With the exception of phenol (Moravek Biochemicals, Brea, CA) and toluene (American Radiolabeled Chemicals, St. Louis, MO), all 14C-labeled reagents (aniline, benzoic acid, chlorobenzene, phthalic acid, p-toluic acid, and salicylic acid) were obtained from Sigma-Aldrich.
P toluic acid
P-toluic acid is a chemical compound with the formula CH3C6H4COOH. It is a colorless crystalline solid that is a derivative of toluene. P-toluic acid is used as an intermediate in the production of various chemicals, pharmaceuticals, and other industrial applications.
Lab products found in correlation
2 protocols using p toluic acid
Purification and Characterization of Organic Compounds
With the exception of phenol (Moravek Biochemicals, Brea, CA) and toluene (American Radiolabeled Chemicals, St. Louis, MO), all 14C-labeled reagents (aniline, benzoic acid, chlorobenzene, phthalic acid, p-toluic acid, and salicylic acid) were obtained from Sigma-Aldrich.
Synthesis and Characterization of Benzyl and tert-Butyl Isocyanides
Reactions were carried out using a CEM Discover microwave synthesis unit.
1H–NMR and 13C–NMR spectra were obtained using a Bruker DRX 400 MHz spectrometer. Mass spectrometry was performed on an Agilent Technologies 6520 Accurate-Mass Q-TOF LC/MS connected to an Agilent Technologies1200 HPLC system with UV detector and autosampler.
Radio-HPLC analysis was performed on an Agilent Technologies 1200 Series with UV detector (254 nm) and Lablogic β + radio-detector using an Agilent Eclipse XDB-C18 column (5 μm, 4.6 × 150 mm). The following mobile phase conditions were used: solvent A: H2O + 0.1% TFA; solvent B: MeOH +0.1% TFA; time:%B 0:5, 1:5, 10:95, 18:5, 23:5. Flow rate was 1 mL/min.
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