Ethyl isothiocyanate (97%), butyl isothiocyanate (99%), allyl isothiocyanate (99.7%), phenyl isothiocyanate (99%), 4-methoxyphenyl isothiocyanate (98%), 4-methylphenyl isothiocyanate (97%), benzyl isothiocyanate (98%), phenylEthyl isothiocyanate (98.5%), and quercetin (>95%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). 4-Hydroxybenzyl isothiocyanate (98%) was purchased from Santacruz Biotechnologies (Santacruz, TX, USA). Thin-layer chromatography (TLC) plates (250 μm thickness, 2−25 μm particle size) were purchased from Macherey–Nagel (Macherey-Nagel, Düren, Germany). Sepabeads resin styrenic adsorbent (130 Å porosity) was obtained from Sorbtech (Peachtree Corners, GA, USA). LC-MS grade acetonitrile, water, and formic acid, and ACS-grade n-hexane, ethyl acetate, acetone, chloroform, and methanol were purchased from Sigma-Aldrich. Moringa seeds collected in West Bengal, India, were purchased from Amazon (Bellevue, WA, USA) in May 2019.
4 methoxyphenyl isothiocyanate
Manufactured by Merck Group
Sourced in United States
4-methoxyphenyl isothiocyanate is a chemical compound used in various laboratory applications. It is a colorless to pale yellow liquid with a characteristic odor. The compound is often utilized as a precursor or intermediate in organic synthesis and chemical research.
Automatically generated - may contain errors
Lab products found in correlation
Benzyl isothiocyanate, by Merck Group (1 mentions)
Ethylisothiocyanate, by Merck Group (1 mentions)
Butyl isothiocyanate, by Merck Group (1 mentions)
Phenylethyl isothiocyanate, by Merck Group (1 mentions)
Phenyl isothiocyanate, by Merck Group (1 mentions)
Allyl isothiocyanate, by Merck Group (1 mentions)
Lc ms grade acetonitrile, by Merck Group (1 mentions)
Chloroform, by Merck Group (1 mentions)
Acetone, by Merck Group (1 mentions)
Methanol, by Merck Group (1 mentions)
Formic acid, by Merck Group (1 mentions)
Quercetin, by Merck Group (1 mentions)
Ethyl acetate, by Merck Group (1 mentions)
Thin layer chromatography plates, by Macherey-Nagel (1 mentions)
Cyclohexyl isothiocyanate, by Merck Group (1 mentions)
Spectrum bx ft ir spectrometer, by PerkinElmer (1 mentions)
Vnmrs spectrometer, by Agilent Technologies (1 mentions)
4 nitrophenyl isothiocyanate, by Merck Group (1 mentions)
Spectrum one ft ir spectrophotometer, by PerkinElmer (1 mentions)
1 indanone, by Merck Group (1 mentions)
3 protocols using 4 methoxyphenyl isothiocyanate
1
Isothiocyanate Compounds and Quercetin Analysis
2
Synthesis and Characterization of Isothiocyanate Compounds
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4-(Trifluorophenyl) isothiocyanate, 4-fluorophenyl isothiocyanete, 4-(methoxyphenyl) isothiocyanate, 2,4-dichlorophenyl isothiocyanate, 2,6-dimethyl isothiocyanate, p-tolyl isothiocyanate and cyclohexyl isothiocyanate were purchased from Sigma Aldrich and Merck. The solvents were dried and distilled according to the standard procedures.
Infrared spectra were recorded on a Perkin-Elmer FT-IR System Spectra BX over the range 4000-500 cm -1 . All NMR measurements were carried out on a Varian 600 Spectrometer operating at 600 MHz. 13 C-NMR was acquired on an Agilent VNMRS Spectrometer at 125 MHz. The chemical shifts were reported in δ (ppm) with respect to the internal standard TMS. Attenuated total reflectance Fourier transform infrared (ATR-FTIR) spectroscopy measurements were recorded using a Perkin-Elmer Spectrum BX FT-IR spectrometer over the range of 4000-500 cm -1 . Melting points (ºC) were measured using the Schmelzpunktbestimmer SMP II melting point apparatus.
Infrared spectra were recorded on a Perkin-Elmer FT-IR System Spectra BX over the range 4000-500 cm -1 . All NMR measurements were carried out on a Varian 600 Spectrometer operating at 600 MHz. 13 C-NMR was acquired on an Agilent VNMRS Spectrometer at 125 MHz. The chemical shifts were reported in δ (ppm) with respect to the internal standard TMS. Attenuated total reflectance Fourier transform infrared (ATR-FTIR) spectroscopy measurements were recorded using a Perkin-Elmer Spectrum BX FT-IR spectrometer over the range of 4000-500 cm -1 . Melting points (ºC) were measured using the Schmelzpunktbestimmer SMP II melting point apparatus.
3
Characterization of Indanone Derivatives
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Melting points (uncorrected) were determined on a Thomas Hoover apparatus. Thin layer chromatography (TLC) was used to monitor reactions. IR spectra were recorded as KBr pellets using a Perkin Elmer Spectrum One FT-IR spectrophotometer. 1 H and 13 C NMR spectra were recorded on a Bruker 500 MHz spectrometer. High resolution mass spectra were acquired on Bruker micrOTOF-Q II spectrometer. 1-indanone, 5,6-dimethoxy-1indanone, 4-fluorophenyl isothiocyanate, 4-nitrophenyl isothiocyanate, and 4methoxyphenyl isothiocyanate were purchased from Sigma-Aldrich and used as received.
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