Advance 400 solids nmr spectrometer

Example 4

M2¹, M3², M4³ and M5⁵ were synthesized according to procedure reported in the literature [36-39]. M1 and other starting reagents were purchased from Aldrich and Alfa-Aesar, and used as received without further purification. Thermogravimetric analysis (TGA) data were collected on Mettle-Toledo TGA-DSC-1 with heating rate 10° C./min from 30° C. to 900° C. under N₂ atmosphere. Solid state nuclear magnetic resonance (NMR) data were collected on Bruker Advance-400 Solids NMR spectrometer. N₂ adsorption data were collected on a Micrometrics ASAP 2020 surface area and pore size analyzer.

Example 4

M2¹, M3², M4³ and M5⁵ were synthesized according to procedure reported in the literature [36-39]. M1 and other starting reagents were purchased from Aldrich and Alfa-Aesar, and used as received without further purification. Thermogravimetric analysis (TGA) data were collected on Mettle-Toledo TGA-DSC-1 with heating rate 10° C./min from 30° C. to 900° C. under N₂ atmosphere. Solid state nuclear magnetic resonance (NMR) data were collected on Bruker Advance-400 Solids NMR spectrometer. N₂ adsorption data were collected on a Micrometrics ASAP 2020 surface area and pore size analyzer.