The largest database of trusted experimental protocols

6 protocols using lead oxide

1

Synthesis of Nanocrystalline Materials

Check if the same lab product or an alternative is used in the 5 most similar protocols
Cadmium acetate dihydrate (Sigma-Aldrich,
98%), myristic acid (Sigma-Aldrich, 98%), selenium (Se, Sigma-Aldrich,
99.99%), tellurium (Te, SigmaAldrich, 99.99%), copper chloride dihydrate
(ACS reagent, 99.8%), zinc acetate trihydrate (Zn(CH3COO)2·2H2O, Sigma-Aldrich, 98%), sodium borohydride
(NaBH4, Sigma-Aldrich, 96%), trioctylphosphine (TOP, Sigma-Aldrich,
technical grade, 90%), 1-octadecene (ODE, Sigma-Aldrich, technical
grade, 90%), oleylamine (technical grade, 70%), sulfur (S, Sigma-Aldrich,
<99.5%), oleic acid (technical grade, Sigma-Aldrich, 90%), cadmium
oxide (Sigma-Aldrich, 99.9%), and lead oxide (Alfa Aesar, 99.9%).
Hexane (AR grade, 99%), 1,4-butanediol (90%, AR), dextrose (95% anhydrous,
AR), HCl (99%), and HNO3 (98%) were purchased from SD Fine
Chemicals. All chemicals were used without further purification.
+ Open protocol
+ Expand
2

Synthesis of Lead Halide Perovskite Nanocrystals

Check if the same lab product or an alternative is used in the 5 most similar protocols
All chemicals were used as received unless otherwise noted. Lead oxide (PbO, 99.999%), lead iodide (PbI2, 99.9985%) and selenium shot (99.999%) were purchased from Alfa Aesar. Oleic acid (OA, technical grade, 90%), diphenylphosphine (DPP, 98%), 1-octadecene (ODE, 90%), anhydrous ethylene glycol (EG, 99.8%), anhydrous acetonitrile (99.99%), anhydrous hexanes (99%), anhydrous toluene (99.8%), 3-mercaptopropyltrimethoxysilane (3-MPTMS, 95%), trimethylaluminum (TMA, 97%), ammonium thiocyanate (NH4SCN, 99.99%) and anhydrous dimethyl sulfoxide (DMSO, 99.9%) were purchased from Sigma Aldrich. Anhydrous 1,2-ethylenediamine (EDA, > 98.0%) was purchased from TCI. Trioctylphosphine (TOP, technical grade, >90%) was acquired from Fluka and mixed with selenium shot for 24 h to form a 1 M TOP-Se stock solution. 18.2 MΩ water (Milli-Q Gradient) was used for substrate cleaning and atomic layer deposition (ALD). Water for ALD was degassed with three freeze-pump-thaw cycles before use.
+ Open protocol
+ Expand
3

Synthesis of Colloidal Lead-Based Nanocrystals

Check if the same lab product or an alternative is used in the 5 most similar protocols
Lead oxide (PbO, 99.99%), 1-octadecene (ODE, 99%), and oleic acid (OA, 99%) were purchased from Alfa Aesar. Bis(trimethylsilyl)sulfide (TMS, 97%) was purchased from TCI America. Zinc acetate dihydrate (98%), potassium hydroxide (85%), lead iodide (PbI2, 99%), lead bromide (PbBr2, 98%), ammonium acetate (NH4Ac, 98%), acetonitrile (99.8%), and 1,2-ethanedithiol (EDT, 98%) were purchased from Sigma-Aldrich.
+ Open protocol
+ Expand
4

Synthesis of Colloidal Nanocrystals

Check if the same lab product or an alternative is used in the 5 most similar protocols
Oleic acid (OA, 90 %), lead oxide (PbO, 99.9 %), 1-octadecene (ODE), CdCl2, and oleic amine (OLA) were purchased from Alfa Aesar. Mercaptopropionic acid Hexamethyldisilathiane (TMS), octyl-phosphine acid (OPA), tetradecyl phosphonic acid (TDPA), and octodecyl-phosphine acid (ODPA) were purchased from Aladdin. All chemicals were used directly without any further purification.
+ Open protocol
+ Expand
5

Synthesis of Semiconductor Nanocrystals

Check if the same lab product or an alternative is used in the 5 most similar protocols
Lead oxide (PbO, 99.995%), selenium (Se, 99.999% pure), n-octane (>98%) were purchased from Alfa Aesar. Hexane (anhydrous) and toluene (anhydrous) were purchased from VWR. Bis(trimethylsilyl)sulphide (TMS, >98%), cadmium oxide (CdO, 99.99%), 1-octadecene (ODE, technical grade 90%), oleic acid (OA, technical grade 90%), acetone (ACE, analytical grade), isopropanol (IPA, analytical grade), methanol (analytical grade), sulfuric acid (H 2 SO 4 , 97.5%) and hydrogen peroxide (H 2 O 2 , 30%) were purchased from Sigma Aldrich. Double-side polished silicon wafers were purchased from Siegert Wafer.
+ Open protocol
+ Expand
6

Synthesis of Lead Oxide Nanoparticles

Check if the same lab product or an alternative is used in the 5 most similar protocols
Lead oxide (PbO, 99.999%) was purchased from Alfa Aesar. Ethanol and 1-butanol (Hi-Dry anhydrous) were purchased from Romil. TIPS-Tc was obtained from Ark Pharm. All other chemicals were purchased from Sigma-Aldrich. All materials were used as received without further purification.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!