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2 protocols using dimethylformamide dmf

1

Chitosan-Based Composite Materials

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Ferrous sulfate, ammonium ferric (III) sulfate dodecahydrate ((FeSO4⋅7H2O; >99.0%) and (NH4)Fe(SO4)2⋅12H2O; >99.0%, respectively), epichlorohydrin (epi; >99.0%), chitosan (Degree of Acetylation (DA): greater than 75%) (CHI), sodium hydroxide pellets (>99.99% for pH adjustment), sodium ethoxide (C2H5ONa) solution (50%), thiourea (CH4N2S; 99%), diethyl malonate (C7H12O4; 99%), glutaraldehyde (C5H8O2; 25% in H2O) and potassium dichromate (K2Cr2O7) were supplied by Sigma Aldrich (Merck, Darmstadt, Germany). Acetone (99.9%) and dimethylformamide (DMF; 99.9%) were purchased from Chron Chemicals (Qionglai, China). Other chemicals were obtained from Prolabo (VWR, Avantor Group, Fontenay-sous-Bois, France), which are used without further purification.
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2

Synthesis and Characterization of Chitosan-Uranium Composites

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All chemicals used in this study were analytical grade. Epichlorohydrin (EPI), ferrous sulfate (FeSO4·7H2O), chitosan (Chit, degree of acetylation, DA: <25%), ammonium ferric (III) sulfate dodecahydrate ((NH4)Fe(SO4)2·12H2O), sodium hydroxide, phosphoric acid, Muller-Hinton agar (microbiological growth medium), and dimethylsulfoxide (DMSO) were purchased from Sigma Aldrich (Merck KGAa, Darmstadt, Germany). Uranyl nitrate hexahydrate (UO2(NO3)2·6H2O) was obtained from Spi Supplies (West Chester, PA, USA). Dimethylformamide (DMF) and acetone were purchased from Chron Chemicals (Qionglai, China). Guar gum (GG) was obtained from Alpha Chemika (Mumbai, Maharashtra, India). Urea was supplied by Chem Lab (Zedelgem, Belgium). Other chemicals are Prolabo products (VWR, Avantor, France) and they were used as received.
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