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4 protocols using hexyl salicylate

1

Retention Index Determination of Volatile Compounds

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A mixture of n-alkanes (C8—C20) dissolved in hexane for retention index determination was purchased from Fluka (Buchs, Switzerland). Reference compounds, (E)-2-hexen-1-ol (> 96%), (E)-2-octen-1-ol (> 97%), 1-decyne (> 98%), 1-dodecene (≥ 99%), (E,E)-2,4-hexadienal (≥ 97%), 2-cyclohexen-1-ol (> 95%), (E)-2-hexenal (≥ 99%), (E)-2-octenal (≥ 95%), 4-tert-butylcyclohexyl acetate (mixture of E and Z, > 98%), allyl cyclohexanepropionate (≥ 98%), cyclopentanemethanol (≥ 98%), cyclopentanol (≥ 99%), cyclopentanone (≥ 99%), decanal (≥ 98%), 1-dodecanol (≥ 98%), dodecyl acetate (> 97%), hexyl acetate (≥ 99%), hexyl salicylate (≥ 99%), limonene (> 97%), nonanal (≥ 97%), octyl acetate (≥ 99%), p-cymene (> 99%), 1-tridecanol (≥ 99%), and α-hexylcinnamaldehyde (≥ 95%) were supplied by Sigma Aldrich (Munich, Germany).
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2

Gum Arabic and Fungal Chitosan Biomaterials

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Gum Arabic and fungal chitosan (fCh; deacetylation degree 79%, molecular weight ~150 kDa) were purchased from Nexira Food (Rouen Cedex, France, EU) and Kitozyme (Herstal, Belgium, EU), respectively. Analytical grade chemicals being hexylsalicylate (HS; 1.04 g·mL−1), sorbitan triolate (Span85), triethanolamine (TEA), aqueous glutaraldehyde (GLT; 50% w/w), fuming hydrochloric acid (HCl; 36% w/v), LR white acrylic resin were bought from Sigma-Aldrich (Gillingham, Dorset, UK), stored according to the safety data sheet (SDS) instructions, and used without any additional purification. All admixtures were prepared with demineralised water (18.2 MΩ·cm at 25 °C).
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3

Identification of Volatile Compounds

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Analytical standards were used for the identification of hexyl salicylate (supplied by Sigma-Aldrich), α-isomethylionone (supplied by Sigma-Aldrich), and β-ionone (supplied by Supelco). The rest of the specific compounds studied in this research were identified by comparing their mass spectrum with the NIST database, for which NIST MS search 2.0 software was used.
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4

Synthesis of PMMA-CTAB Nanoparticles

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Poly(methyl methacrylate) (PMMA) (120 kDa), cetyltrimethylammonium bromide (CTAB) 98%, dichloromethane (DCM) >99%, poly(vinyl pyrrolidone) (PVP) (40 kDa), chloroplatinic acid (H2PtCl6) 99%, chloroauric acid (HAuCl4) 99.99%, 30% hydrogen peroxide, hexyl salicylate 99%, and sodium borohydride, 98%, were obtained from Sigma-Aldrich and used as received. All solutions were prepared using ultrapure Milli-Q water (resistivity of ~18 M .cm -1 ).
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