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Mercury vxr 300

Manufactured by Agilent Technologies

The Mercury VXR-300 is a nuclear magnetic resonance (NMR) spectrometer designed for laboratory use. It operates at a frequency of 300 MHz and is capable of conducting various NMR experiments to analyze the chemical structure and properties of samples.

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2 protocols using mercury vxr 300

1

Spectroscopic Characterization and Bioactivity

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All melting points (MPs) were measured on an Electrothermal Gallenkamp apparatus (Weiss Technik, London, UK). Infrared (IR) spectra were recorded in potassium bromide disks on SP3300 (Pye Unicam, Cambridge, England) and 8101 PC (Shimadzu, Tokyo, Japan) IR spectrophotometers. 1H nuclear magnetic resonance (NMR) and 13C NMR spectra were recorded on a Varian Mercury VXR-300 spectrometer (300 MHz). Mass spectra were recorded on Shimadzu GCMS-Q1000-EX and GCMS 5988-A HP spectrometers, and ionizing voltage was 70 eV. Elemental analyses were carried out at the Microanalytical Center of Cairo University, Giza, Egypt. Biological evaluation of the products was carried out in the Microbiology Division of the Microanalytical Center of Cairo University.
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2

Characterization of Newly Synthesized Compounds

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An electrothermal Gallenkamp apparatus was operated to measure the melting points for the newly synthesized compounds. A Pye-Unicam SP300 instrument in potassium bromide discs was used to measure IR spectra. A Varian Mercury VXR-300 spectrometer (300 MHz for 1H-NMR and 75 MHz for 13C-NMR) was manipulated to measure the 1H-NMR and 13C-NMR spectra, and the chemical shifts were related to those of the solvent. GCMS-Q1000-EX Shimadzu and GCMS 5988-A HP spectrometers were used to record the mass spectra of the samples at an ionizing voltage of 70 eV. Elemental analyses were carried out at the Microanalytical Centre of Cairo University, Giza, Egypt.
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