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Vnmr 500 mhz spectrometer

Manufactured by Agilent Technologies

The VNMR 500 MHz spectrometer is a nuclear magnetic resonance (NMR) instrument designed for high-resolution spectroscopic analysis. It provides a magnetic field strength of 500 MHz for the detection and characterization of chemical samples.

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2 protocols using vnmr 500 mhz spectrometer

1

Characterization of Amphiphilic Polymers

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1H, 13C, 29Si and 31P NMR spectra were recorded using either a JEOL Eclipse 300 MHz, JEOL Eclipse 400 MHz, Varian VNMR 400 MHz or Varian VNMR 500 MHz spectrometer. The chemical shifts (δ) are reported in parts per million (p.p.m.) and the coupling constants (J) in Hertz (Hz). Chemical shifts were referenced to residual dichloromethane at δ 5.32 p.p.m. (1H), and benzene at δ 7.14 p.p.m. (1H) and δ 128.06 p.p.m. (13C). 1H NMR integrations for the polymers were calculated after setting the methyl protons (6H) of PFS to 378H for PFS63-b-PDMS513, 408H for PFS68-b-PMVS670 and 360H for PFS60-b-PMVS574.
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2

Synthesis of Dihydrofuranaphthoquinones for Antifungal Screening

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All the dihydrofuranaphthoquinones used for antifungal screening against S. brasiliensis and S. schenckii were prepared from lawsone by different methods (Scheme 1) with a yield of 23–76%. The α- and β-2,3-dihydrofuranaphthoquinones 518 were prepared as previously described in the literature [35 (link),48 (link)] and were confirmed by 1H-NMR spectra recorded on a Varian VNMR (500 MHz) spectrometer using chloroform-d as a solvent and tetramethylsilane as an internal standard. The α- and β-2,3-dihydrofuranaphthoquinones 1921 were prepared from nor-lapachol, as previously described [49 (link),50 (link)].
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