Trios software

Manufactured by TA Instruments

Sourced in United States, Canada, United Kingdom

TRIOS software is a comprehensive thermal analysis data analysis and reporting platform developed by TA Instruments. It provides users with tools to collect, analyze, and present data obtained from TA Instruments' thermal analysis instruments.

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TRIOS software package (8 citations) TA Trios Software (2 citations) TRIOS software V4.3 (2 citations) Trios software version 3.3.0.4055 (2 citations) TRIOS data analysis software (2 citations) TRIOS software 5.2 (2 citations) TRIOS TA Universal Analysis Software (1 citations)

149 protocols using trios software

Thermal Analysis of Humic Acids

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Thermogravimetric and differential scanning calorimetric (TG–DSC) analyses of HAs were conducted using a Discovery series SDT 650 simultaneous DSC/TGA instrument (TA Instruments Inc., New Castle, DE, USA) under the He flow rate of 50 mL·min⁻¹. The HA samples (4 mg) were placed in alumina pans without cover and heated from 50 to 650 °C at a heating rate of 20 °C·min⁻¹. TG, DSC curves, and mass loss were obtained via TRIOS software (TA Instruments, Delaware, DE, USA).
Thermogravimetric and differential scanning calorimetric (TG–DSC) analyses of HAs were conducted using a Discovery series SDT 650 simultaneous DSC/TGA instrument (TA Instruments Inc., New Castle, DE, USA) under the He flow rate of 50 mL·min⁻¹. The HA samples (4 mg) were placed in alumina pans without cover and heated from 50 to 650 °C at a heating rate of 20 °C·min⁻¹. TG, DSC curves, and mass loss were obtained via TRIOS software (TA Instruments Inc., New Castle, DE, USA).

De la Rosa J.M., Santa-Olalla A., Campos P., López-Núñez R., González-Pérez J.A., Almendros G., Knicker H.E., Sánchez-Martín Á, & Fernández-Boy E. (2022). Impact of Biochar Amendment on Soil Properties and Organic Matter Composition in Trace Element-Contaminated Soil. International Journal of Environmental Research and Public Health, 19(4), 2140.

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Thermal Analysis of Microhydrogel Samples

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A Discovery DSC (TA Instruments-Waters LLC, New Castle, USA) was used to perform the DSC measurements. The instrument is controlled by TRIOS software (TA Instruments, New Castle, DE, USA). Samples around 7 mg were placed into T-zero aluminium pans and sealed. Samples were subjected to a controlled heating rate of 10 °C/min under nitrogen purge (40 mL/min). The measurements were done in triplicate.
The water content in TP MH and NF MH II was determined using a Discovery TGA (TA Instruments, New Castle, DE, USA), which was controlled by TRIOS software (TA Instruments, New Castle, DE, USA). Samples around 7 mg were analysed in an aluminium pan and heated at 10 °C/min from 25 °C to 100 °C for TP MH and 25 °C to 200 °C for NF MH II. The measurements were done in triplicate.

Okeyo P.O., Ilchenko O., Slipets R., Larsen P.E., Boisen A., Rades T, & Rantanen J. (2019). Imaging of dehydration in particulate matter using Raman line-focus microscopy. Scientific Reports, 9, 7525.

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Thermal Analysis of IND-PAR Eutectic and CAMS

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The thermal behavior of the samples was analyzed using a Discovery DSC (TA Instruments, New Castle, DE, USA). All measurements were conducted under a constant 50 mL/min nitrogen gas flow. An amount of 2–5 mg of sample were weighed into aluminum pans and sealed with pierced lids. To measure the eutectic behavior of the samples, crystalline IND, crystalline PAR, and the PM of IND–PAR at different mixing ratios were heated up from 25 °C to 180 °C (at a rate of 10 °C/min to achieve better resolution). All measurements for the eutectic behavior investigation were conducted in triplicates. To investigate the thermal behavior of the CAMS or G-CAMS, samples were equilibrated at −20 °C for 1 min, then heated up to 180 °C (at a rate of 20 °C/min for better sensitivity). The DSC data was collected and analyzed using Trios software (version 5.1.1, TA Instruments, New Castle, DE, USA).
The water content of the samples was assessed by using thermogravimetric analysis (TGA) (Discovery TGA, TA Instruments, New Castle, DE, USA). Samples (around 10 mg) were heated from 25 °C to 300 °C at a rate of 20 °C/min. All measurements were conducted under a constant 50 mL/min nitrogen gas flow. Data was collected and analyzed using Trios software (version 5.1.1, TA Instruments, New Castle, DE, USA).

Di R., Rades T, & Grohganz H. (2023). Destabilization of Indomethacin-Paracetamol Co-Amorphous Systems by Mechanical Stress. Pharmaceutics, 16(1), 67.

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Rheological Characterization of Biomaterials

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The experimental data were statistically analyzed by determining the average values and standard deviation, at the significance level of 95%, for each parameter evaluated. Statistical analysis (RStudio, Version 1.1.423) was performed by applying variance analysis, the one factor (ANOVA), and post-hoc comparisons (Tukey test). Experimental rheology data were fitted to the non-linear Carreau model, using the TA Instruments/TRIOS software.

Graça C., Raymundo A, & Sousa I. (2022). Yogurt and curd cheese as alternative ingredients to improve the gluten-free breadmaking. Frontiers in Nutrition, 9, 934602.

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Thermal Stability Analysis of Nanofibers

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The thermal stability analysis of the nanofibers was realized on TGA 550 equipment (TA Instruments, New Castle, DE, USA). 3-5 mg of sample were placed in the chamber under a nitrogen atmosphere (N 2 ). The heating ramp was from 25 to 600°C at a rate of 5 °C/min. The results were analyzed with the TA Instruments TRIOS software (TA Instruments, New Castle, DE, USA).

Cruz-Salas C.N., Prieto C., Calderón-Santoyo M., Lagarón J.M., Ramos-Hernández J.A, & Ragazzo-Sánchez J.A. (2022). Antimutagenic and Antiproliferative Activity of the Coccoloba uvifera L. Extract Loaded in Nanofibers of Gelatin/Agave Fructans Elaborated by Electrospinning. Anti-cancer agents in medicinal chemistry, 22(15).

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Rheological Characterization of Viscoelastic Fluids

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A Discovery Hybrid Rheometer 2 (DHR-2) (TA Instruments) with attached 40 mm parallel plate at gap height of 0.25 mm and 25°C was used for all experiments. Rotational shear rate sweeps were executed between 10⁻³-10³ s⁻¹ to determine the power law region. Power-law parameter n (flow behavior index) and K (flow consistency index) were calculated using TRIOS software (TA Instruments). Rotational time sweeps were executed at three different shear rates (s⁻¹) in sequential order: 10⁻² (60 s), 3000 (5s), 10⁻² (120s) to determine shear recovery of solutions.^{[20 ]} Time to 80% recovery was manually observed/calculated.^{[47 (link)]} Oscillatory shear stress sweeps between 10⁻¹-10³ performed at 1 Hz and frequency sweeps between 10⁰-10² performed at 10 Pa to further validate yield points and investigate dependence on frequency.

Peak C.W., Singh K.A., Adlouni M., Chen J, & Gaharwar A.K. (2019). Printing Therapeutic Proteins in 3D using Nanoengineered Bioink to Control and Direct Cell Migration. Advanced healthcare materials, 8(11), e1801553.

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Rheological Characterization of Fluid Samples

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Steady state shear flow measurements were carried out at increasing shear rates from 0.1 to 100 s⁻¹ to measure the shear viscosities of samples.
Rheological data was analyzed using TRIOS software (TA Instruments, New Castle, DE, USA). Measurements were made in triplicate and average values are reported. To characterize the flow behavior of samples, the Newtonian or power law models were used. The flow behavior index (n, dimensionless) and consistency coefficient (K, Pa·sⁿ) values were computed by fitting the rheological data to the power law model (Eq. (1)).

Equation 1.

Where, τ is the shear stress (Pa) and

\dot{γ}

is the shear rate (s⁻¹). When n = 1, n < 1, and n > 1 the fluids are called Newtonian, pseudoplastic, and dilatant, respectively. The correlation coefficient (R) and standard error of estimates (SEE) were determined using Eqs. (2), (3)).

Equation 2.

Equation 3.

Where, x is the observed value, y is the estimated value,

\overline{x}

and

ȳ

are the means of observed and estimated values, respectively, and n is the count of the total number of (x,y) pairs.

Janahar J.J., Balasubramaniam V.M., Jiménez-Flores R., Campanella O.H., Patel B, & Ortega-Anaya J. (2023). Impact of ultra-shear technology on quality attributes of model dairy-pea protein dispersions with different fat levels. Current Research in Food Science, 6, 100439.

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Quantitative Mineral Analysis by TGA

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TGA of SHHs was carried out for a quantitative estimation of mineral composition [17 (link)] using a TGA5500 TA^® instrument. The temperature range was 30–600 °C with a step of 20 °C/min. Results were treated using TRIOS^® Software (TA Instrument, New Castle, DE, USA).

Hanachi A., Bianchi A., Kahn C.J., Velot E., Arab-Tehrany E., Cakir-Kiefer C, & Linder M. (2022). Encapsulation of Salmon Peptides in Marine Liposomes: Physico-Chemical Properties, Antiradical Activities and Biocompatibility Assays. Marine Drugs, 20(4), 249.

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Differential Scanning Calorimetry Analysis of Starch Samples

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Differential Scanning Calorimetry (DSC) measurements were performed with a TA Instruments differential scanning calorimeter (model DSC 2500, New Castle, DE, USA) and the collected data were evaluated using TA instruments TRIOS software (V5.1.1.46572). Temperature and cell constant calibration of the instrument were carried out with Indium reference samples and calibration of heat capacity C_p was performed with sapphire crystal, provided by TA Instruments. Samples of model system suspension (~10 mg) were placed in hermetically sealed Tzero Aluminium pans and an identical empty pan was used as a reference.
All of the samples were heated from 25 to 100 °C with a heating rate of 5 °C/min. We subtracted baselines and divided the resulting heat flow by starch mass and heating rate, thus obtaining the change in heat capacity per gram of starch as a function of temperature. The observed heat effects were characterized by calculating the change in enthalpy as the area under experimental curve and transition temperature was determined as the curve peak position. Positive changes in heat capacity correspond to endothermic processes (endo up) and negative changes in heat capacity correspond to exothermic processes (exo down).

Megusar P., Stopar D., Poklar Ulrih N., Dogsa I, & Prislan I. (2022). Thermal and Rheological Properties of Gluten-Free, Starch-Based Model Systems Modified by Hydrocolloids. Polymers, 14(16), 3242.

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Thermal Analysis of Crystalline Form I

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Example 7

Differential scanning calorimetry (DSC) was performed using a TA Instruments Model Discovery DSC. Data was collected with TRIOS software and was analyzed using TA Instruments Universal Analysis software. A sample of the crystalline form was accurately weighed into an aluminum pan covered with a TZero hermetic pinhole lid. The sample was initially cooled to −20° C. after which the sample was heated using a linear heating ramp of 10° C./min from −20° C. to 250° C. A representative DSC thermogram of Form I is shown in FIG. 2.

Thermogravimetric analysis (TGA) measurements were performed using a TA Instruments Model Discovery TGA module equipped with high resolution capability. Data were collected using TA Instruments TRIOS software and analyzed using TA Instruments Universal Analysis software. A weighed sample was placed onto a platinum pan and scanned with a heating rate of 10° C. per minute from ambient temperature to 260° C. The balance and furnace chambers were purged with nitrogen flow during use. A representative TGA trace of Form I is shown in FIG. 3. A weight loss of about 3.4% between 27° C. and 100° C. was observed and corresponds to dehydration of a monohydrate form.

US11702415B2. Crystalline hydrate of a JAK inhibitor compound (2023-07-18). THERAVANCE BIOPHARMA R&D IP, LLC [US]. Inventors: Gene Timothy Fass [US].

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