Mo foil (99.95%) was purchased from Alfa Aesar, manually thinned and cut into pieces of required dimensions using steel and tungsten micro-tools. MgO (100 μm, <100> plane orientation) and Al2O3 (100 μm, <0001> c-plane orientation) single-crystal plates were obtained from MTI Corporation. Rhenium DAC gaskets, as well as MgO and Al2O3 parts for the sample encapsulation assembly, were prepared using the laser micromachining system at HPCAT19 .
Mo foil
Manufactured by Thermo Fisher Scientific
Mo foil is a thin sheet of molybdenum metal. Molybdenum is a refractory metal known for its high melting point and resistance to corrosion. The foil form provides a versatile material for various applications requiring a durable, high-temperature-resistant metal.
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Lab products found in correlation
3 protocols using mo foil
1
Fabrication of High-Pressure Samples
2
Synthesis of High-Purity Mo2C Crystals
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Three-layer, 25-μm-thick Cu foil (Alfa Aesar, 99.95% purity) was cut into pieces and placed on a 50-μm-thick Mo foil (Alfa Aesar, 99.95% purity). The Cu/Mo substrate was placed in a single-temperature-zone CVD system and heated to above 1096 °C under 200 sccm Ar (type I method, see below). The other Mo foil was placed near the Cu/Mo substrate (type II method). CH4 (5 sccm) and H2 (300 sccm) were introduced into the chamber to grow the Mo2C crystals. Finally, the tube furnace was naturally cooled to room temperature before collecting the Mo2C sample.
3
Laser-Fabricated Metal-Based Batteries
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An ultraviolet laser prototyping system (LPKF U4) defined the shapes of the anodes and cathodes from foils of Mg (50 or 100 µm, Alibaba), Zn (10 or 20 µm, Alibaba), Mo (5 or 50 µm, Alibaba), and W (50 µm, Alibaba) and from foils of Fe (3 or 25 µm, Alfa Aesar). Mg-Fe, Mg-Mo, and Mg-W batteries incorporated anodes of Mg, cathodes of Fe, Mo, or W, and electrolytes of phosphate buffered solution (PBS, Sigma-Aldrich). Mg-MoO3 and Zn-MoO3 batteries combined anodes of Mg or Zn with MoO3 cathodes, respectively, in PBS electrolytes. Mixing 0.45 g MoO3 (Sigma Aldrich), 0.05 g carbon black, and 800 µL of 300 mg/mL poly (D,L-lactide-co-glycolide) (PLGA, lactide/glycolide 65:35, Mw 40 to 75k, Sigma-Aldrich) in ethyl acetate within a planetary mixer (Thinky ARE-30) yielded a slurry for the MoO3 cathode. Mo gauze (40 mesh, Alfa Aesar) and Mo foil (5 or 50 µm) served as current collectors for the cathode materials. Applying the slurries on these current collectors and baking at 65 °C for 30 min completed the process.
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