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3 protocols using n dimethylacetamide dmac

1

Cellulose Acetate Synthesis and Characterization

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Cellulose acetate (CA, Mn ~30,000) was provided by Sigma-Aldrich (St. Louis, MO, USA). Acetone was purchased from Hengfa Chemical Reagent Co., Ltd. (Tianjin, China). Methanol anhydrous, anhydrous citric acid, sodium citrate, sodium chloride, sodium hydroxide, N, N-Dimethylacetamide (DMAc), and 2,2-Diphenyl-1-picrylhydrazyl (DPPH) were obtained from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). Anhydrous ethanol was provided by Kermel Chemical Reagent Co., Ltd. (Tianjin, China). Hydrochloric acid was purchased from China Pingmei Shenma Group Kaifeng Dongda Chemical Co., Ltd. (Kaifeng, China).
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2

Fabrication of LiF/Ti3AlC2 Nanocomposite

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Lithium fluoride (LiF, 99%) was purchased by Sigma-Aldrich Co., Ltd. Ti3AlC2 powder was obtained from Jilin 11 Technology Co., Ltd. 4,4’-diaminodiphenyl ether (ODA, 99%), pyromellitic dianhydride (PMDA), N, N-dimethylacetamide (DMAc), hydrochloric acid (HCl, 37%), and triethylamine (TEA) were all purchased from Sinopharm Chemical Reagent Co. Multiwalled carbon nanotubes (CNT, TNWDM-M8) were acquired from Chengdu Organic Chemicals Co. Ltd.
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3

Fabrication of Polyacrylonitrile Membranes

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Polyacrylonitrile (PAN, Mw = 90,000 g/mol) was provided by Kunshan Hongyu Plastic Co. (Suzhou, China). Analytical grade N, N-dimethylformamide (DMF), N, N-dimethylacetamide (DMAC), sodium chloride (NaCl), magnesium chloride (MgCl2·6H2O) and hexane were obtained from Sinopharm Chemical Reagent Co. Ltd. (Shanghai, China). Chemicals used in PA formation: MPD (>99%) and TMC (98%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). All water used in this work was deionized (DI) water.
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