For this study, SubPc (99%), mCP (99%), TPBi (99%), C545T (99%), TAPC (99%), and PTB7 (Mw > 50,000) were obtained from Lumtec Inc., C60 (99%) and C70 (99%) were obtained from MER Corporation, MoO3 (99%) and BCP (98%) were obtained from Alfa Aesar, chloroform (99%), 3-mercaptopropionic acid (99%), octane (98%), oleic acid (tech. grade 90%) acetonitrile (99.5%), and methyl acetate (anhydrous) were obtained from Sigma–Aldrich, selenium dioxide (99.8%) and 1-octadecene (90%) were obtained from Acros Organics. All materials above were used as received. The NPD (99%) was synthesized by the Dow Chemical Company and purified once by temperature-gradient sublimation69 (link). Cadmium myristate was prepared on a multi-gram scale according to the method reported by Chen et al.70 (link).
3 mercaptopropionic acid
Manufactured by Thermo Fisher Scientific
Sourced in United States
3-mercaptopropionic acid is a chemical compound with the molecular formula CH₃CH₂CH₂SH. It is a clear, colorless liquid with a pungent odor. The compound is commonly used as a chemical intermediate in various industrial and research applications.
Automatically generated - may contain errors
Lab products found in correlation
Octane, by Thermo Fisher Scientific (2 mentions)
Oleic acid, by Merck Group (2 mentions)
1 octadecene, by Thermo Fisher Scientific (2 mentions)
Oleylamine, by Merck Group (2 mentions)
Indium acetate, by Merck Group (2 mentions)
Sodium borohydride, by Merck Group (2 mentions)
Hydrochloric acid (hcl), by Merck Group (2 mentions)
Oleic acid, by Thermo Fisher Scientific (1 mentions)
Chloroform, by Thermo Fisher Scientific (1 mentions)
Methyl acetate, by Merck Group (1 mentions)
Acetonitrile, by Merck Group (1 mentions)
1 octadecene, by Merck Group (1 mentions)
Zinc acetate, by Merck Group (1 mentions)
Sulfur powder, by Merck Group (1 mentions)
Copper iodide, by Merck Group (1 mentions)
Trimethylamine, by Avantor (1 mentions)
Allylamine, by Thermo Fisher Scientific (1 mentions)
Hexachlorocyclotriphosphazene, by Thermo Fisher Scientific (1 mentions)
Cetyltrimethylammonium bromide ctab, by Avantor (1 mentions)
Deuterated chloroform, by Eurisotop (1 mentions)
15 protocols using 3 mercaptopropionic acid
1
Organic Materials Synthesis and Purification
2
Synthesis of Copper-Indium-Zinc Sulfide
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Zinc acetate (Zn(OAc)2, 99.99%), indium acetate (In(OAc)3, 99.99%), oleylamine (OAm, 95%), 1-octadecene (ODE, 97%), sulfur powder (99.99%) were purchased from Aldrich, copper iodide (CuI, 99.99%), 3-mercaptopropionic acid (MPA, 99%) were obtained from Alfa Aesar. All reagents were used as received without further treatments.
3
Synthesis of Hexachlorocyclotriphosphazene Derivatives
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Hexachlorocyclotriphosphazene (98%) was purchased from Acros organics; 3-mercaptopropionic acid (99%) and allylamine (>98%) from Alfa Aesar (Karlsruhe, Germany); 2,2-dimethoxy-2-phenylacetophenone (DMPA) (99%) and (3-mercaptopropyl)trimethoxysilane (95%) were obtained from Sigma-Aldrich (Vienna, Austria); anhydrous THF, trimethylamine and cetyltrimethylammonium bromide (CTAB) (≥99%) from VWR (Vienna, Austria); ethanol (99%) from Fluorochem (Derbyshire, UK); and NaOH (98%) from J. T. Baker (Fisher Scientific, Wien, Austria). Deuterated chloroform and methanol for NMR experiments from Eurisotop (Saint Aubin, France). Triethylamine was distilled before usage for the substitution reaction. All other chemicals and solvents were used as received.
4
Synthesis of Gold Nanoparticles Using CTAB
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Cetyltrimethylammonium bromide (CTAB, ≥99.9%), l -ascorbic acid (AA, 100%), sodium borohydride (NaBH4, ≥99%), trisodium citrate dihydrate (Na3C6H5O7·2H2O, Na3Cit), gold chloride hydrate (HAuCl4·xH2O, 99.999%) and poly(ethylene glycol) methyl ether thiol (thiolated polyethylene glycol, PEG–SH, average Mn = 2000) were obtained from Sigma-Aldrich. Cetyltrimethylammonium chloride (CTAC, ≥98%) was obtained from Wako. Sodium hydroxide (NaOH, 1 M), anhydrous ethanol (C2H5OH ≥ 99.9%) and dichloromethane (CH2Cl2 ≥99.5%) were obtained from Daejung. 3-Mercaptopropionic acid (MPA ≥ 99%) was purchased from Alfa Aesar. Si wafers and wet oxidized (300 nm) SiO2/Si wafers were purchased from DASOM RMS. These chemicals were used without further purification with deionized water (Pure Water Corporation). Fluorine-doped tin oxide (FTO, 8 Ω □−1) was purchased from Wooyang GMS. Titanium dioxide (TiO2), tungsten oxide (WO3) and hematite (α-Fe2O3) were purchased from Kojundo Chemical (grain shape, 99.9%).
5
Colloidal Nanocrystal Synthesis Protocol
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Copper(I) iodide (CuI, 99.998%), indium(III) iodide (InI3, 99.999%), and 3-mercaptopropionic acid (MPA, 99%) were purchased from Alfa-Aesar. Dichloromethane (99.8%), oleylamine (OAm, technical grade), oleic acid (OAc, technical grade), trioctylphosphine (TOP, 97%), selenium (99.99%), 1-dodecanethiol (DDT, 98%), 1-octylamine (OcAm, 99%), zinc nitrate hexahydrate (Zn(NO3)2·6H2O, 98%), sodium sulfide (Na2S), and sodium sulfite (Na2SO3, ≥98.0%) were purchased from Sigma-Aldrich. Ethanol (99.5% anhydrous), mEthanol (99.5%), chloroform (99.95%), and sodium hydroxide (NaOH, 99.8%) were purchased from Samchun Chemicals. n-Butanol (99%) was purchased from Daejung Chemicals & Metals. The OAm was dried under a vacuum before use.
6
Synthesis of Colloidal Nanocrystals
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Indium acetate (In(OAc), 99.99%, Sigma‐Aldrich), oleic acid (OA, 90%), hexane (95% anhydrous, Sigma‐Aldrich), 2‐methyltetrahydrofuran (2‐meTHF, 99.0% anhydrous, Sigma‐Aldrich), 2‐methylanisole (2‐MA, 99.0%, Sigma‐Aldrich), toluene (99.5%, Sigma‐Aldrich), 1,2‐ethanedithiol (EDT, 99.0%, Sigma‐Aldrich), ethanethiol (ET, 97%, Sigma‐Aldrich), chlorobenzene (CB, 99.8% anhydrous, Sigma‐Aldrich), acetonitrile (ACN, 99.5%, Sigma‐Aldrich), ethyl acetate (EA, 99.5%, Sigma‐Aldrich), chloroform (CF, 99.8%, Sigma‐Aldrich), butylamine (BTA, 99.5%, Sigma‐Aldrich), benzoic acid (BA, 99.5%, Sigma‐Aldrich), nitrosyl tetrafluoroborate (NOBF4, 95%, Sigma‐Aldrich), and dioctylamine (DOA, 97%, Sigma‐Aldrich) were purchased and used as received. The compounds 1‐octadecene (ODE, 90%, Alfa Aesar), octane (98%, Alfa Aesar), and 3‐mercaptopropionic acid (MPA, 99%, Alfa Aesar) were purchased and used without further purification. 1‐butanol (BuOH, 99.8%) was purchased from Junsei chemical, ME (99%) was purchased from Daejung, and Tris(trimethylsilyl)arsine ((TMSi)3As, 99%) was purchased from JSI Silicone and was distilled before use.
7
Catechin Quantification in Green Tea Extract
8
SARS-CoV-2 Spike Protein Detection
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Phosphate buffered saline (PBS), glycine, hydrochloric acid and tyrosine were purchased from Sigma Aldrich (USA). Tris(2-carboxyethyl) phosphine (TCEP) and 3-mercaptopropionic acid (MPA) were purchased from Thermo Scientific (USA). Recombinant spike S1 protein of SARS-CoV-2 (molecular weight = 78.3 KDa) and anti S1 monoclonal antibody were purchased from Sino Biological Inc. (China). Erythropoietin, troponin and insulin were purchased from Abcam (Australia). All preparations were made using deionized water (ultrapure Millipore, 18.2 MΩ cm, 25 °C). Gold coated silicon nanopillar substrate (Au@SNP) was outsourced from Silmeco ApS (Denmark), molecular sieve columns (illustra NAP-5) were outsourced from GE Healthcare Life Science (Australia).
9
Optimized Biomolecular Conjugation Protocol
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All the following chemicals were purchased from Sigma-Aldrich: skimmed milk powder (70,166), 2-(N-Morpholino)ethanesulfonic acid monohydrate MES (69,889), Sodium dodecyl sulfate (L3771), Glycine (G8898), Ammonium persulfate (A3678), Agarose (A9539), Trizma base (T1503), Tween 20 (P1379), Ethylenediaminetetraacetic acid disodium salt dihydrate, EDTA (E4884), N,N,N′,N′-Tetramethylethylenediamine (T9281), Acrylamide/bis-acrylamide,40% solution (A7802), , DL-Dithiothreitol (D5545), Ethanol (32,294–2), Methanol (24,229–2), Phosphate buffered saline PBS tablet (P4417), 3-Mercaptopropionic acid (M5801), Cadmium chloride (202,908), 4-Aminophenyl β-D -galactopyranoside (A9545), Sodium borhydride (S9125), N-(3-Dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride (E6383), N-Hydroxysulfosuccinimide sodium salt (56,485).Tellurium, 99.8%, powder (315,990,250) was purchased from Acros Organics.
10
Synthesis of Fluorescent Silica Nanoparticles
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Cadmium chloride hemipentahydrate (CdCl2·2.5 H2O; >98%), sodium borohydride (NaBH4; 99%), tetraethyl orthosilicate (TEOS, 98%), L-Arginine (>98%), rhodamine 6G (99% dye content), rhodamine 800, and silica nanoparticles (12 nm, surface area 175–225 m2/g, purity 99.8%) were obtained from Aldrich (Milwaukee, WI, USA). Zinc chloride (ZnCl2; 99.99%), 3-mercaptopropionic acid (MPA), and selenium powder (Se; 99.5+%, 200 mesh) were obtained from Acros (Geel, Belgium). Sodium hydroxide (NaOH) and ammonium hydroxide (NH4OH; 28%–30%) were obtained from Mallinckrodt Chemicals (Phillipsburg, NJ, USA). All chemicals were used without further purification. The H2O used in this study was purified by a Barnstead NANOpure Infinity ultrapure water system (Dubuque, IA, USA).
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