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5 protocols using acetylacetone

1

Vanadium Oxytripropoxide Synthesis

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The vanadium (V) oxytripropoxide (98%, Sigma Aldrich, Saint Louis, MO, USA), anhydrous ethyl alcohol (99.8%, POCH, Gliwice, Poland), anhydrous 2-propanol alcohol (99.5%, Sigma Aldrich, Darmstadt, Germany), acetylacetone (99%, Alfa Aesar, Kandel, Germany), and methylene blue (82%, Chempur, Piekary Slaskie, Poland) were used without further purification. MiliQ water (0.05 µS cm−1) was used in all experiments.
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2

Synthesis of Perovskite Thin Films via Solution Processing

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Indium nitrate hydrate (In(NO3)3·xH2O, 99.999%) powder, N,N-dimethylacetamide (DMAC, 99.5%) were purchased from Sigma-Aldrich. 2-methoxyethanol (2-ME, 99.3%), acetylacetone (AcAc, 99%) and ammonium hydroxide (NH3·H2O, 28%) were obtained from Alfa Aesar. Formamidinium iodide (FAI, >98.0%), Methylammonium iodide (MAI, >99.0%), Cesium iodide (CsI, >99.0%), Lead (II) iodide (PbI2, 99.99%), Methylammonium bromide (MABr, >99.0%) and Lead(II) bromide (PbBr2, 99.99%) were purchased from Tokyo Chemical Industry Co. Ltd (TCI). Temozolomide (DMSO, 99%), N,N-Dimethylformamide (DMF, 98%) and chlorobenzene (CB, 99.8%) were purchased from J&K Scientific. Dichloromethane (DCM) was obtained from Innochem Science & Technology Co., Ltd. Colorless polyimide (CPI) powder was from Zhejiang OCAs New Materials Co. Ltd. Silicon wafer with 100 nm thick SiO2 layer was obtained from Silicon Valley Microelectronics, Inc. Isopropyl alcohol (AR, 99.7%), acetone (AR, 99.5%) and hydrochloric acid (HCl; AR, 36–38%) were provided by China National Medicines Co. Ltd. (Shanghai, China). Poly(perfluoroalkyl vinyl ether) (CYTOP) was purchased from Asahi glass company (Japan) and consisted of CTL-809M (solute) and CT-Solv.180 (solvent). Polymethyl methacrylate (PMMA, 495 K A2) was purchased from Kayaku Advanced Materials.
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3

Synthesis of 64Cu-Incorporated Iron Oxide Nanoparticles

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To synthesize 64Cu-incorporated iron oxide (64Cu-IO) NPs, we purchased the reagents acetylacetone, sodium acetate, copper chloride, benzyl ether, iron acetylacetonate, lauric acid, dodecylamine, cyclohexane, ammonia hydroxide, and tetraethylorthosilicate from Alfa Aesar. In addition, reagents 1,2-hexadicanediol and igepal CO-520 were purchased from Sigma Aldrich (Burlington, MA, USA). 64Cu was supplied by Korea Institute of Radiological & Medical Sciences.
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4

Synthesis of Nanomaterials for Environmental Applications

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The following materials were used in the experiments: ethanol (EtOH, 99.7+%, Reanal, Budapest, Hungary), 2-propanol (99+%, Acros Organics, Geel, Belgium), purified distilled water (filtered with Millipore Simplicity 185 system to reach 18.2 MΩ cm), tetraethyl orthosilicate (TEOS, 99%, Merck, Budapest, Hungary), titanium (IV) butoxide (98%, Merck, Budapest, Hungary), titanium (IV) isopropoxide (98+%, Acros Organics, Geel, Belgium), hydrochloric acid (HCl, 37%, Reanal, Budapest, Hungary), nitric acid (HNO3, 65%, Lach-Ner, Bratislava, Slovakia), ammonia aqueous solution (NH3, 25%, Lach-Ner, Bratislava, Slovakia), acetylacetone (99+%, Acros Organics, Geel, Belgium), hexadecyltrimethylammonium bromide (CTAB, 99+%, Acros Organics, Geel, Belgium), Pluronic P123 (P123, average mol wt 40000, Sigma Aldrich, Budapest, Hungary), AgNO3 (99.8%, Lach-Ner, Bratislava, Slovakia), rhodamine 6G (R6G, 95%, Sigma Aldrich, Budapest, Hungary), methylene blue (MB, 95+%, Reanal, Budapest, Hungary) and methyl orange (MO, 95%, Acros Organics, Geel, Belgium) dyes. All materials were analytical grade and used without further purification.
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5

Fabrication of FTO-based Optoelectronic Devices

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The following materials
were used: FTO substrate (7 Ω sq–1), titanium(IV)
tetraisopropoxide (TTIP)—99 wt % (Acros Organics), acetylacetone—99
wt % (Acros Organics), ethanol—96.6 vol % (Estonian Spirit),
methanol—99.9 vol % (Sigma-Aldrich), antimony trichloride—99.99
wt % (Sigma-Aldrich), thiourea—99 wt % (Sigma-Aldrich), chlorobenzene—99.5
vol % (Sigma-Aldrich), poly(3-hexyl-thiophene-2,5-diyl) (P3HT)—100
kDa, >90% regioregular (Sigma-Aldrich), and materials related to
HTM
synthesis as mentioned in the S1. The materials
were used as received.
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