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6 protocols using dpo3034

1

Fabrication of Particle-Embedded Polymeric Microstructures via Dielectrophoresis

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The polymeric matrix is composed of 1,6-hexanediol diacrylate (HDDA) and photoinitiator (1173), and the monomer concentration of photoinitiator was fixed 0.2%. The PS particles (5 μm in diameter, purchased from Tianjin Saierqun Technology Co., Ltd.) were dispersed in deionized water. After the water was completely evaporated at 60 °C, the polymeric matrix was added to the reagent bottle containing PS particles, and ultrasonic vibration was carried out for 2 hours at room temperature to obtain a uniformly dispersed PS particles solution. After that, the solution was rapidly injected into the sealed chamber device. A sinusoidal AC signal (5 MHz, 20 Vpp), generated by a waveform generator (Unit UTG2062A), was applied to electrodes lines to create a non-uniform electric field. A digital phosphor oscilloscope (Tektronix DPO 3034) was used to confirm the generated waveform. The viscometer SCYN1301 was used to measure the kinematic viscosity of the solution. The DEP-induced behavior of the microparticles was observed using an optical microscope (IX71, Olympus Co., Japan) equipped with a digital CCD camera and a computer screen.
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2

Characterization of Ferroelectric P(VDF-TrFE) Films

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The zeta potential of the suspension was estimated from the electrophoretic mobility measured using a zeta potential analyzer (Otsuka Electronics, ELS-Z2). The surface morphology was observed by scanning electron microscopy (SEM, S-4800, Hitachi). The film thickness was measured by an Alpha-step 500 surface profilometer (Tencor instruments). The formation of the ferroelectric β-phase in P(VDF-TrFE) films was confirmed by X-ray diffraction (XRD) (Rigaku D/Max-2500) and Fourier transform infrared (FTIR) spectroscopy in the attenuated total reflection mode (Bruker, IFS66V/S & HYPERION 3000) with a scanning resolution of 2 cm−1. The polarization-electric field (P-E) hysteresis loop was measured using a virtual-ground technique using an RT66A test system (Precision, RT-66A) equipped with a high-voltage amplifier (Trek Inc.). The output voltage of the spring type energy harvesters was monitored by a digital oscilloscope (DPO3034, Tektronix, Inc.). Input resistance and capacitance at the probe tip were 10 MΩ and <8 pF, respectively.
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3

Characterization of Infrared Photodetector

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The detector chip was mounted in a ceramic LCC. Ultrasonically extruded, gold wires connected the gold contact pads on the chip to the LCC leads. The LCC was then mounted in a custom-designed, printed circuit board (PCB). For responsivity measurements, the detector was illuminated with a cavity blackbody radiator (Santa Barbara Infrared Inc.) at 1000 °C equipped with a mechanical chopper. The PCB was connected by way of triaxial cables to a low-noise current preamplifier (SR570, Stanford Research Systems) and lock-in amplifier (SR830, Stanford Research Systems). Data acquisition was computer-controlled using a custom written program. A Spectra-Physics Solstice femtosecond laser (1-kHz repetition rate, 90 fs pulse width, 800 nm) was used to pump a TOPAS optical parametric amplifier to produce a wavelength of 1550 nm with a pulse width of 150 fs and a repetition rate of 1 kHz. A pair of linear polarizers was used to control the laser power. The photocurrent was routed by way of triaxial cables to an SR570 current preamplifier and voltage amplifier (SR560, Stanford Research Systems) and then finally to a 300 MHz digitizing oscilloscope (Tektronix DPO3034). Electrical phase angle measurements were made using an Agilent E4980 LCR meter.
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4

Bending Activated Triboelectric Nanogenerator Characterization

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A liner motor was applied as the external force to drive the BD-TENG (operating distance, 50 mm; maximum speed, 1 m/s; acceleration, 1 m/s2; deceleration, 1 m/s2). The resulting applied strain (ε) on the BD-TENG was 0.04% ε=h2R where h is the thickness of BD-TENG and R is the bending radius. The Voc was measured by an oscilloscope (Tektronix DPO3034), and the Isc and the transferred charge were detected by an electrometer (Keithley 6517B).
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5

Characterization of Dark Current-Voltage in OPDs

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Dark current-voltage of OPDs was characterized with a semiconductor parameter analyzer (B1500 A, Agilent Technologies) inside an N2-filled glovebox. Spectrally resolved EQE was performed outside the glove box with measured samples kept in nitrogen atmosphere inside a holder. Light from the monochromator (Cornerstone™ 130) was chopped at 80 Hz, and the signal was read using a lock-in amplifier (EG & G 7265). Frequency measurements were conducted using a green light emitting diode (LED) modulated by a square pulse using AFG3252 Tektronix, waveform generator. The dynamic photocurrent response of the OPDs was recorded using a digital oscilloscope (DPO3034 Tektronix)29 (link).
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6

Characterizing PDMS Surface Modifications

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The chemical compositional
changes to the PDMS surface after N2 plasma treatment were
analyzed using X-ray photoelectron spectroscopy (XPS, ULVAC-PHI).
The sheet resistance of the Ag layer was measured using a four-point
probe (Napson Corporation, RT-70V). The crystallinity of the EM was
identified through X-ray diffraction (XRD) with Cu Kα radiation
(λ = 1.5418 Å) at 30 kV and 20 mA at a scan rate of 2°
min–1 from 5 to 40° (2θ). Field emission
scanning electron microscopy (FE-SEM, Hitachi S-5200) operating at
2 kV was employed to determine the morphology of the EM and Ag layers.
The surface roughnesses of the EMs were measured using an atomic force
microscope (Bruker, Dimension Edge). The output voltages and currents
from the bio-triboelectric devices were measured using an oscilloscope
(Tektronix, DPO 3034). The dynamic mechanical pressure was applied
using a magnetic shaker (Sinocera, Model JZK-20). The surface potential
was measured using an electrostatic field meter (AccuraxS050C1). The
dielectric constant was measured using a precision impedance analyzer
(Microtest 6632). The surface charge was measured using a Keithley
6517B system electrometer (impedance: >200 TΩ).
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