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14 protocols using chloroplatinic acid

1

Synthesizing PDMS-PEG Copolymer Surfaces

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1-Octene (98%), silica, and PEG-200 were purchased from Aladdin Industrial Corporation. PDMS-2000 were purchased from Alfa Aesar (China) Chemicals Co., Ltd. N, N-dimethylaniline (99%) and 1,1,1,3,5,5,5-heptamethyltrisiloxane (98%) were purchased from Tokyo Chemical Industrial Co., LTD. Hydrochloric acid, chloroplatinic acid, ethanol, and ammonium hydroxide were purchased from Sinopharm Chemical Reagent Co., Ltd. PDMS-PEG was purchased from Guangzhou Tinci Materials Technology Co., Ltd. The molecular weight of each block is 30,000 for PDMS and 545 for PEG-12. Ultrapure water purified by Milli-Q Advantage A10 was used.
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2

Synthesis of Oleylamine-Capped Nanoparticles

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Oleylamine (C18H37N) was purchased from J&K Scientific, Ltd. Oleic acid (C18H34O2, 90%) was purchased from Alfa Aesar. Chloroplatinic acid (H2PtCl6·6H2O), cobalt(ii) acetate tetrahydrate (Co(Ac)2·4H2O), formaldehyde (HCHO), ethanol (C2H5OH), hexane (C6H14) and n-butylamine (C4H11N) were purchased from Sinopharm Chemical Reagent Co., Ltd. All chemicals were of analytical reagent grade and directly used after purchase without further purification.
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3

Synthesis of Metal Nanoparticles

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Chloroauric acid tetrahydrate (HAuCl4·4H2O), chloroplatinic acid (H2PtCl4·6H2O), sodium borohydride (NaBH4), hydrazine hydrate, 4-nitrophenol (4-NP), and silver nitrate (AgNO3) were obtained from Sinopharm Chemical Reagent Co., Ltd.
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4

Synthesis and Characterization of Pt-Based Catalysts

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Carbon black (Black Pearls 2000, BP2000) was produced by America Cabot Corporation. Commercial Pt/C (TEC10E20E) was purchased from TANAKA. All others chemicals were commercially available from Sinopharm Chemical Reagent Co. Ltd., China, including chloroplatinic acid (H2PtCl6·6H2O), cobalt chloride hexahydrate (CoCl2·6H2O), copper chloride dehydrate (CuCl2·2H2O), cickel chloride hexahydrate (NiCl2·6H2O), ethanol, and isopropanol. All the chemicals were used as received without further purification. DI water (18.2 MΩ/cm) used in all experiments was prepared by passing through an ultra-pure purification system.
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5

Synthesis of Platinum Group Metal Catalysts

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Commercial carbon black supports, including XC-72R, KJ-300J, KJ-600J, and BP2000 were produced by America Cabot Corporation and Japan Ketjenblack Internation Corporation, respectively. 2,2’-bithiophene (98%) was purchased from J&K Scientific Ltd. All other chemicals were commercially available from Sinopharm Chemical Reagent Co. Ltd., China, including chloroplatinic acid (H2PtCl6·6H2O), ruthenium (III) chloride hydrate (RuCl3·H2O), rhodium (III) chloride hydrate (RhCl3·3H2O), and iridium (III) chloride hydrate (IrCl3·H2O). DI water (18.2 MΩ/cm) used in all experiments was prepared by passing through an ultra-pure purification system. All the chemicals were used as received without further purification.
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6

Synthesis of Bismuth Oxychloride Nanoparticles

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Commercial bismuth oxychloride (BiOCl) was purchased from Sigma-Aldrich. Ethanol, thiourea, chloroplatinic acid (H2PtCl6), sodium borohydride (NaBH4), ascorbic acid, and silver nitrate (AgNO3) were from Sinopharm Chemical Reagent Co., Ltd. All the reagents were analytically pure and used without further purification. Water used in the experiment was Millipore water prepared by a Milli-Q instrument.
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7

Synthesis of Nanocomposite Materials

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Chloroplatinic acid (H2PtCl6·6H2O, AR, Pt > 37.5%), copper nitrate (Cu(NO3)2·3H2O, AR, 99%), iron nitrate (Fe(NO3)3·9H2O, AR), methanal (CH2O, AR), potassium permanganate (KMnO4, ≥99.5%), sodium hydroxide (NaOH, ≥96%), and aqueous hydrogen peroxide solution (H2O2, AR, H2O2 being 30 wt%) were provided by Sinopharm Chemical Reagent Co, Ltd. Imidazolidinyl urea (C11H16N8O8, AR, 98%) was provided by Aladdin Reagent (Shanghai) Co, Ltd. Alumina (Al2O3) particles were provided by Yantai Henghui Chemical Co, Ltd. SiO2 (20–40 mesh) particles were provided by Qingdao Ocean Chemical. Activated carbon (20–40 mesh) was provided by FuJian Xinsen Carbon Co, Ltd. All chemicals were of analytical purity and used without further treatment. Deionized (DI) water was applied for the whole experiment.
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8

Synthesis of Organofunctional Siloxanes

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Octamethylcyclotetrasiloxane (99.9%), Tetramethyldisiloxane (99.0%) were purchased from Shenzhen Osbang New Material Co., Ltd. (Shenzhen, China). Glycidyl methacrylate (97.0%) was obtained from Aladdin Reagents (Shanghai, China) Co., Ltd. Other chemicals (Ethanol (99.0%), Toluene (99.5%), Sulfuric acid (98.5%) and Chloroplatinic acid (>99.9%)) were procured from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). In this synthesis experiment, all drugs were sampled as received unless otherwise without further purification.
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9

Synthesis and Characterization of Bismuth-Platinum Nanomaterials

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All of the reagents in this study were of analytical grade and used without further purification. Bismuth nitrate pentahydrate (Bi(NO3)3·5H2O), tri-sodium citrate (Na3C6H5O7) and chloroplatinic acid (H2PtCl6) were purchased from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). Distilled water was used for the whole experiments.
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10

Fabrication of Hydrophilic Porous Nylon Membranes

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Hydrophilic porous nylon membranes with the average pore size of 0.22, 0.45, 1, 8, and 10 μm were purchased from Haining Zhongli Filtering Equipment Factory, Ltd. Dodecane (>99.0%) was purchased from Shanghai Aladdin Bio-Chem Technology Co., Ltd. AKYPO RO 90 VG was provided by Kao Chemicals GmbH. DuPont Krytox GPL 100, 103, and 107 were purchased from MiDRIEr-Stephenson. Fe3O4 nanoparticles (diameter: 10 to 30 nm, 25% in H2O) were purchased from Macklin. Vinyl dimethicone and hydrogen silicone oil were purchased from Zhejiang Xinan Chemical Industrial Group Co., Ltd. Nile Red was purchased from Tianjin HEOWNS Bio-Chem Technology Co., Ltd. Chloroplatinic acid (analytical reagent grade [AR]), toluene (AR), and ethanol (AR) were purchased from Sinopharm Chemical Reagent Co., Ltd. Lipase from Candida rugosa was purchased from Sigma-Aldrich. A lipase activity assay kit was purchased from Beijing Boxbio Science & Technology Co., Ltd. Milli-Q deionized (DI) water with a resistivity of 18.2 MΩ·cm was used in all experiments.
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