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Methylammonium chloride macl

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Methylammonium chloride (MACl) is a chemical compound used in various laboratory applications. It serves as a precursor material in the synthesis of perovskite materials, which are of interest in the field of photovoltaics and other optoelectronic technologies. MACl provides the methylammonium component required for the formation of these perovskite structures.

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Lab products found in correlation

4 tert butylpyridine tbp, by Merck Group (2 mentions) Formamidinium iodide fai, by Greatcell Solar (2 mentions) Methylammonium bromide mabr, by Greatcell Solar (2 mentions) Dimethyl sulfoxide (dmso), by Merck Group (1 mentions) Acetonitrile, by Merck Group (1 mentions) Isopropanol, by Merck Group (1 mentions) N n dimethylformamide (dmf), by Merck Group (1 mentions) Chlorobenzene, by Merck Group (1 mentions) Nickel 2 acetate tetrahydrate, by Merck Group (1 mentions) Sodium dodecylbenzenesulfonate, by Merck Group (1 mentions) Spiro ometad, by Merck Group (1 mentions) Lithium bis trifluoromethanesulfonyl imide litfsi, by Merck Group (1 mentions) Litfsi, by Merck Group (1 mentions) Chlorobenzene cb, by Thermo Fisher Scientific (1 mentions) Isopropanol ipa, by Thermo Fisher Scientific (1 mentions) Dimethyl sulfoxide (dmso), by Thermo Fisher Scientific (1 mentions) Dimethylformamide dmf, by Thermo Fisher Scientific (1 mentions) Deionized water, by Merck Group (1 mentions) Methylammonium iodide mai, by Greatcell Solar (1 mentions) Copper bromide, by Merck Group (1 mentions)

3 protocols using methylammonium chloride macl

1

Fabrication of Perovskite Solar Cells

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All reagents and chemicals were purchased from commercial
suppliers
without further purification. Tin dioxide(IV) and 15% hydrocolloid
dispersion (SnO2) were purchased from Alfa Aesar. Nickel(II)
acetate tetrahydrate (Ni(OCOCH3)2·4H2O, 99.995% trace metals basis), PbI2, spiro-OMeTAD
(purity ≥99.8%), sodium dodecylbenzene sulfonate (SDBS), isopropanol
(IPA), N,N-dimethylformamide (DMF),
dimethyl sulfoxide (DMSO), chlorobenzene (CB), acetonitrile (ACN),
4-tert-butylpyridine (tBP), lithium bis(trifluoromethane
sulfonyl)imide (Li-TFSI), and FK 209 Co(III) TFSI salts were from
Sigma-Aldrich. Formamidinium iodide (FAI), methylammonium chloride
(MACl), and methylammonium bromide (MABr) were obtained from GreatCell
Solar.
Quy H.V, & Bark C.W. (2022). Ni-Doped SnO2 as an Electron Transport Layer by a Low-Temperature Process in Planar Perovskite Solar Cells. ACS Omega, 7(26), 22256-22262.
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2

Fabrication of Perovskite Solar Cells

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All chemicals were used as received without further purification. SnO2 15% in H2O colloidal dispersion (Alfa Aesar, Haverhill, MA, USA), deionized water (Sigma Aldrich, St. Louis, MI, USA), perovskite precursor: formamidinium iodide (FAI, 99.995%, GreatCell Solar, Queanbeyan, Australia), Methylammonium Iodide (MAI, 99.995% GreatCell Solar), methylammonium chloride (MACl, 98% GreatCell Solar), benzamidine hydrochloride (Ph-FACl, 99.95%, Sigma Aldrich), PbI2 (99.99%, TCI Japan, Tokyo, Japan), dimethylformamide (DMF, 99.8%, Acros, Geel, Belgium), dimethyl sulfoxide (DMSO, 99.9%, Acros), isopropanol (IPA, 99.5%, Acros Organics), X60 (99.8%, Dyen-amo, Stockholm, Sweden), 4-tert-butylpyridine (tBP, 96%, Sigma Aldrich), Li-bis(trifluoromethanesulfonyl) imide (Li-TFSI, 99.95%, Sigma Aldrich), Acetonitrile (ACN, 99.8%, Acros Organics), Chlorobenzene (CB, 99.8%, Acros Organics), 1-Ethyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide (EMIM-TFSI, 98%, TCI America, Portland, OR, USA), MoO3 (99.99%, J.K Lesker, Jefferson Hills, PA, USA), Ag (99.999%, J.K Lesker).
Tzoganakis N., Tsikritzis D., Chatzimanolis K., Zhuang X, & Kymakis E. (2023). A Low-Cost and Lithium-Free Hole Transport Layer for Efficient and Stable Normal Perovskite Solar Cells. Nanomaterials, 13(5), 883.
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3

Synthesis of Perovskite Nanocrystal Powders

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Perovskite Nanocrystals powder of MA2CuBr4, MA2CuCl4, MA2CuCl3.7Br0.3, and MA2CuCl3.34Br0.66 were synthesized from methanol solutions. The precursors methyl-ammonium chloride (MACl, 99.99%, GreatCell Solar), methyl-ammonium bromide (MABr, 99.99%, GreatCell Solar), CuCl2 (copper chloride, 99% Sigma-Aldrich) and CuBr2 (copper bromide, 99% Sigma-Aldrich). The chemicals were mixed in the desired stoichiometry. For example, to synthesize MA2CuCl3.7Br0.3, 0.134 g of CuCl2, 0.118 g of MACl, and 0.027 g of MABr were mixed in 100 mL of MeOH, stirred for 2 h at 70 ○ C, and left to crystallize for 48 hours in an ice bath (0 ○ C). The powder crystals product was recovered by a rotary evaporator followed by washing the product with diethyl ether and drying at 65 ○ C for 12 h in a vacuum. Finally, the products are stored in an argon-filled glove box. The appearance of perovskite crystal is presented in Figure S1, supporting information.
Gassara M., Hemasiri N.H., Kazim S., Costantino F., Naïli H, & Ahmad S. (2023). Uncovering the Role of Electronic Doping in Lead-free Perovskite (CH3 NH3 )2 CuCl4-x Brx and Solar Cells Fabrication. ChemSusChem, 16(11).
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