All commercially available solvents and reagents were analytical grade or better and were directly used without further purification unless otherwise stated. Silica gel was obtained from Yantai Xinnuo Chemical Industry Co., Ltd. (Shandong, China). Diethylenetriaminepentaacetic acid, nitrolotriacetic acid, 1-hexene (99%), 1-heptene (99%), 1-hexa-decene (95%) and 1-octa-decene (≥95%) were from Shanghai Macklin Biochemical Co., Ltd. (Shanghai, China). Butanedioic anhydride was from Tianjin Guangfu Fine Chemical Research Institute (Tianjin, China). 1-Octene (99%) and norbornene (99%) were from J&K Scientific Ltd. (Beijing, China). 1-Do-decene (95%) and 1-tetra-decene (99%) were from Meryer Chemical Technology Co., Ltd. (Shanghai, China). 1-Decene (≥95%) was from Adamas Reagent Co., Ltd. (Shanghai China). Dichloromethylhexylsilane (98%) was from CNW Technologies Co., Ltd. (Nordrhein Westfalen, Germany). cis-2-Hexene was from Alfa Aesar Co., Ltd. (Massachusetts, USA). H2PtCl6·6H2O and cyclohexene (≥98%) were from Tianjin Kemat Chemical Technology Co., Ltd. (Tianjin, China). CDCl3 was from Energy Chemical Co., Ltd. (Shanghai, China). Other solvents were obtained from Tianjin Jiangtian Scientific Co., Ltd. (Tianjin, China).
Cdcl3
Manufactured by Energy Chemical
Sourced in China
CDCl3 is a deuterated chloroform solvent commonly used in nuclear magnetic resonance (NMR) spectroscopy. It serves as a reference compound and solvent for the analysis of organic compounds.
Automatically generated - may contain errors
Lab products found in correlation
Fticr ms spectrometer, by Bruker (2 mentions)
Alpha t spectrometer, by Bruker (2 mentions)
Dmso d6, by Energy Chemical (2 mentions)
1 hexene, by Maclin Biochemical Technology (1 mentions)
1 octadecene, by Maclin Biochemical Technology (1 mentions)
2 2 bipyridine, by Energy Chemical (1 mentions)
Cd3cn, by Cambridge Isotopes (1 mentions)
Ethidium bromide, by Merck Group (1 mentions)
Phosphate buffer saline (pbs), by Solarbio (1 mentions)
Av 400 spectrometer, by Bruker (1 mentions)
D8 venture x diffractometer, by Bruker (1 mentions)
Dimethyl sulfoxide (dmso), by Tianjin Damao (1 mentions)
Sodium hydroxide (naoh), by Guangzhou Chemical (1 mentions)
Dichloromethane, by Tianjin Damao (1 mentions)
Anhydrous ethanol, by Tianjin Damao (1 mentions)
Acetonitrile, by Tianjin Damao (1 mentions)
Tetrahydrofuran thf, by Tianjin Damao (1 mentions)
7 protocols using cdcl3
1
Solvent-Assisted Synthesis of Alkenes
2
Synthesis of Amino Acid Esters
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Ethyl L-tryptophanate hydrochloride was purchased from Tokyo Chemical Industry Co. Ltd. (Tokyo, Japan). L-arginine ethyl ester dihydrochloride, L-cysteine ethyl ester hydrochloride and CDCl3 were purchased from Energy Chemical (Shanghai, China). Ethyl L-phenylalaninate hydrochloride, ethyl L-serinate hydrochloride, ethyl L-alaninate hydrochloride, ethyl L-valinate hydrochloride, ethyl L-leucinate hydrochloride, L-isoleucine ethyl ester hydrochloride, ethyl L-methionate hydrochloride, diethyl L-glutamate hydrochloride, diethyl L-aminosuccinate hydrochloride and sodium tetrakis (3,5-bis(trifluoromethyl)phenyl) borate were purchased from Adamas Reagent, Ltd. (Shanghai, China). Ethyl D-serinate hydrochloride, ethyl D-phenylalaninate hydrochloride and ethyl D-tryptophanate hydrochloride were purchased from Bide Pharmatech Ltd. (Shanghai, China). HPLC chloroform was purchased from Chron Chemicals (Chengdu, China). All reagents purchased from commercial suppliers were used without further purification.
3
Purification and Characterization of Pyridine Derivatives
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4,4′-Bipyridine, 2,2′-bipyridine, 4-phenylpyridine, 2-phenylpyridine, CDCl3, and HPLC CD3CN were purchased from Energy Chemical. CD3CN was purchased from Cambridge Isotope Laboratories (CIL). HPLC CHCl3 and CH3CN were purchased from Chron Chemicals (Chengdu, China). All reagents purchased from commercial suppliers were used without further purification.
4
Multifunctional Polymer Nanocomposite Synthesis
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1,4-Butanediol (BDO), methylene-bis(4-cyclohexylisocyanate) (HMDI), stannous octoate, and CDCl3 were purchased from Energy Chemical Co. Ltd (Shanghai, China). Poly(ethylene glycol)-block-poly(propylene glycol)-block-poly(ethylene glycol) (Pluronic L-81, average Mn ∼ 2800) and ethidium bromide (EB) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Poly(perfluoroethoxy)difluoroethyl PEG ether (E10H, Mn ∼ 1700) and acridine orange (AO) were purchased from Alfa Aesar Chemical Co. Ltd (Shanghai, China). Tryptone, yeast extract powder, agar powder, and glucose were purchased from Beijing Oboxing Biotechnology Co., Ltd (Beijing China). Phosphate buffer saline (PBS) was purchased from Beijing Solarbio Science & Technology Co., Ltd (Beijing China). Other solvents were all purchased from Tianjin Damao Chemical Reagent Factory (Tianjin, China). Oil-soluble AgNPs (50 nm) was purchased from Nanjing XFNANO Materials Tech Co., Ltd (Nanjing, Jiangsu, China). All commercially available reagents and solvents were used directly without further purification.
5
Synthesis and Characterization of Novel Compounds
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All the reagents were of analytical grade and used without further purification. Melting points were determined on a Beijing Taike melting point apparatus (X-4) (Taike, Beijing, China) and were uncorrected. IR spectra were obtained on a Bruker ALPHA-T spectrometer (BRUKER Inc., Beijing, China). 1H NMR and 13C NMR spectra were recorded on a Bruker AV400 spectrometer (BRUKER Inc., Beijing, China) with CDCl3 (Energy Chemical., Shanghai, China) as the solvent and TMS (Energy Chemical., Shanghai, China) as the internal standard. HRMS spectra were recorded on an FTICR-MS spectrometer (BRUKER Inc.). X-ray diffraction data were recorded on a BRUKER D8 VENTURE X-diffractometer (BRUKER Inc.) with Mo Kα radiation (λ = 0.71073 Å) at 273(2) K.
6
Synthesis of Aromatic Compounds
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3,3′-Diaminobenzidine, glutaric acid, and bromopentane (n-C5H11Br) were purchased from Energy chemical technology (Shanghai) Co. Ltd. Polyphosphoric acid (PPA) was purchased from Macklin biochemical technology Co. Ltd. All soluble metal ion salts and sodium hydroxide (NaOH) are purchased from Guangzhou Chemical reagent factory. All the nitroaromatic compounds purchased from Guangzhou Chemical reagent factory. Tetrahydrofuran (THF), acetonitrile (MeCN), anhydrous ethanol (EtOH), dimethyl formamide (DMF), dichloro-methane (DCM), and dimethyl sulfoxide (DMSO) were purchased from Tianjin Damao chemical reagent factory. DMSO-d6 and CDCl3 were purchased from Energy chemical technology (Shanghai) Co. Ltd. All these reagents were used without further purification.
7
Spectroscopic Characterization of Compounds
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All the reagents were analytical grade, and were used without further purification. The IR spectra were recorded on a Bruker ALPHA-T spectrometer (BRUKER Inc., Beijing, China). The 1H-NMR and 13C-NMR spectra were recorded on a Bruker AVANVE 300 MHz (BRUKER Inc., Beijing, China) using CDCl3 (Energy Chemical., Shanghai, China) or DMSO-d6 (Energy Chemical., Shanghai, China) as solvent and TMS (Energy Chemical., Shanghai, China) as internal standard. The melting point was measured on a Beijing Taike melting point apparatus (X-4) (Beijing, China), and was uncorrected. The high-resolution mass spectrometry was recorded on a FT-ICR MS spectrometer (BRUKER Inc., Beijing, China). The spectrogram datas of compounds could be found in the Supplementary Materials .
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