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2 protocols using δ bhc

1

Comprehensive Pesticide Residue Analysis

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Pesticide reference standards including malathion, diazinon, profenofos, primiphos-methy, chlorpyrifos-methyl, monocrotophos, dimethoate, cypermethrin, deltamethrin, fenpropathrin, oxamyl, imidacloprid, acetamiprid, metalaxyl, difenoconazole, α-BHC, β-BHC, γ-BHC, δ-BHC, heptachlor, aldrin, heptachlor epoxide, trans-chlordane, α-endosulfan, β-endosulfan, cis-chlordane trans-nonachlor, dieldrin, P-P-DDE, endrin, cis-nonachlor, P-P-DDD, endosulfan-sulfate, P,P-DDT, and methoxychlor were purchased from Dr. Ehrenstorfer GmbH (Augsburg, Germany), with certified purity ranging from 97% to 99%. Acetonitrile, tolune, ammonia solution, sodium chloride, acetic acid, triphenylphosphate (TPP), and ethoprophos were obtained from Merck (Darmstadt, Germany), and anhydrous magnesium sulfate, Bondesil sorbents (primary and secondary amine; PSA particle size 40 μm), and graphite carbon black (GCB) from Sigma-Aldrich (St. Louis, MO, USA). All the organic solvents used were higher performance liquid chromatography (HPLC) grade.
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2

Pesticide and Heavy Metal Analysis Protocol

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All pesticides standards including α-BHC(100 mg L−1), β-BHC (100 mg L−1), γ-BHC (100 mg L−1), δ-BHC (100 mg L−1), p,p′-DDE (100 mg L−1), o,p′-DDT (100 mg L−1), p,p′-DDT (100 mg L−1), p,p′-DDD (100 mg L−1), azoxystrobin (99.0%), carbendazim (99.0%), chlorothalonil (98.9%), chlorpyrifos (99.5%), cypermethrin (98.2%), chlorantraniliprole (98.2%), dichlorvos (99.7%), difenoconazole (99.2%), fenpropathrin (98.9%), isocarbophos (98.9%), procymidone (99.5%), prochloraz (99.2%), pyraclostrobin (98.1%), thiophanate-methyl (99.3%), tebuconazole (99.5%) and λ-cyhalothrin (93.5%) were purchased from Dr Ehrenstorfer GmbH (Augsburg, Germany). Acetonitrile (HPLC grade) were provided by Bangyi Chemical Co., Ltd. (Hangzhou, China). Anhydrous magnesium sulphate, anhydrous sodium sulphate and n-hexane were of analytical grade. Primary secondary amine (PSA) was provided by Agela Technologies.
Each single element stock solution (1000 mg L−1) of Cu, Zn, Cr, Ni, Pb, As, Cd, and Hg were purchased from National Standard Material Research Centre (Beijing, China). Guaranteed reagent nitric acid (HNO3) was provided by Fanhong Trading Co., Ltd. (Guangzhou, China).
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