Incl3

Manufactured by Merck Group

Sourced in India

InCl3, also known as indium chloride, is a chemical compound that is primarily used as a precursor in various industrial and scientific applications. It is a colorless to white crystalline solid at room temperature. InCl3 is soluble in water and other polar solvents. The main function of InCl3 is to serve as a starting material for the synthesis of other indium-containing compounds and materials.

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Indium (III) chloride (InCl3) (4 citations) Indium chloride(InCl3) (2 citations) InCl3·4H2O (2 citations)

16 protocols using incl3

Synthesis of Chalcogenide Semiconductors

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All materials
including SmCl₃, InCl₃, SbCl₃, NaBH₄, and Te powder purchased from Sigma Aldrich, having purity
above 99%, were used without further purification.

Komal N., Mansoor M.A., Mazhar M., Sohail M., Malik Z, & Anis-ur-Rehman M. (2023). Effect of (Sm, In) Doping on the Electrical and Thermal Properties of Sb2Te3 Microstructures. ACS Omega, 8(11), 9797-9806.

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Synthesis and Characterization of Nanomaterials

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InCl₃ (99.99%), GaCl₃ (99.99%), lauric acid (98%), palmitic acid (99%), Cs₂(CO₃) (99.9%), GdCl₃·6H₂O (99.9%),
Br₂ (≥99%), oleylamine (technical grade), 1-ODE
(technical grade), Se (≥99.5%), trioctylphosphine (97%) 1,
and 2-dimethoxyethane (99.5%) were all purchased from Sigma-Aldrich,
India. Pb(NO₃)₂ (99%), FeCl₃ (96%),
CoCl₂·6H₂O (98%), NiCl₂ (97%),
MnCl₂ (99%), Mg(NO₃)₂ (99%), and
oleic acid (65–88%) were purchased from Merck, India. 1-Dodecanthiol
(98%) was purchased from Loba Chemie. CuCl₂·2H₂O (99%), ZnCl₂ (97%), CdCl₂·H₂O (98%), KNO₃(99%), SnCl₂·2H₂0, and stearic acid (90%) were purchased from Thomas Baker,
India. Myristic acid (95%), AgNO₃ (99.8%), and AlCl₃ (96%) were purchased from SRL, Rankem, and Finar, respectively.
All the FTIR spectra were acquired using Bruker ALPHA E, 200396; the
TGA data were recorded on the TA Instrument Q-50 TGA. ¹H NMR was obtained in CDCl₃ and DMSO-d₆ using Bruker ASCEND 400. The UV–visible spectra
were collected using PerkinElmer (model: LS 55). The PL spectra were
acquired using the HORIBA scientific spectrophotometer (model: PTI-QM
510), and PXRD was recorded on a PANalytical X-ray diffractometer
using Cu Kα (λ = 1.54 Å) as the incident radiation
(40 kV and 30 mA).

Basel S., Bhardwaj K., Pradhan S., Pariyar A, & Tamang S. (2020). DBU-Catalyzed One-Pot Synthesis of Nearly Any Metal Salt of Fatty Acid (M-FA): A Library of Metal Precursors to Semiconductor Nanocrystal Synthesis. ACS Omega, 5(12), 6666-6675.

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Synthesis of ITO/RGO Nanocomposite

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Graphite oxide was synthesized from graphite powder by a modified Hummers’ method. The prepared graphite oxide (20 mg) was exfoliated in distilled water (10 mL) by sonication for 60 min to form a homogeneous suspension. To prepare ITO/RGO, SnCl₂·2H₂O (400 mg, Sigma-Aldrich, 98%) and InCl₃ (44 mg, Sigma-Aldrich, 98%) were dissolved in 200 ml HCl solution (0.02 M, Sigma-Aldrich, 37%). The graphite oxide suspension and SnCl₂–HCl solution were mixed under vigorous stirring while adding 500 mg urea (Sigma-Aldrich, 98%) to form a uniform solution. The resulting solution was ultrasonicated for 30 min, then refluxed at 120 °C for 6 h. When cooled to room temperature, the solid products were washed with distilled water 6 times to remove the byproducts, followed by drying at 100 °C under vacuum overnight. The powders were further heat-treated in a tube furnace at 500 °C for 2 h under Ar flow with a heating rate of 2 °C min⁻¹. SnO₂/RGO and In₂O₃/RGO were prepared in the same way without the presence of indium and tin additions, respectively.

Liu Y., Palmieri A., He J., Meng Y., Beauregard N., Suib S.L, & Mustain W.E. (2016). Highly Conductive In-SnO2/RGO Nano-Heterostructures with Improved Lithium-Ion Battery Performance. Scientific Reports, 6, 25860.

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Iron Binding Protein Interaction Study

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InCl₃, deferiprone, HQ, HQS, maltol, citric acid, oxalic acid, 4-(2-hydroxyethyl)-1-piperazineethanesulfonic acid (HEPES), HSA (product Nr.: A8763, essentially globulin free), apoTf (iron-free form, T2036), Tf containing physiological amount of iron (product Nr.: T3309, loaded with Fe(III) in 20–40%) and human serum (from male AB plasma, H4522) were purchased from Sigma-Aldrich. Inorganic chemicals such as KOH, KCl, HCl, NaCl, NaH₂PO₄, NaHCO₃ were products of Molar Chemicals or Reanal.

Dömötör O., Keppler B.K, & Enyedy É.A. (2022). Solution speciation and human serum protein binding of indium(III) complexes of 8-hydroxyquinoline, deferiprone and maltol. Journal of Biological Inorganic Chemistry, 27(3), 315-328.

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Synthesis of Nanocrystalline Materials

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Indium acetate (InOAc, 99.99%), OA (≥99%), dioctylamine (DOA, ≥97%), 1‐octadecene (ODE, 90%), ME (≥99%), and InCl₃ (≥98%) were purchased from Sigma‐Aldrich Chemical Co. Trimethylsilylarsine ((TMSi)₃As, 99%) was purchased from JSI Silicone. All solvents used in the experiments (hexane, butanol, and ethyl alcohol) were purchased from Sigma‐Aldrich Chemical Co.

Kim J., Jung B.K., Kim S., Yun K., Ahn J., Oh S., Jeon M., Lee T., Kim S., Oh N., Oh S.J, & Seong T. (2023). Ultrasensitive Near‐Infrared InAs Colloidal Quantum Dot‐ZnON Hybrid Phototransistor Based on a Gradated Band Structure. Advanced Science, 10(18), 2207526.

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Fabrication of CdS/CdTe Solar Cell Layers

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Indium tin oxide (ITO, ≤15 Ω/∀) sheet glass, titanium foil (Ti, Sigma-Aldrich, 0.25-mm thickness, 99.7% purity), ammonium fluoride (NH₄F, Sigma-Aldrich, 98 + %), ethylene glycol (Junsei Chemical Co, 99.0%), cadmium chloride (CdCl₂, Kanto Chemical Co, 98.0%), indium choride (InCl₃, Sigma-Aldrich, 99.999%), sodium sulfide nonahydrate (Na₂S, Sigma-Aldrich, 98.0%), cupric chloride (CuCl₂, Junsei Chemical co., Ltd, >97.0 + %), and Ti(OCH₂CH₂CH₂CH₃)₄ (Ti(OBu)₄, Sigma-Aldrich, 97%). All the materials were used directly without further purification.

Chen C., Ling L, & Li F. (2017). Double-Sided Transparent TiO2 Nanotube/ITO Electrodes for Efficient CdS/CuInS2 Quantum Dot-Sensitized Solar Cells. Nanoscale Research Letters, 12, 4.

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Synthesis of Colloidal Nanocrystals

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All
chemicals were used before and used as
purchased, without any further purification: InCl₃ (Sigma-Aldrich,
99.999% trace metal basis), ZnCl₂ (Sigma-Aldrich, 99.999%
trace metal basis), oleylamine (OAm, Acros, 80–90% grade),
tris(diethylamino)phosphine ((DEA)₃P, Sigma-Aldrich,
97%), sulfur powder (Sigma-Aldrich, ≥99.0%), trioctylphosphine
(TOP, Sigma-Aldrich, 97%), zinc stearate (ZnSt₂ Sigma-Aldrich,
technical grade), 1-octadecence (ODE, Alfa Aesar, 90%), R5011 and
S5011 (Henan Tianfu Chemical, 99%). All reagents and solvents used
in L, OIM, and P-8-OPIMB synthesis were obtained from Sigma-Aldrich.

Parzyszek S., Tessarolo J., Pedrazo-Tardajos A., Ortuño A.M., Bagiński M., Bals S., Clever G.H, & Lewandowski W. (2022). Tunable Circularly Polarized Luminescence via Chirality Induction and Energy Transfer from Organic Films to Semiconductor Nanocrystals. ACS Nano, 16(11), 18472-18482.

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Synthesis of Colloidal Metal Nanoparticles

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The materials used were oleylamine (OLA,
Sigma-Aldrich, 70%), octadecylamine (ODA, Sigma-Aldrich, ≥99.0%),
hexadecylamine (HDA, Sigma-Aldrich, 98%), dodecylamine (DDA, Sigma-Aldrich,
≥99.0%), octylamine (Sigma-Aldrich, 97%), toluene (anhydrous,
Sigma-Aldrich, 99.8%), tris(dimethylamido)antimony(III) (Sb[NMe₂]₃, Sigma-Aldrich, 99.99%), indium(III)chloride
(InCl₃, Sigma-Aldrich, 98%), lithium triethylborohydride
(LiEt₃BH, Super-Hydride, Sigma-Aldrich, 1 M in tetrahydrofuran,
THF), dioctyl ether (DOE, Alfa Aesar, 99%), 1-butanol (anhydrous,
Sigma-Aldrich, 99.8%), methanol (anhydrous, Sigma-Aldrich, 99.8%),
methyl acetate (MeOAc, anhydrous, Sigma-Aldrich, 99.5%), and oleic
acid (Sigma-Aldrich, 90%). All chemicals were used as received except
for oleylamine and oleic acid, which were degassed before use. The
degassing was performed at 100 °C under reduced pressure (∼1
mbar) for 4 h.

Busatto S., Ruiter M.D., Jastrzebski J.T., Albrecht W., Pinchetti V., Brovelli S., Bals S., Moret M.E, & de Mello Donega C. (2020). Luminescent Colloidal InSb Quantum Dots from In Situ Generated Single-Source Precursor. ACS Nano, 14(10), 13146-13160.

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Synthesis of Semiconductor Nanocrystals

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Polyacrylonitrile (PAN, M_w = 150 000) was purchased from Sigma Aldrich (USA). N,N-Dimethylformamide (DMF) was purchased from Sigma Aldrich (USA). CdO (99.9%), oleic acid (OA, 90%), 1-octadecene (1-ODE, 90%), trioctylphosphine (TOP, 97%), and Se powder (99.99%) were purchased from Sigma Aldrich. PbO (99.99%), bis(trimethylsilyl)sulfide ((TMS)₂S, synthesis grade), InCl₃ (98%), ZnCl₂ (97%), oleylamine (70%), tris(dimethylamino)phosphine (P(DMA)₃, 97%), 1-dodecanethiol (DDT, 98%), CuI (99.999%), indium acetate (99.99%), zinc acetate (99.99%), sulfur (99.998%), zinc diethyldithiocarbamate (Zn DDTC, 97%), cadmium acetate (99.995%), ZnO (99.999%), sodium sulfide nonahydrate (98+%), and sodium sulfite (≥98%) were purchased from Sigma Aldrich.

Song T., Cheong J.Y., Choi J.Y., Park C., Lee C., Lee C., Lee H.M., Choi S.Y., Song H., Kim I.D, & Jeon D.Y. (2019). A feasible strategy to prepare quantum dot-incorporated carbon nanofibers as free-standing platforms. Nanoscale Advances, 1(10), 3948-3956.

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Synthesis of In-Cd-S Nanoparticle Precursors

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Three stock solutions
were prepared by dissolving 0.1 M InCl₃ (Sigma-Aldrich),
0.1 M Cd(CH₃COO)₂ (Fisher), and 0.2 M CH₄N₂S (Showa) in water–glycerol (3:1) solutions.
The In–Cd–S mixed precursors were prepared by mixing
InCl₃, Cd(CH₃COO)₂ and CH₄N₂S solutions in a volume ratio of 0.2:0.8:1. For the
screening test, 15 different metal salts solutions (0.1 M), VCl₂·xH₂O, Cr(NO₃)₃·9H₂O, Mn(NO₃)₂, Fe(NO₃)₃·9H₂O, Co(NO₃)₂·6H₂O, Ni(NO₃)₂·6H₂O, CuSO₄·5H₂O, Zn(NO₃)₂·6H₂O, (NH₄)₆Mo₇O₂₄·4H₂O, RuCl₃·xH₂O, AgNO₃, (NH₄)₆W₁₂O₃₉, IrCl₄, and TeCl₄ were prepared in water–glycerol (3:1) solutions. All
chemicals were of reagent grade and used as received.

Weng Y.C., Su Y.W, & Chiu K.C. (2019). Characterization and Optimization of Silver-Modified In0.2Cd0.8S-Based Photocatalysts. ACS Omega, 4(25), 21214-21222.

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