EHA (99%), HEA (95%), DEGDA, and TEGDA were purchased from TCI (Tokyo, Japan). (3-mercaptopropyl)trimethoxysilane (MPTMS; 95%) was purchased from Sigma–Aldrich (St. Louis, MO, USA), and hexylamine (HA; 99%) was purchased from Acros Organics. Irgacure 184, which is a photoinitiator, was purchased and used by Shinyoung Radchem. 1-dodecanethiol (98%), which is a chain-transfer agent, was purchased from Alfa Aesar. All materials were used without purification.
1 dodecanethiol
Manufactured by Thermo Fisher Scientific
Sourced in United States
1-dodecanethiol is a chemical compound with the formula CH3(CH2)11SH. It is a colorless liquid with a characteristic odor. 1-dodecanethiol is primarily used as a chemical reagent in various laboratory applications.
Automatically generated - may contain errors
Lab products found in correlation
Dulbecco modified eagle medium (dmem), by Thermo Fisher Scientific (2 mentions)
3 mercaptopropyl trimethoxysilane mptms, by Merck Group (1 mentions)
Tetraethyl orthosilicate, by Thermo Fisher Scientific (1 mentions)
Ferric chloride hexahydrate, by Merck Group (1 mentions)
Ferrous chloride tetrahydrate, by Merck Group (1 mentions)
Benzyl ether, by Merck Group (1 mentions)
Zinc chloride, by Merck Group (1 mentions)
Zinc acetate, by Thermo Fisher Scientific (1 mentions)
Dodecylamine, by Thermo Fisher Scientific (1 mentions)
Indium acetate, by Thermo Fisher Scientific (1 mentions)
3 mercaptopropyl trimethoxysilane, by Thermo Fisher Scientific (1 mentions)
Iron 3 acetylacetonate, by Thermo Fisher Scientific (1 mentions)
Copper 1 iodide, by Thermo Fisher Scientific (1 mentions)
Dextran dx, by Merck Group (1 mentions)
Polyethyleneimine pei, by Thermo Fisher Scientific (1 mentions)
Oleylamine ola, by Merck Group (1 mentions)
Silver nitrate, by Merck Group (1 mentions)
Ethanol, by Echo Medical Systems (1 mentions)
Silver nitrate agno3, by Resonac (1 mentions)
Tetrahydrofuran thf, by Tedia (1 mentions)
8 protocols using 1 dodecanethiol
1
Synthesis of Photopolymer Coatings
2
Synthesis of Multifunctional Nanoparticles
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Ferric chloride hexahydrate (99%), ferrous chloride tetrahydrate (99%), dextran (DX) (M.w. 20,000), zinc chloride (99%), silver nitrate (99.8%), oleylamine (OLA) (70%), benzyl ether (98%), octylphenyl-polyethylene glycol (IGEPAL CA-630), poly(isobutylene-alt-maleic andydride) (PBMA) were purchased from Sigma-Aldrich. Glutathione (GSH) (98%), tetramethylammonium hydroxide (TMAH) (25% solution in methanol), iron(III) acetylacetonate (99%), myristic acid (MA) (99.5%) were purchased from Acros Organics; sodium diethyldithiocarbamate (98%), indium acetate (99.99%), polyethyleneimine (PEI) (99%, M.w. 10,000), zinc acetate (99.98%), copper(I) iodide (99.998%), tetraethylorthosilicate (TEOS) (99%), 3-mercaptopropyltrimethoxysilane (MPTMS) (97%), 1-dodecanethiol (DDT) (98%), dodecylamine (DDA) (98%) were purchased from Alfa Aesar, 3-glycidyloxypropyl-trimethoxysilane (GOPTS) (95%) was from TCI America. All chemical and organic solvents were obtained commercially as analytical-graded materials without further purification.
3
Synthesis and Characterization of Nanoparticles
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Hexadecyltrimethylammonium bromide (CTAB), ascorbic acid, triethylamine (TEA), and HSA were purchased from Sigma-Aldrich Co. (St Louis, MO, USA). 1-Dodecanethiol was purchased from Alfa Aesar (Ward Hill, MA, USA). Silver nitrate (AgNO3) and hydrogen tetrachloroaurate (III) tetrahydrate (HAuCl4⋅4H2O) and trisodium citrate were purchased from Showa (Tokyo, Japan). PLGA (molecular weight [MW]=40,000) was purchased from Green Square (Taipei, Taiwan, Republic of China). Polyvinyl alcohol (PVA) (MW=16,000) was purchased from Acros. Sodium tetrahydridoborate (NaBH4) was purchased from Fluka. DOX was purchased from Seedchem. Dithiothreitol, MTT, and ampicillin were purchased from MDBio, Inc. (Taipei, Taiwan, Republic of China). Ethanol was purchased from Echo. Tetrahydrofuran (THF) was purchased from Tedia. Chloroform (CHCl3) was purchased from J.T. Baker. DMEM and Dulbecco’s phosphate-buffered saline (DPBS) were purchased from Thermo Fisher Scientific (Waltham, MA, USA). Penicillin–streptomycin (P/S) and FBS were purchased from HyClone (Logan, UT, USA).
4
Hydrophobic Acrylic PSA Synthesis
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2-Ethylhexyl acrylate (EHA, 98%), isobornyl acrylate (IBOA), 2-hydroxyethyl acrylate (HEA, 96%), PVA, HA, and isophorone diisocyanate (IPDI, 98%) were purchased from Sigma Aldrich (Seoul, Korea). Irgacure 184 and darocur TPO (photoinitiators) were purchased from Shinyoung Rad Chem (Seoul, Korea). 1-dodecanethiol (98%), a chain transfer agent, was purchased from Alfa Aesar. SA3000, a commercial acrylic PSA with hydrophobicity (Mw: 700,000–800,000 g/mol, contact angle: 95.19°), was purchased from Samwha Co., (Seoul, Korea) All materials were used without further purification.
5
Thiol Functionalization of NPG Samples
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Some NPG samples were functionalized by a method adapted from Hakamada et al. [22 (link)]. In summary, samples were immersed in a 10 mM thiol solution for 3 h. After immersion samples were thrice rinsed with ethanol and allowed to dry overnight. 10 mM thiol solutions were prepared from 1-dodecanethiol (Alfa Aesar) and ethanol.
6
Synthesis of Colloidal Nanocrystals
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All chemicals were acquired and used without further purification. 1-dodecanethiol (Alfa Aesar, 98%), trioctylphosphine (Sigma-Aldrich, 97%), 1-octadecene (Acros Organics, 90%), Oleic acid (for Figure 1 experiment: Sigma Aldrich >99%; otherwise: Alfa Aesar, 90%), Indium (III) Acetate (Alfa Aesar, 99.99% metals basis), Copper (I) Iodide (Aldrich, 98%), Zinc Acetate Dihydrate (Sigma-Aldrich, >99%), Diethyl Zinc (Beantown Chemicals, 96%). Caution: Diethyl zinc is extremely pyrophoric and must be handled under an inert atmosphere.
7
Synthesis of Alkylated Gold Nanoparticles
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The following reagents were obtained from
the indicated suppliers and used as received: tetra-n-octylammonium bromide (98%), 1-dodecanethiol (98%), and sodium borohydride
(98%) were obtained from ACROS. 1-Bromododecane (97%) was obtained
from Sigma-Aldrich. Potassium hexachloroiridate(IV) (39.8% Ir) was
obtained from Alfa Aesar. Sodium thiosulfate pentahydrate (Na2S2O3·5H2O) along with
solvents such as toluene, acetone, ethanol, and methanol was purchased
from Fisher Scientific. Chloroform-d was obtained
from Cambridge Isotope Laboratories. Sodium S-dodecylthiosulfate
was synthesized using the published procedure.11 ,18 Water was purified by using a Barnstead Nanopure Diamond ion exchange
resins purification unit.
the indicated suppliers and used as received: tetra-n-octylammonium bromide (98%), 1-dodecanethiol (98%), and sodium borohydride
(98%) were obtained from ACROS. 1-Bromododecane (97%) was obtained
from Sigma-Aldrich. Potassium hexachloroiridate(IV) (39.8% Ir) was
obtained from Alfa Aesar. Sodium thiosulfate pentahydrate (Na2S2O3·5H2O) along with
solvents such as toluene, acetone, ethanol, and methanol was purchased
from Fisher Scientific. Chloroform-d was obtained
from Cambridge Isotope Laboratories. Sodium S-dodecylthiosulfate
was synthesized using the published procedure.11 ,18 Water was purified by using a Barnstead Nanopure Diamond ion exchange
resins purification unit.
8
Synthesis and Characterization of Inorganic Nanoparticles
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Acetone (≥99.5%, Sigma-Aldrich), ammonium persulfate (≥98.0% Sigma-Aldrich), chlorobenzene (99.9%, Sigma-Aldrich), didodecyldimethylammonium bromide (98.0%, Sigma-Aldrich), 1-dodecanethiol (98.0%, ACROS Organics), 1,2-ethanedithiol (≥98.0%, Sigma-Aldrich), hydrochloric acid (37.0%, VWR Chemicals), mercury(ii ) chloride (≥99.5%, Sigma-Aldrich), methanol (≥99.9%, Sigma-Aldrich), methyl-iso-butyl ketone (MIBK; 99.8%, VWR Chemicals), oleylamine (>95.0%, Strem Chemicals), tellurium (99.999%, Sigma-Aldrich), anhydrous tetrachloroethylene (≥99.0%, Sigma-Aldrich), tri-n-octylphosphine (97.0%, STREM), 50 K PMMA (4.0% in anisole, Allresist), 950 K PMMA (4.5% in anisole, Allresist) and 2-propanol (≥99.8%, Sigma-Aldrich).
All the chemicals were used as received, unless otherwise stated. oleylamine was dried and degassed under reduced pressure at a temperature of 120 °C for 1 h before its use.
Trioctylphosphine telluride (TOP:Te) was synthesized by stirring 5.08 g tellurium (0.04 mol) in dry trioctylphosphine (20 ml) for three days yielding a 2 M TOP:Te solution. The solution was filtered through a 0.45 μm polytetrafluoroethylene syringe filter resulting in a clear, yellowish solution.
Cleanroom: 21.5 °C; 45–50% relative humidity; particle class, 10–10,000; >18 MΩ cm purified water.
All the chemicals were used as received, unless otherwise stated. oleylamine was dried and degassed under reduced pressure at a temperature of 120 °C for 1 h before its use.
Trioctylphosphine telluride (TOP:Te) was synthesized by stirring 5.08 g tellurium (0.04 mol) in dry trioctylphosphine (20 ml) for three days yielding a 2 M TOP:Te solution. The solution was filtered through a 0.45 μm polytetrafluoroethylene syringe filter resulting in a clear, yellowish solution.
Cleanroom: 21.5 °C; 45–50% relative humidity; particle class, 10–10,000; >18 MΩ cm purified water.
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