Butyl bromide

Manufactured by Merck Group

Butyl bromide is a chemical compound commonly used in laboratory settings. It is a colorless, volatile liquid with a characteristic odor. Butyl bromide is primarily used as a reactant or intermediate in various chemical synthesis processes.

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2 protocols using butyl bromide

Synthesis and Characterization of Novel Ionic Liquids

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Chemicals and reagents (viz., 1-methyl imidazole; pyridine; diethylamine (DEA); butyl bromide; methane sulfonic acid; dichloroacetic acid; potassium hydrogen sulfate; lithium bis(trifluoromethanesulfonyl)imide (Li [Tf₂N]); sodium tetrafluoroborate (Na [BF₄]); potassium hydrogen sulfate (K[HSO₄]); sodium hydroxide) were procured from Sigma Aldrich. All solvents, such as methanol (CH₃OH), chloroform (CHCl₃), acetonitrile (CH₃CN), n-Hexane, ethyl acetate, and distilled water, were purchased from Sigma Aldrich. All organic solvents were dried with the help of distillation assembly.

Hassan R., Nazir F., Roosh M., Qaisar A., Habib U., Sajini A.A, & Iqbal M. (2022). Synthesis, Characterization, Biological Evaluation, and In Silico Studies of Imidazolium-, Pyridinium-, and Ammonium-Based Ionic Liquids Containing n-Butyl Side Chains. Molecules, 27(19), 6650.

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Synthesis of 1-Butylimidazole from Imidazole

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Imidazole (Him), methyl Imidazole (mim), butyl bromide, 1,4butanesultone, sodium ethoxide, p-nitrophenyl acetate, sulfuric acid (97-98%), and sodium bisulfate used as precursors or reactants were from Sigma-Aldrich. Methanol, sulfuric ether, ethyl acetate, hexane, acetone, butyl alcohol, and dichloromethane used as solvents or eluents were from Sigma-Aldrich. 1-ButylImidazole (bim) was synthesized by reaction of Imidazole with butyl bromide through an aliphatic nucleophilic substitution, following a previously reported method that employs sodium ethoxide for deprotonating the Imidazole, 27, 28 as it described in the ESI. †

Martini M.B., Fernández J.L, & Adam C.G. (2021). Insights on the catalytic behaviour of sulfonic acid-functionalized ionic liquids (ILs) in transesterification reactions - voltammetric characterization of sulfonic task-specific ILs with bisulfate anions. Physical chemistry chemical physics : PCCP, 23(4).

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