A Wilmad 522-PV-7 pressure NMR tube with a 5 mm outer diameter (OD) and a maximum pressure rating of 200 psi was used for all high pressure gas experiments. The tube comes equipped with a PV-ANV valve that is capable of accepting a Swagelok® 1/8” tubing nut and ferrule. PTFE tubing (OD = 1/8”) and Swagelok® 1/8” tubing nuts and ferrules were used for all the connections. PTFE tubing was used to connect the gas regulator to a T-shaped splitter which provided two paths. One path connected through PTFE tubing a high pressure gas gauge and the PV-ANV valve on the NMR tube. The second path connected the PTFE tubing to a Swagelok® valve, which was connected to a metal O-ring joint. The other part of the O-ring joint was equipped with a metal to glass flange that had a glass 14/20 female joint. This allowed the apparatus to be attached to the Schlenk line for evacuation.
522 pv 7 pressure nmr tube
Manufactured by Wilmad
The 522-PV-7 pressure NMR tube is a laboratory equipment designed for nuclear magnetic resonance (NMR) spectroscopy. It is a pressure-resistant glass tube used to contain samples during NMR analysis. The tube is engineered to withstand pressure, enabling the study of materials under elevated pressure conditions.
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2 protocols using 522 pv 7 pressure nmr tube
1
High Pressure NMR Tube Setup
2
High-Pressure NMR Tube Apparatus Setup
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A Wilmad
522-PV-7 pressure NMR tube with a 5 mm outer diameter (OD) and a maximum
pressure rating of 200 psi was used for all high-pressure gas experiments.
The tube comes equipped with a Wilmad PV-ANV valve that is capable
of accepting a Swagelok 1/8″ tubing nut and ferrule. Poly(tetrafluoroethylene)
(PTFE) tubing (OD = 1/8″) and Swagelok 1/8″ tubing nuts
and ferrules were used for all the connections. PTFE tubing was used
to connect the gas regulator to a T-shaped splitter, which provided
two paths. One path connected through PTFE tubing a high-pressure
gas gauge and the PV-ANV valve on the NMR tube. The second path connected
the PTFE tubing to a Swagelok valve, which was connected to a metal
O-ring joint. The other part of the O-ring joint was equipped with
a metal-to-glass flange that had a glass 14/20 female joint. This
allowed the apparatus to be attached to the Schlenk line for evacuation.
522-PV-7 pressure NMR tube with a 5 mm outer diameter (OD) and a maximum
pressure rating of 200 psi was used for all high-pressure gas experiments.
The tube comes equipped with a Wilmad PV-ANV valve that is capable
of accepting a Swagelok 1/8″ tubing nut and ferrule. Poly(tetrafluoroethylene)
(PTFE) tubing (OD = 1/8″) and Swagelok 1/8″ tubing nuts
and ferrules were used for all the connections. PTFE tubing was used
to connect the gas regulator to a T-shaped splitter, which provided
two paths. One path connected through PTFE tubing a high-pressure
gas gauge and the PV-ANV valve on the NMR tube. The second path connected
the PTFE tubing to a Swagelok valve, which was connected to a metal
O-ring joint. The other part of the O-ring joint was equipped with
a metal-to-glass flange that had a glass 14/20 female joint. This
allowed the apparatus to be attached to the Schlenk line for evacuation.
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