Terephthalic acid (H
2BDC, 99% purity), methyl sulfoxide-d6 (99.8% atom% D purity), cinnamyl alcohol (98% purity), 3-nitrobenzyl alcohol (>99% purity), 4-methylbenzyl alcohol (98% purity), and TEMPO (98% purity) were supplied by Beijing InnoChem Science & Technology Co., Ltd. CO
2 ( >99.95% purity), water, N
2 ( >99.95% purity), Ar (>99.999% purity), and O
2 (99.99% purity) were purchased from Beijing Analysis Instrument Factory. TEA (A. R. grade), ethanol (A. R. grade),
methanol (A. R. grade), DMF (A. R. grade),
acetonitrile (A. R. grade), Na
2CO
3 (A. R. grade), and NaHCO
3 (A. R. grade) were supplied by Beijing Chemical Works. CoCl
2·6H
2O (A. R. grade), Cu(NO
3)
2·3H
2O (A. R. grade), and NiCl
2·6H
2O (A. R. grade) were brought from China National Medicines Co., Ltd. 1,4-Naphthalenedicarboxylic acid (H
2NDC, 99% purity), 2-naphthalene
methanol (98% purity), 1-phenylethanol (97% purity), 1-(4-methoxyphenyl)ethanol (95% purity), and
furfuryl alcohol (98% purity) were purchased from J&K Scientific Co., Ltd. Benzyl alcohol was supplied by Alfa Aesar China Co., Ltd. All these materials were used directly without further purification.
Zhang F., Zhang J., Zhang B., Zheng L., Cheng X., Wan Q., Han B, & Zhang J. (2020). CO2 controls the oriented growth of metal-organic framework with highly accessible active sites. Nature Communications, 11, 1431.