The bulk carbon and oxygen levels of both the powder and sintered compacts were determined using LECO TC-600 and LECO CS-844 instruments. The oxygen present in the sample reacted with the crucible, forming CO and CO2. The amounts of CO and CO2 were measured using infrared (IR) sensors and employed to estimate the amount of oxygen. To measure carbon, the sample was combusted in an induction furnace under the flow of oxygen. The amount of carbon in the sample was determined based on the CO and CO2 formed via reactions between the carbon in the sample and oxygen.
Tc 600
Manufactured by Leco
Sourced in Germany
The TC-600 is a thermal conductivity detector (TCD) designed for gas chromatography (GC) analysis. It measures the thermal conductivity of the carrier gas and separated analytes to detect and quantify their presence in a sample. The TC-600 provides a reliable and consistent method for analyte detection and identification in GC applications.
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Lab products found in correlation
2 protocols using tc 600
1
Determining Bulk Carbon and Oxygen Levels
2
Comprehensive Sample Characterization Methods
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A set of different techniques were used for a comprehensive sample characterization covering density measurements following the Archimedes principle (Secura 225D-1S equipped with YDK 01, Sartorius Lab Instruments GmbH & Co KG, Göttingen, Germany) and metallographic preparation described in detail in [36 (link)]. With respect to the final carbon and oxygen content in the sintered part, a combustion analysis (CS600 and TC600, LECO Instruments GmbH, Mönchengladbach, Germany) was performed.
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