Ball-milled NMR samples were prepared according to the method previously described [33 (link)]. The crushed molding (200 mg) was ball-milled with a planetary Mono Mill PULVERISETTE 6 classic line (Fritsch GmbH, Idar-Oberstein, Germany), with vibration at 600 rpm in zirconium dioxide (ZrO2) vessels (12 mL) containing ZrO2 50 balls (5 mm × 5 mm). The grinding time to obtain samples was 80 min, in 20 min grinding/10 min intervals for four cycles to avoid excessive heating.
Mono mill pulverisette 6 classic line
Manufactured by Fritsch
Sourced in Germany
The Mono Mill PULVERISETTE 6 classic line is a laboratory equipment designed for the grinding and pulverization of solid samples. It features a vertical grinding chamber and a single grinding tool for efficient size reduction of materials.
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Lab products found in correlation
2 protocols using mono mill pulverisette 6 classic line
1
Ball-milled NMR Sample Preparation
2
Ball-Milling Method for NMR Sample Preparation
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The ball-milled NMR samples were prepared according to the method described in the literature [28 (link)]. The crushed molding (200 mg) was ball-milled with a planetary Mono Mill PULVERISETTE 6 classic line (Fritsch GmbH, Idar-Oberstein, Germany), with vibration at 600 rpm in zirconium dioxide (ZrO2) vessels (12 mL) containing ZrO2. 50 balls (5 mm × 5 mm). The grinding time was 80 min, in 20 min grinding/10 min intervals for four cycles to avoid excessive heating. The ball-milled sample was obtained.
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