The largest database of trusted experimental protocols

Avance dpx 600

Manufactured by Bruker
Sourced in United States

The Avance-DPX 600 is a high-performance nuclear magnetic resonance (NMR) spectrometer designed for advanced research applications. It features a 600 MHz superconducting magnet and a range of hardware and software components to enable precise analysis of chemical and biological samples.

Automatically generated - may contain errors

2 protocols using avance dpx 600

1

Synthesis and Characterization of Porphyrin Complexes

Check if the same lab product or an alternative is used in the 5 most similar protocols
The unmetallated porphyrins for P242 and P343 were synthesized following previously published procedures followed by platination using the traditional PtCl2 in benzonitrile procedure.44 45 Synthetic details for P2 and P3 provided in the supporting information. 1H NMR spectra were recorded on a Bruker 400 MHz FT NMR (Model: Avance-DPX 600) and the spectral shifts are calibrated with respect to residual protonated solvent peaks (δ 7.26 and 2.49 for d6-chloroform and d6-dmso, respectively). Due to low solubility we were unable to obtain 13C NMR for the compounds.
+ Open protocol
+ Expand
2

Spectroscopic Characterization of Compounds

Check if the same lab product or an alternative is used in the 5 most similar protocols
Optical rotations were measured in MeOH using a 1.0 cm cell on a Rudolph Research (Autopol III, Hackettstown, NJ, USA). UV spectra were also recorded in MeOH on a Scinco UVS-2100 (Seoul, Korea). CD spectra were taken in MeOH in an Applied Photophysics Chirascan plus (Leatherhead, UK). IR spectra were recorded on KBr plates with a Thermo Nicolet 570 (Waltham, MA, USA). NMR spectra were recorded on a Bruker Avance DPX-600 (Billerica, MA, USA) and Bruker Ascend 700 spectrometer using MeOD as solvent. High resolution mass spectra were acquired on a JEOL, JMS-AX505WA mass spectrometer (Tokyo, Japan).
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!