Rapid auto

Manufactured by Rigaku

The RAPID-AUTO is a high-speed X-ray diffraction (XRD) system designed for automated powder sample analysis. It features a high-intensity X-ray source, a high-speed detector, and an automated sample handling system. The RAPID-AUTO is capable of performing rapid, high-resolution XRD measurements on a variety of powder samples.

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Lab products found in correlation

Crystalstructure, by Rigaku (16 mentions) R axis rapid diffractometer, by Rigaku (2 mentions) Rapid 2, by Rigaku (1 mentions) Raxis spider ip diffractometer, by Rigaku (1 mentions) Ultima 4, by Rigaku (1 mentions) Crystalclear, by Rigaku (1 mentions)

30 protocols using rapid auto

X-ray Structure Determination Protocol

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Data collection: RAPID-AUTO (Rigaku, 1998 ▶ ); cell refinement: RAPID-AUTO; data reduction: CrystalClear (Rigaku/MSC, 2002 ▶ ); program(s) used to solve structure: SHELXS97 (Sheldrick, 2008 ▶ ); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▶ ); molecular graphics: DIAMOND (Brandenburg, 1999 ▶ ); software used to prepare material for publication: SHELXTL (Sheldrick, 2008 ▶ ).

Qiu Z.Z., Jing B., Li Q.X, & Zhu A.X. (2014). 4,4′-{[1,2-Phenylenebis(methylene)]bis(oxy)}dibenzoic acid dimethylformamide disolvate. Acta Crystallographica Section E: Structure Reports Online, 70(Pt 5), o534-o535.

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Single Crystal X-Ray Diffraction

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Data collection: RAPID-AUTO (Rigaku, 1998 ▶ ); cell refinement: RAPID-AUTO; data reduction: CrystalStructure (Rigaku/MSC, 2006 ▶ ); program(s) used to solve structure: SHELXS97 (Sheldrick, 2008 ▶ ); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▶ ); molecular graphics: ORTEPII (Johnson, 1976 ▶ ); software used to prepare material for publication: SHELXL97.

Li J.Q., Mu D, & Fan M.B. (2014). Bis[5-(pyridin-2-yl-κN)tetrazolido-κN 1]copper(II). Acta Crystallographica Section E: Structure Reports Online, 70(Pt 3), m79.

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Single Crystal X-Ray Diffraction

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Data collection: RAPID-AUTO (Rigaku, 2011 ▸ ); cell refinement: RAPID-AUTO; data reduction: RAPID-AUTO; program(s) used to solve structure: Il Milione (Burla et al., 2007 ▸ ); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▸ ); molecular graphics: CrystalStructure (Rigaku, 2011 ▸ ); software used to prepare material for publication: CrystalStructure.

Morimoto Y., Ogawa K., Uto Y., Nagasawa H, & Hori H. (2015). Crystal structure of (2-{[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl](5-methyl-2H-pyrrol-2-ylidene)methyl}-5-methyl-1H-pyrrolido-κ2 N,N′)difluoridoboron. Acta Crystallographica Section E: Crystallographic Communications, 71(Pt 9), o694-o695.

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Single Crystal X-ray Diffraction Protocol

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Data collection: RAPID-AUTO (Rigaku, 2001 ▸ ); cell refinement: RAPID-AUTO; data reduction: RAPID-AUTO; program(s) used to solve structure: SIR92 (Altomare et al., 1994 ▸ ); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▸ ); molecular graphics: CrystalStructure (Rigaku, 2010 ▸ ); software used to prepare material for publication: CrystalStructure.

Begum M.S., Zangrando E., Sheikh M.C., Miyatake R, & Hossain M.M. (2015). Crystal structure of S-octyl (E)-3-(4-methoxybenzylidene)dithiocarbazate. Acta Crystallographica Section E: Crystallographic Communications, 71(Pt 4), o265-o266.

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X-ray Crystallographic Analysis Protocol

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Data collection: RAPID-AUTO (Rigaku, 2006 ▶ ); cell refinement: RAPID-AUTO; data reduction: RAPID-AUTO; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008 ▶ ); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▶ ); molecular graphics: locally modified version of ORTEP (Johnson, 1965 ▶ ); software used to prepare material for publication: WinGX (Farrugia, 2012 ▶ ).

Lee Y., Yoon W, & Yun H. (2014). The mixed-metal tris(disulfide) thiophosphate, KNb1.77Ta0.23PS10. Acta Crystallographica Section E: Structure Reports Online, 70(Pt 2), i8.

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Cultivation and Structural Characterization of PNBA Crystals

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The single crystals of PNBA form (I), (I)·DMSO solvate, (I)·DMF-solvate, (I)·NMP-solvate and (I)·DMA-solvate were cultivated using the slow solvent evaporation method. A saturated solution (2 ml) of PNBA sealed with plastic film was placed into an oven and kept at 298.15 K. Then, crystals of PNBA form (I) and solvates with suitable sizes for single crystal X-ray diffraction were collected after several days. The single-crystal data collection was conducted at 113 K on a Rigaku Rapid II diffractometer, Mo Kα radiation (λ = 0.71073 Å). Data collection and processing were performed with Rapid-auto (Rigaku/MSC, 2004 ▸ ). Data reduction and cell refinement were performed with SHELXS-97 (Sheldrick, 2008 ▸ ) and SHELXL-97 (Sheldrick, 2015 ▸ ), respectively.

Zong S., Wang J., Wu H., Liu Q., Hao Y., Huang X., Wu D., Zhou G, & Hao H. (2019). Insight into the role of pre-assembly and desolvation in crystal nucleation: a case of p-nitrobenzoic acid. Acta Crystallographica Section B, Structural Science, Crystal Engineering and Materials, 75(Pt 5), 845-854.

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Single Crystal X-ray Diffraction Protocol

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Howlader M.B., Begum M.S., Sheikh M.C., Miyatake R, & Zangrando E. (2015). Crystal structure of bis[S-hexyl 3-(4-methylbenzylidene)dithiocarbazato-κ2 N 3,S]nickel(II). Acta Crystallographica Section E: Crystallographic Communications, 71(Pt 2), m26-m27.

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Crystal Structure Determination Protocol

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Data collection: RAPID-AUTO (Rigaku, 2009 ▸ ); cell refinement: RAPID-AUTO; data reduction: RAPID-AUTO; program(s) used to solve structure: SIR2011 (Burla et al., 2012 ▸ ); program(s) used to refine structure: SHELXL2013 (Sheldrick, 2015 ▸ ); molecular graphics: CrystalStructure (Rigaku, 2014 ▸ ); software used to prepare material for publication: CrystalStructure.

Ishii T., Sakane G., Yoshihara A., Fukada K, & Senoo T. (2015). Crystal structure of β-d,l-psicose. Acta Crystallographica Section E: Crystallographic Communications, 71(Pt 5), o289-o290.

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Single Crystal X-Ray Diffraction of POM-AMB-acy

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A red single crystal of POM-AMB-acy with three dimensions of 0.40 mm × 0.50 mm × 0.50 mm was selected for diffraction analysis. The data collection was performed on a Rigaku RAXIS-SPIDER IP diffractometer at 50 kV and 20 mA, using graphite monochromatized Mo K_α radiation (λ = 0.71073 Å) at 94(2) K. Data collection, data reduction, cell refinement, and experimental absorption correction were performed with the software package of Rigaku RAPID AUTO (Rigaku, 1998, Ver2.30). Structures were solved by direct methods and refined against F² by full matrix least squares. All non-hydrogen atoms, except disordered atoms, were refined anisotropically. Hydrogen atoms were generated geometrically. All calculations were performed using the SHELXS-97 program package.

She S., Bian S., Huo R., Chen K., Huang Z., Zhang J., Hao J, & Wei Y. (2016). Degradable Organically-Derivatized Polyoxometalate with Enhanced Activity against Glioblastoma Cell Line. Scientific Reports, 6, 33529.

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Single-Crystal Diffraction at 90K

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Single-crystal diffraction measurements at 90 K for crystals of A and B, immersed in a paratone N-oil and mounted on Micro Mounts holder, were conducted using Rigaku R-axis RAPID diffractometer. Collected data were processed by using RAPID AUTO (Rigaku). Crystal structures were solved by a direct method with SIR2011 (ref. 12 (link)) for A and SHELXS97 (ref. 13 (link)) for B using CrystalStructure 4.2 crystallographic software package¹⁴ with the exception of refinement, which was performed using SHELXL-2018/3 (ref. 15 ) by a full-matrix least-squares technique. For disordered parts, isotropic refinements were performed. The disordered model was fixed with some restraints and constraints. Molecular graphics were prepared using Mercury 3.8 software.^{16 (link)}

Kumar K., Abe D., Komori-Orisaku K., Stefańczyk O., Nakabayashi K., Shakirova J.R., Tunik S.P, & Ohkoshi S.I. (2019). Neodymium β-diketonate showing slow magnetic relaxation and acting as a ratiometric thermometer based on near-infrared emission. RSC Advances, 9(41), 23444-23449.

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