Meta-aminophenol, para-aminophenol, 4-hydroxycoumarin, acetic acid, methanol, ethanol, toluene, acetone, dimethyl sulfoxide, potassium-tetrachloridopalladate(II), and phosphoryl chloride were obtained from Sigma-Aldrich, Germany.
Phosphoryl chloride
Manufactured by Merck Group
Sourced in Poland
Phosphoryl chloride is a colorless, fuming liquid chemical compound with the formula POCl3. It is commonly used as a reagent in organic synthesis and as a precursor for the production of other phosphorus-containing compounds.
Automatically generated - may contain errors
Lab products found in correlation
Sodium hydride, by Merck Group (2 mentions)
Crotonaldehyde, by Merck Group (2 mentions)
2 iso propylaniline, by Merck Group (2 mentions)
Silica gel 60, by Macherey-Nagel (2 mentions)
Ethanol, by Merck Group (2 mentions)
Para aminophenol, by Merck Group (1 mentions)
Dimethyl sulfoxide (dmso), by Merck Group (1 mentions)
4 hydroxycoumarin, by Merck Group (1 mentions)
Ferrous chloride tetrahydrate, by Merck Group (1 mentions)
α methylbenzylamine, by Merck Group (1 mentions)
Dl tartaric acid, by Merck Group (1 mentions)
R α methylbenzylamine, by Merck Group (1 mentions)
S α methylbenzylamine, by Merck Group (1 mentions)
3 aminopropyltrimethoxysilane, by Merck Group (1 mentions)
Methanol, by Merck Group (1 mentions)
Glycerol, by Merck Group (1 mentions)
Ammonium hydroxide, by Merck Group (1 mentions)
Ferric chloride hexahydrate, by Merck Group (1 mentions)
Triethylamine, by Merck Group (1 mentions)
Tetraethyl orthosilicate, by Merck Group (1 mentions)
4 protocols using phosphoryl chloride
1
Synthesis of Organic Compounds
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Meta-aminophenol, para-aminophenol, 4-hydroxycoumarin, acetic acid, methanol, ethanol, toluene, acetone, dimethyl sulfoxide, potassium-tetrachloridopalladate(II), and phosphoryl chloride were obtained from Sigma-Aldrich, Germany.
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Meta-aminophenol, para-aminophenol, 4-hydroxycoumarin, acetic acid, methanol, ethanol, toluene, acetone, dimethyl sulfoxide, potassium-tetrachloridopalladate(II), and phosphoryl chloride were obtained from Sigma-Aldrich, Germany.
2
Chiral Amines and Silica Nanoparticle Synthesis
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Phosphoryl chloride (POCl3, 99%), (R)-(+)-α-methylbenzylamine (RMBA, 98%), (S)-(−)-α-methylbenzylamine (SMBA, 98%) and (±)-α-methylbenzylamine (MBA, 98%) were bought from Sigma-Aldrich. Methanol, ethanol, tetrahydrofuran (THF), sodium chloride (NaCl), ferric chloride hexahydrate (FeCl3·6H2O), ferrous chloride tetrahydrate (FeCl2·4H2O), ammonium hydroxide (25% (w/w)), glycerol, tetraethyl orthosilicate (TEOS), 3-aminopropyltrimethoxysilane (APTMS), dl -tartaric acid (99%), dl -phenylalanine (99%), dl -valine (99%) and triethylamine (TEA, 99%) were purchased from Merck.
3
Synthesis of Heterocyclic Compounds
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All experiments were carried out in an atmosphere of dry argon, and flasks were flame dried. Solvents were dried by usual methods (diphenyl ether, diethyl ether, and THF over benzophenone ketyl, CHCl3, and CH2Cl2 over P4O10, hexane over sodium-potassium alloy) and distilled. Chromatographic purification was carried out on silica gel 60 (0.15–0.3 mm, Macherey-Nagel GmbH & Co. KG, Düren, Germany). Sodium hydride (dry, 95%), potassium tert-butoxide, trimethyl orthoformate, 2-iso-propylaniline, 2-(tert-butyl)aniline, 2-nitroaniline, phosphoryl chloride, 9H-carbazole, Meldrum’s acid, acrolein, and crotonaldehyde were purchased from Sigma-Aldrich (Poznań, Poland), and were used without further purification.
4
Reagent Preparation and Purification for Organic Synthesis
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All experiments were carried out in an atmosphere of dry argon, and flasks were flame dried. Solvents were dried by usual methods (diphenyl ether, diethyl ether, and THF over benzophenoneketyl, CHCl3, and CH2Cl2 over P4O10, hexane, and pyridine over sodium-potassium alloy) and distilled. Chromatographic purification was carried out on silica gel 60 (0.15–0.3 mm, Macherey-Nagel GmbH & Co. KG, Dueren, Germany). Crotonaldehyde, 4a,12a-dihydro-12H-benzo[5,6][1,4]thiazino[2,3-b]quinoxaline, N1,N1-dimethylbenzene-1,4-diamine, 2,2-dimethylpropane-1,3-diol, 10H-phenothiazine, phosphoryl chloride, 2-isopropylaniline, isoquinolin-5-amine, quinolin-5-amine, sodium hydride (dry, 95%), stannous chloride, silver carbonate on Celite and o-toluidine were purchased from Sigma–Aldrich (Poznań, Poland), and were used without further purification.
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