Methyl sulfoxide d6

Manufactured by Thermo Fisher Scientific

Methyl sulfoxide-d6 is a deuterated organic solvent commonly used in nuclear magnetic resonance (NMR) spectroscopy. It is a clear, colorless liquid with a high boiling point and high polarity, making it a suitable solvent for a variety of organic compounds.

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Lab products found in correlation

Mercury 400 mhz nmr, by Agilent Technologies (1 mentions) Aluminum oxide, by Merck Group (1 mentions) Deuterium oxide, by Thermo Fisher Scientific (1 mentions) Catechol, by Thermo Fisher Scientific (1 mentions) Benzene boronic acid, by Thermo Fisher Scientific (1 mentions) N n dimethylformamide (dmf), by Thermo Fisher Scientific (1 mentions) Methacrylate acid, by Merck Group (1 mentions) Butyl acrylate, by Thermo Fisher Scientific (1 mentions) Methyl methacrylate, by Thermo Fisher Scientific (1 mentions) Chloroform d, by Thermo Fisher Scientific (1 mentions) Triton x 405, by Merck Group (1 mentions) Acrylic acid, by Merck Group (1 mentions)

2 protocols using methyl sulfoxide d6

NMR Characterization of Electrolytes

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¹H NMR was performed on a Varian Mercury 400 MHz NMR. The temperature was set at 25°C. Samples were prepared in the glove box by injecting 300 μl of electrolyte into a new and dried NMR tube, together with 600 μl of methyl sulfoxide-d6 (Acros Organics, 99.9% D, maximum 0.03% water impurity). It was then sealed with polytetrafluoroethylene caps and immediately put into the NMR machine for data acquisition. The samples were locked and shimmed using the external standard.

Vilá R.A., Boyle D.T., Dai A., Zhang W., Sayavong P., Ye Y., Yang Y., Dionne J.A, & Cui Y. (2023). LiH formation and its impact on Li batteries revealed by cryogenic electron microscopy. Science Advances, 9(12), eadf3609.

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Synthesis of Functional Latex Polymers

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Diethyl methylene malonate (Chemi-lian M1000, DEMM) and Forza B3100 (DEMM)₆ were provided by Sirrus Inc. (Loveland, OH). Methyl methacrylate (MMA, Fisher), butyl acrylate (BA, Acros Organics), and methacrylate acid (MAA, Sigma-Aldrich) were used as monomers for latex synthesis. 2,2′-Azobis[2-(2-imidazolin-2-yl) propane] dihydrochloride (AIBI, TCI) was used as an initiator, and Triton X-405 (Sigma-Aldrich) was used as a surfactant. Acrylic acid (AA, Sigma-Aldrich), catechol (Acros Organics), 2-vinylbenzoic acid (VBA, Fisher), and benzeneboronic acid (BBA, Alfa Aesar) were used to prepare initiators for DEMM polymerization. Aluminum oxide (Sigma-Aldrich) was used to remove the inhibitor from monomers. N,N-Dimethylformamide (DMF, Fisher) was used as an extractor. Deuterium oxide (D₂O, 99.8% atom D), chloroform-d (CDCl3, 99.8% atom D), and methyl sulfoxide-d₆ (DMSO-d₆, 99.5+% atom D) were obtained from Acros Organics. Doubly deionized (DDI) water was used throughout the work.

Huang M., Liu Y., Yang G., Klier J, & Schiffman J.D. (2019). Anionic Polymerization of Methylene Malonate for High-Performance Coatings. ACS applied polymer materials, 1(4), 657-663.

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