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5 protocols using zinc undecylenate

1

Synthesis of Semiconductor Nanocrystals

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Zinc undecylenate (99%), OA (99%), OAM (99%),
ODE (90%), indium (III) chloride (InCl3) (99%), P(TMS)3 (95%), and Zn(acac)2 (99.995%) were purchased
from Sigma-Aldrich. ODE was purified at 100 °C by evacuating
and refilling repeatedly with nitrogen for 1 h. All the procedures
were performed in a glovebox under a nitrogen atmosphere.
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2

Synthesis of Colloidal Nanocrystals

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Indium chloride (InCl3) (99.99%, trace metals basis), hexadecylamine (HDA‐98%), zinc undecylenate (98%), 1‐octadecene (ODE‐technical grade, 90%), stearic acid (SA) (98%), tris(trimethylsilyl)phosphine (P(TMS)3) (95%), sulfur (99.98%, trace metals basis), zinc stearate (Zn(St)2‐technical grade), and trioctylphosphine (TOP‐97%) were used from Sigma–Aldrich.
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3

Synthesis of Colloidal Nanocrystals

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Zinc undecylenate (99%), OA (99%), OAM (99%),
ODE (90%), indium(III) chloride (InCl3) (99%), P(TMS)3 (95%), Zn(St)2, TOP, sulfur (S) (reagent grade,
powder, purified by refining, −100 mesh particle size), and
zinc acetylacetonate hydrate [Zn(acac)2] (99.995%) were
purchased from Sigma-Aldrich. ODE was purified at 120 °C by evacuating
and refilling repeatedly with nitrogen for 1 h. All the procedures
were performed in a glovebox under a nitrogen atmosphere.
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4

Synthesis of Quantum Dots

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Indium chloride (InCl3) (99.99%, trace metals basis), HDA (98%), zinc undecylenate (98%), 1‐octadecene (ODE‐technical grade, 90%), stearic acid (SA) (98%), tris(trimethylsilyl)phosphine (P(TMS)3) (95%), sulfur (99.98%, trace metals basis), zinc stearate (Zn(St)2‐technical grade), and trioctylphosphine (TOP‐97%) were used from Sigma‐Aldrich.
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5

Colloidal Nanocrystal Synthesis Protocol

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Zinc undecylenate (99%), oleic acid (OA) (99%),
oleylamine (OAM) (99%), 1-octadecene (ODE) (90%), indium chloride
(InCl3) (99%), Tris(trimethylsilyl)phosphine (P(TMS)3) (95%), and zinc acetylacetonate hydrate (Zn(acac)2) were purchased from Sigma-Aldrich. ODE was purified at 100 °C
by evacuation and refilling with nitrogen for 1 h. All the procedures
were performed in a nitrogen-filled glovebox with an O2 level below 1 ppm using anhydrous solvents.
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