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Agilent 6510 q tof apparatus

Manufactured by Agilent Technologies
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The Agilent 6510 Q-TOF is a high-resolution quadrupole time-of-flight mass spectrometer. It is designed to provide accurate mass measurements and detailed structural information for a wide range of analytes.

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Lab products found in correlation

Agilent 1260 infinity 2, by Agilent Technologies (5 mentions) Supelcosil lc si, by Merck Group (4 mentions) Amx 500, by Bruker (3 mentions) Avance 3 700 ft nmr, by Bruker (3 mentions) Synergi fusion rp, by Phenomenex (3 mentions) Ascentis rp amide, by Merck Group (3 mentions) 343 polarimeter, by PerkinElmer (3 mentions) Avance 3 700, by Bruker (1 mentions) Agilent 1100 apparatus, by Agilent Technologies (1 mentions)

6 protocols using agilent 6510 q tof apparatus

1

Analytical Characterization of Compounds

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Specific rotation, PerkinElmer 343 Polarimeter (PerkinElmer, Waltham, MA, USA); NMR, Bruker AMX 500 (Bruker BioSpin GmbH, Rheinstetten, Germany) (500.12/125.67 MHz (1Н/13C) spectrometer; Bruker AVANCE III-700 spectrometer at 700.13 MHz/176.04 MHz (1H/13C); ESI MS (positive and negative ion modes), Agilent 6510 Q-TOF apparatus (Agilent Technology, Santa Clara, CA, USA), sample concentration 0.01 mg/mL; HPLC, Agilent 1260 Infinity II with a differential refractometer (Agilent Technology, Santa Clara, CA, USA); columns Supelcosil LC-Si (4.6 × 150 mm, 5 µm) and Discovery HS F5-5 (10 × 250 mm, 5 µm) (Supelco, Bellefonte, PA, USA), Diasfer 110 C-8 (4.6 × 250 mm, 5 µm) (Biochemmack, Moscow, Russia).
Silchenko A.S., Avilov S.A., Andrijaschenko P.V., Popov R.S., Chingizova E.A., Grebnev B.B., Rasin A.B, & Kalinin V.I. (2022). The Isolation, Structure Elucidation and Bioactivity Study of Chilensosides A, A1, B, C, and D, Holostane Triterpene Di-, Tri- and Tetrasulfated Pentaosides from the Sea Cucumber Paracaudina chilensis (Caudinidae, Molpadida). Molecules, 27(21), 7655.
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2

Characterization of Organic Compounds

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Specific rotation, PerkinElmer 343 Polarimeter (PerkinElmer, Waltham, MA, USA); NMR, Bruker Avance III 700 Bruker FT-NMR (Bruker BioSpin GmbH, Rheinstetten, Germany) (700.00/176.03 MHz) (1H/13C) spectrometer; ESI MS (positive and negative ion modes), Agilent 6510 Q-TOF apparatus (Agilent Technology, Santa Clara, CA, USA), sample concentration 0.01 mg/mL; HPLC, Agilent 1260 Infinity II with a differential refractometer (Agilent Technology, Santa Clara, CA, USA); columns Supelcosil LC-Si (4.6 × 150 mm, 5 μm) and Ascentis RP-Amide (10 × 250 mm, 5 μm) (Supelco, Bellefonte, PA, USA), Phenomenex Synergi Fusion RP (10 × 250 mm, 5 μm) (Phenomenex, Torrance, CA, USA).
Silchenko A.S., Kalinovsky A.I., Avilov S.A., Andrijaschenko P.V., Popov R.S., Dmitrenok P.S., Chingizova E.A, & Kalinin V.I. (2021). Unusual Structures and Cytotoxicities of Chitonoidosides A, A1, B, C, D, and E, Six Triterpene Glycosides from the Far Eastern Sea Cucumber Psolus chitonoides. Marine Drugs, 19(8), 449.
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3

Spectroscopic Characterization of Samples

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We used for specific rotation a Perkin-Elmer 343 Polarimeter (Perkin-Elmer, Waltham, MA, USA); for NMR, a Bruker Avance III 700 Bruker FT-NMR (Bruker BioSpin GmbH, Rheinstetten, Germany) (700.00/176.03 MHz) (1H/13C) spectrometer; for ESI MS (positive and negative ion modes), an Agilent 6510 Q-TOF apparatus (Agilent Technology, Santa Clara, CA, USA), sample concentration of 0.01 mg/mL; and for HPLC, an Agilent 1100 apparatus with a differential refractometer (Agilent Technology, Santa Clara, CA, USA). The column was a Supelco Discovery HS F5-5 (10 × 250 mm, 5 μm) (Supelco, inc., Bellefonte, PA, USA).
Silchenko A.S., Kalinovsky A.I., Avilov S.A., Andrijaschenko P.V., Popov R.S., Dmitrenok P.S., Chingizova E.A, & Kalinin V.I. (2020). Kurilosides A1, A2, C1, D, E and F—Triterpene Glycosides from the Far Eastern Sea Cucumber Thyonidium (= Duasmodactyla) kurilensis (Levin): Structures with Unusual Non-Holostane Aglycones and Cytotoxicities. Marine Drugs, 18(11), 551.
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4

Detailed Characterization of Compound

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Specific rotation, Perkin-Elmer 343 Polarimeter (Perkin-Elmer, Waltham, MA, USA); NMR, Bruker Avance III 700 Bruker FT-NMR (Bruker BioSpin GmbH, Rheinstetten, Germany) (700.00/176.03 MHz) (1H/13C) spectrometer; ESI MS (positive and negative ion modes), Agilent 6510 Q-TOF apparatus (Agilent Technology, Santa Clara, CA, USA), sample concentration 0.01 mg/mL; HPLC, Agilent 1260 Infinity II with a differential refractometer (Agilent Technology, Santa Clara, CA, USA); column Phenomenex Synergi Fusion RP (10 × 250 mm, 5 μm) (Phenomenex, Torrance, CA, USA).
Silchenko A.S., Kalinovsky A.I., Avilov S.A., Andrijaschenko P.V., Popov R.S., Dmitrenok P.S., Chingizova E.A, & Kalinin V.I. (2021). Triterpene Glycosides from the Far Eastern Sea Cucumber Thyonidium (=Duasmodactyla) kurilensis (Levin): The Structures, Cytotoxicities, and Biogenesis of Kurilosides A3, D1, G, H, I, I1, J, K, and K1. Marine Drugs, 19(4), 187.
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5

Spectroscopic Analysis of Chemical Compounds

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We used specific rotation with a PerkinElmer 343 Polarimeter (PerkinElmer, Waltham, MA, USA); NMR, Bruker AMX 500 (Bruker BioSpin GmbH, Rheinstetten, Germany) (500.12/125.67 MHz (1H/13C) spectrometer; ESI MS (positive and negative ion modes), Agilent 6510 Q-TOF apparatus (Agilent Technology, Santa Clara, CA, USA)), sample concentration 0.01 mg/mL; HPLC, Agilent 1260 Infinity II with a differential refractometer (Agilent Technology, Santa Clara, CA, USA); and columns Supelcosil LC-Si (4.6 × 150 mm, 5 µm) and Ascentis RP-Amide (10 × 250 mm, 5 µm) (Supelco, Bellefonte, PA, USA) and Phenomenex Synergi Fusion RP (10 × 250 mm, 5 µm) (Phenomenex, Torrance, CA, USA).
Silchenko A.S., Avilov S.A., Andrijaschenko P.V., Popov R.S., Chingizova E.A., Dmitrenok P.S., Kalinovsky A.I., Rasin A.B, & Kalinin V.I. (2022). Structures and Biologic Activity of Chitonoidosides I, J, K, K1 and L-Triterpene Di-, Tri- and Tetrasulfated Hexaosides from the Sea Cucumber Psolus chitonoides. Marine Drugs, 20(6), 369.
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6

Comprehensive Analytical Characterization

Check if the same lab product or an alternative is used in the 5 most similar protocols
Specific rotation, PerkinElmer 343 Polarimeter (PerkinElmer, Waltham, MA, USA); NMR, Bruker AMX 500 (Bruker BioSpin GmbH, Rheinstetten, Germany) (500.12/125.67 MHz (1H/13C) spectrometer; ESI MS (positive and negative ion modes), Agilent 6510 Q-TOF apparatus (Agilent Technology, Santa Clara, CA, USA), sample concentration 0.01 mg/mL; HPLC, Agilent 1260 Infinity II with a differential refractometer (Agilent Technology, Santa Clara, CA, USA); columns Supelcosil LC-Si (4.6 × 150 mm, 5 µm) and Ascentis RP-Amide (10 × 250 mm, 5 µm) (Supelco, Bellefonte, PA, USA).
Silchenko A.S., Kalinovsky A.I., Avilov S.A., Andrijaschenko P.V., Popov R.S., Chingizova E.A., Kalinin V.I, & Dmitrenok P.S. (2021). Triterpene Glycosides from the Far Eastern Sea Cucumber Psolus chitonoides: Chemical Structures and Cytotoxicities of Chitonoidosides E1, F, G, and H. Marine Drugs, 19(12), 696.
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