Anhydrous solvents

Manufactured by Thermo Fisher Scientific

Sourced in Austria

Anhydrous solvents are purified organic solvents that contain minimal or no water content. They are designed to provide a controlled, dry environment for sensitive applications in research and industrial settings.

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Lab products found in correlation

Paraformaldehyde (pfa), by Thermo Fisher Scientific (1 mentions) Diethyl malonate, by Merck Group (1 mentions) Sodium metal, by Merck Group (1 mentions) Potassium persulfate, by Merck Group (1 mentions) Triethyl orthoformate, by Merck Group (1 mentions) Ethyl cyanoacetate, by Merck Group (1 mentions) Lithium aluminum hydride solution, by Merck Group (1 mentions) Urea 15n2, by Merck Group (1 mentions) N tert butyldimethylsilyl n methyltrifluoroacetamide, by Thermo Fisher Scientific (1 mentions) Reagent grade solvents, by Thermo Fisher Scientific (1 mentions) 15n2 uracil, by Eurisotop (1 mentions) Triethylamine, by Merck Group (1 mentions) Silver nitrate, by Merck Group (1 mentions) Sunitinib, by LC Laboratories (1 mentions) Cesium iodide, by Thermo Fisher Scientific (1 mentions) Poly triaryl amine ptaa, by Merck Group (1 mentions) Organic halide salts, by Greatcell Solar (1 mentions) Nanobret 590 se, by Promega (1 mentions) Nanobret nano glo detection system, by Promega (1 mentions) 60f254 silica gel, by Merck Group (1 mentions)

6 protocols using anhydrous solvents

Isotopic Labeling of Biomolecules

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Triethyl orthoformate, ethyl cyanoacetate, diethyl malonate, sodium metal, lithium aluminum hydride solution, triethylamine, potassium persulfate, silver nitrate, and ¹⁵N₂-urea were obtained from Sigma-Aldrich (St. Louis, MO). Potassium perruthenate, paraformaldehyde, N-tert-butyldimethylsilyl-N-methyltrifluoroacetamide + 1% tert-butyldimetheylchlorosilane (MTBSTFA + 1% TBDMCS), reagent grade solvents, and anhydrous solvents were purchased from Fisher Scientific (Pittsburgh, PA). ¹⁵N₂-Orotic acid, ²H₄-thymine, DMSO-d₆, and methanol-d₄ were purchased from Cambridge Isotope Laboratory (Cambridge, MA). ²H₄-5-methylcytosine and ²H₂-cytosine were obtained from CDN Isotopes (Quebec, Canada). ¹⁵N₂-uracil was purchased from Euriso-top (Saint-Aubin, France).

Patel J.P., Sowers M.L., Herring J.L., Theruvathu J.A., Emmett M.R., Hawkins B.E., Zhang K., DeWitt D.S., Prough D.S, & Sowers L.C. (2015). Measurement of Postreplicative DNA Metabolism and Damage in the Rodent Brain. Chemical research in toxicology, 28(12), 2352-2363.

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Synthesis of Sunitinib Analogs

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All solvents and reagents were obtained from commercial suppliers and used without further purification. Anhydrous solvents were bought from Fisher Scientific GmbH (Austria) over molecular sieves. Sunitinib was purchased from LC Laboratories®, N^ϵ‐allyloxycarbonyl‐l‐lysine from Chem‐Impex International, Inc., and morpholin‐4‐yl‐acetic acid from Activate Scientific GmbH.

Karnthaler‐Benbakka C., Koblmüller B., Mathuber M., Holste K., Berger W., Heffeter P., Kowol C.R, & Keppler B.K. (2018). Synthesis, Characterization and in vitro Studies of a Cathepsin B‐Cleavable Prodrug of the VEGFR Inhibitor Sunitinib. Chemistry & Biodiversity, 16(1), e1800520.

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Synthesis of Substituted Pyridines

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4-amino-3-hydroxypyridine and 4-amino-3-methoxypyridine were purchased from Astatech (cat# 22383 and 35474). Anhydrous solvents were purchased from Acros Organics. All other chemicals were purchased from Sigma.

Guehl N.J., Neelamegam R., Zhou Y.P., Moon S.H., Dhaynaut M., Fakhri G.E., Normandin M.D, & Brugarolas P. (2021). Radiochemical synthesis and evaluation in nonhuman primates of 3-[11C]methoxy-4-aminopyridine: a novel PET tracer for Imaging Potassium Channels in the CNS. ACS chemical neuroscience, 12(4), 756-765.

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Perovskite Solar Cell Fabrication

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Unless otherwise stated, all materials were purchased from Sigma-Aldrich or Alfa Aesar and used as received. Perovskite films and devices were fabricated using PbI₂ and PbBr₂ (99.99% purity) purchased from TCI, organic halide salts were purchased from GreatCell Solar, and cesium iodide (99.99% purity) was purchased from Alfa Aesar. The poly(triaryl amine) (PTAA) was purchased from Sigma-Aldrich. The PC₆₁BM was purchased from Solenne. The bathocuproine (BCP; sublimed grade, 99.99% purity) was purchased from Sigma-Aldrich. All the anhydrous solvents were purchased from Acros Organics.

Degani M., An Q., Albaladejo-Siguan M., Hofstetter Y.J., Cho C., Paulus F., Grancini G, & Vaynzof Y. (2021). 23.7% Efficient inverted perovskite solar cells by dual interfacial modification. Science Advances, 7(49), eabj7930.

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Sourcing of Organic Reagents and Solvents

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All organic reagents were used as received from Sigma-Aldrich (St. Louis, Missouri, USA), Acros Organics (Geel, Belgium) and Fluka (Buchs, Switzerland). Solvents were purchased from Acros Organics, Pro-Labo (Tokyo, Japan), Fluka, and Sigma-Aldrich. Anhydrous solvents were obtained from Acros Organics.

Dressler A., Leydier A, & Grandjean A. (2022). Effects of Impregnated Amidophosphonate Ligand Concentration on the Uranium Extraction Behavior of Mesoporous Silica. Molecules, 27(14), 4342.

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NanoBRET Assay for CBH-001 Evaluation

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All solvents were purchased of HPLC grade from commercial suppliers (Sigma, Thermo Fisher) and used without further purification. Anhydrous solvents were purchased from Acros Organics and stored under a nitrogen atmosphere with activated molecular sieves. CBH-001 was purchased from Enamine. NanoBRET 590 SE, NanoBRET™ Nano-Glo® Detection System and CellTiter-Glo® Luminescent Cell Viability Assay was purchased from Promega.
Reaction progress was monitored by TLC (Thin Layer Chromatography) and LC-MS. For the silica gel TLC, aluminium plates coated with 0.25 mm 60F254 silica gel (Merck) were used and visualized with UV light at l = 254 nm or l = 365 nm.
1H NMR spectra were recorded using a Bruker Avance 400 MHz spectrometer (400 MHz) and the deuterated solvent stated. Chemical shifts (δ) are quoted in parts per million (ppm) and referenced to the residual solvent peak. Multiplicities are denoted as singlet (s), doublet (d), triplet (t), quartet (q) and quintet (p) and derivatives thereof and multiplets (m). (br) denotes a broad resonance peak.
Coupling constants are recorded as Hz and rounded to the nearest 0.1 Hz. Spectra were analysed using MestreNova 14. Compound names were generated using ChemBioDraw Ultra v19.0 systematic naming.

Rothweiler E.M., Stefaniak J., Ward J., Rogers C., Balıkçı E., & Huber K. (2022). A chemical biology toolbox to investigate in-cell target engagement and specificity of PRMT5-inhibitors.

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