acid
(Sigma-Aldrich, 99%), benzyl ether (Sigma-Aldrich, 98%), and octadecene
(Sigma-Aldrich, 90%), YCl3, YbCl3, ErCl3, ammonium fluoride, and sodium oleate, tri-n-octylphosphine oxide (Strem, 99%), tri-n-octylphosphine
(Strem, 97%), n-octadecylphosphonic acid (PolyCarbon
Industries, 99%), cadmium oxide (Sigma-Aldrich, 99.99%), selenium
(Sigma-Aldrich, 99.99%), diethylzinc (Sigma-Aldrich, 1 M in hexane)
and hexamethyldisilathiane (Sigma-Aldrich, synthesis grade), ethanol
(Sigma-Aldrich, 99.8%), methanol (Sigma-Aldrich, 99.9%), toluene (Sigma-Aldrich,
99.5%), and hexane (Sigma-Aldrich, 99%) were used without any further
purification. All reagents for cell cytotoxicity assay were purchased
from Gibco (ThermoFisher Scientific).
anhydride-alt-1-octadecene), Mn 30 000–50 000
g/mol (Aldrich),
Milli-Q water (18.2 MΩ, filtered with filter pore size 0.22
μM) from Millipore, acetonitrile (HPLC grade, J. T. Baker) and
tetrahydrofuran anhydride (Carlo Erba, p.a.), iron oxide hydroxide
(Sigma-Aldrich, #371254), iron acetylacetonate (Sigma-Aldrich, 99%),
manganese acetylacetonate (Sigma-Aldrich, #245763), hexadecanediol
(Sigma-Aldrich, 90%), dodecylamine (Sigma-Aldrich, 98%), lauric acid
(Sigma-Aldrich, 99%), benzyl ether (Sigma-Aldrich, 98%), and octadecene
(Sigma-Aldrich, 90%), YCl3, YbCl3, ErCl3, ammonium fluoride, and sodium oleate, tri-n-octylphosphine oxide (Strem, 99%), tri-n-octylphosphine
(Strem, 97%), n-octadecylphosphonic acid (PolyCarbon
Industries, 99%), cadmium oxide (Sigma-Aldrich, 99.99%), selenium
(Sigma-Aldrich, 99.99%), diethylzinc (Sigma-Aldrich, 1 M in hexane)
and hexamethyldisilathiane (Sigma-Aldrich, synthesis grade), ethanol
(Sigma-Aldrich, 99.8%), methanol (Sigma-Aldrich, 99.9%), toluene (Sigma-Aldrich,
99.5%), and hexane (Sigma-Aldrich, 99%) were used without any further
purification. All reagents for cell cytotoxicity assay were purchased
from Gibco (ThermoFisher Scientific).
8
Synthesis and Characterization of Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Iron acetylacetonate, manganese acetylacetonate, oleic acid, oleylamine, benzyl ether, hexane, ε-caprolactone, tetrahydrofuran (THF), N-(3-dimethylaminopropyl)-Nese acetylacetonate, N-hydroxysuccinimide, stannous octoate, tetramethylammonium hydroxide (TMAH), heparin, L-glutamine, reactive oxygen species (ROS) assay kit, and sodium pyruvate were all purchased from Sigma-Aldrich Co. (St Louis, MO, USA). PEG with a terminal hydroxyl and carboxylic acid functional groups (COOH-PEG-OH) was purchased from JenKem Technology (Beijing, People’s Republic of China). 1,2-Hexadecanediol was obtained from TCI (Shanghai) Development Co., Ltd (Shanghai, People’s Republic of China). Medium 199, Roswell Park Memorial Institute 1640 medium, fetal bovine serum, penicillin/streptomycin, and nonessential amino acid were purchased from Hyclone, Logan, UT, USA. Count Kit-8 (CCK-8) was obtained from Beyotime Biotechnology Company, Beijing, People’s Republic of China. Endothelial cell growth supplement was purchased from Sciencell, CA, Carlsbad, USA. Six-well plates were obtained from Corning Incorporated, Corning, NY, USA.
9
Synthesis of Functionalized Magnetic Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Poly(maleic anhydride-alt-1-octadecene), Mn 30,000–50,000 (Aldrich), Milli-Q
water
(18.2 MΩ, filtered with filter pore size 0.22 μM) from
Millipore, acetonitrile (HPLC grade, J. T. Baker) and tetrahydrofuran
anhydride (Carlo Erba, p.a.), iron oxide hydroxide (Sigma-Aldrich,
#371254), iron acetylacetonate (Sigma-Aldrich, 99%), manganese acetylacetonate
(Sigma-Aldrich, #245763), hexadecanediol (Sigma-Aldrich, 90%), dodecylamine
(Sigma-Aldrich, 98%), lauric acid (Sigma-Aldrich, 99%), benzyl ether
(Sigma-Aldrich, 98%), and octadecene (Sigma-Aldrich, 90%), as well
as 1-ethyl-3-(3-(dimethylamino)propyl)carbodiimide hydrochloride (EDC)
(Aldrich, commercial grade), O-(2-aminoethyl)-O′-methyl polyethylene glycol (“aminoPEG750”,
Aldrich), N,N-dimethylethylenediamine
(for “tertiary amine functionalization”, Aldrich), 2-(2-pyridyl)ethylamine
(for “pyridine functionalization”, Aldrich), and 2,2′-(ethylendedioxy)bis(ethylamine)
(referred to in this article as “diamine” Aldrich),
tetramethylammonium hydroxide (TMAOH, Sigma-Aldrich) were used without
further purification. Acetonitrile (ACN, not anhydrous) was purchased
from J. T. Baker and stored in the glovebox.
water
(18.2 MΩ, filtered with filter pore size 0.22 μM) from
Millipore, acetonitrile (HPLC grade, J. T. Baker) and tetrahydrofuran
anhydride (Carlo Erba, p.a.), iron oxide hydroxide (Sigma-Aldrich,
#371254), iron acetylacetonate (Sigma-Aldrich, 99%), manganese acetylacetonate
(Sigma-Aldrich, #245763), hexadecanediol (Sigma-Aldrich, 90%), dodecylamine
(Sigma-Aldrich, 98%), lauric acid (Sigma-Aldrich, 99%), benzyl ether
(Sigma-Aldrich, 98%), and octadecene (Sigma-Aldrich, 90%), as well
as 1-ethyl-3-(3-(dimethylamino)propyl)carbodiimide hydrochloride (EDC)
(Aldrich, commercial grade), O-(2-aminoethyl)-O′-methyl polyethylene glycol (“aminoPEG750”,
Aldrich), N,N-dimethylethylenediamine
(for “tertiary amine functionalization”, Aldrich), 2-(2-pyridyl)ethylamine
(for “pyridine functionalization”, Aldrich), and 2,2′-(ethylendedioxy)bis(ethylamine)
(referred to in this article as “diamine” Aldrich),
tetramethylammonium hydroxide (TMAOH, Sigma-Aldrich) were used without
further purification. Acetonitrile (ACN, not anhydrous) was purchased
from J. T. Baker and stored in the glovebox.
10
Synthesis of Fe3-δO4 Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Fe3-δO4 nanoparticles (22 nm and 14 nm) were synthesized using thermal decomposition, as previously described30 (link). Briefly, 1.42 g of iron acetylacetonate was mixed with 0.57 mL of oleic acid and 20 mL of trioctylamine (all 3: Sigma-Aldrich, St. Louis, MO). The solution was refluxed at 325 °C in an argon environment for 30 minutes. After the solution had cooled down to room temperature, the precipitates were collected with a magnet and washed 3 times with toluene. The Fe3-δO4 nanoparticles were collected with a magnet and then transferred to chloroform solutions (Merck, Whitehouse Station, NJ) containing 0.4 mg/mL of PSMA (Sigma-Aldrich) and were left there for 6 hours at 55 °C. The Fe3-δO4 nanoparticles were collected, washed 3 times with MQ water, and then stored at 4 °C.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!