Jsm 7800f

Structural analyses were conducted using a JEOL scanning electron microscope (SEM) (model JSM-7800F, JEOL Ltd., Tokyo, Japan). The JEOL JSM-7800F microscope is a high-resolution scanning electron microscope equipped with four detectors: upper electron detector (UED), lower electron detector (LED), backscatter electron detector (BED), and transmission electron detector (TED).
A small amount of the analyzed carbon nanotubes was dispersed in isopropyl alcohol, then the suspension prepared using this method was spotted onto a so-called grid and left under clean conditions to dry. After complete drying, the grid was placed in a holder in the chamber of the microscope. The analysis was performed using the TED detector.

After the laser cladding process, AlCoCr_xCuFe HECs specimens were sectioned into 10 mm × 10 mm × 10 mm pieces perpendicular to the laser cladding path. The cross section of the specimens was ground with 2000 grit sandpaper, polished to a scratch free mirror surface, and subjected to 10% oxalic acid (beilianchem, 99.5%) solution electrolytic corrosion for 30 s. Specimens after oxalic acid electrolytic corrosion surfaces were observed using a scanning electron microscope (SEM) (JEOL JSM-7800F, Tokyo, Japan) with energy dispersive spectroscopy (EDS) (JEOL JSM-7800F, Tokyo, Japan). X-ray diffraction (XRD) (Bruker D8 Advance, Billerica, MA, USA) was used to analyze the phase structure of HECs at a scanning speed of 4° min⁻¹, ranging from 20° to 100°. The nanoindentation characteristics of the AlCoCr_xCuFe HECs were studied by a nanoindentation tester (Keysight Nanoindenter G200, Santa Rosa, CA, USA). The measurements were carried out using a Berkovich indenter with the load of 300 mN and loading time of 25 s. Nanoindentation tests were performed for each sample five times.

The morphology and size of the Au NPs in water solution were analyzed by transmission electron microscopy (TEM) using a FEI Titan 80–300 electron microscope (Hillsboro, OR, USA) with an accelerating voltage of 300 kV. Tissue was analyzed by a Scanning Electron Microscope (SEM) JEOL JSM-7800F (Tokyo, Japan) and by a SEM-Energy Dispersive X-ray Spectrometer (EDS) from Oxford Instruments (Abingdon, UK). UV-Vis absorption measurements were carried out using a Perkin Elmer Lamda 900 spectrometer (Waltham, MA, USA) with a spectral resolution of 2 nm. Optical characterization of cervix tissue was obtained by a Zeiss confocal microscope, model LSM-710-NLO, equipped with a Chameleon Vision-II ultrafast laser system from Coherent (tunable from 680 to 1040 nm, 140 fs, 80 MHz repetition rate). The excitation wavelength used for confocal images was 543 nm and 900 nm for TPI.
The SERS spectra were acquired using an inVia Raman microscope from Renishaw with a 20×/0.4 objective and approximately 5 mW of excitation power at 785 nm wavelength. The integration time for each Raman spectrum was 20 s and the spectral range was from 700 to 1700 cm⁻¹. The Raman data was obtained by mapping a minimum of 10 independent tissue regions in each sample, depending on the quality of each slide, each site was measured twice. The results represent the average of all the mapped regions for each sample.